Effects of organophilic-modified attapulgite nanorods on thermal and mechanical behavior of segmented polyurethane elastomers

The effects of different grafting content of 4,4′‐methlenebis(phenyl isocyanate)‐modified attapulgite (ATT‐MDI) on thermal and mechanical properties of segmented polyurethane (PU) elastomers were investigated. The ATT‐MDI nanorods with different grafting content were prepared by treating ATT with he...

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Published in	Polymer composites Vol. 31; no. 11; pp. 1890 - 1898
Main Authors	Wang, Chia-Hao, Shieh, Yeong-Tarng, Guo, Gangjian, Nutt, Steven
Format	Journal Article
Language	English
Published	Hoboken Wiley Subscription Services, Inc., A Wiley Company 01.11.2010 Wiley Blackwell Publishing Ltd
Subjects	Applied sciences Composites Elastomers Exact sciences and technology Forms of application and semi-finished materials Nanorods Polymer industry, paints, wood Polymer matrix composites Polyurethane resins Technology of polymers Clay Organic isocyanate Organic clay Mechanical properties Thermoplastic rubber Attapulgite Dispersion reinforced material Crystallinity Experimental study Composite material Tensile strength Thermal stability Surface treatment Coupling agent Polyurethane elastomer Thermal properties Morphology Concentration effect Nanocomposite
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Abstract	The effects of different grafting content of 4,4′‐methlenebis(phenyl isocyanate)‐modified attapulgite (ATT‐MDI) on thermal and mechanical properties of segmented polyurethane (PU) elastomers were investigated. The ATT‐MDI nanorods with different grafting content were prepared by treating ATT with heat and acid followed by grafting with MDI molecules. MDI‐modified ATT were characterized by transmission electron microscopy (TEM), thermogravimetric analysis (TGA), and Fourier transform infrared spectroscopy. TGA analysis revealed that at least 30 wt % of MDI was grafted/adsorbed on the surface of ATT following the modification. Three PU/ATT‐MDI nanocomposites were in situ synthesized using ATT with different grafting contents, and the materials were characterized by TEM, thermal analysis, and mechanical testing. The tensile strength and modulus increased with increasing grafting content of MDI molecules, and the crystallinity of soft and hard segments was increased by ATT‐MDI. POLYM. COMPOS., 31:1890–1898, 2010. © 2010 Society of Plastics Engineers.
AbstractList	The effects of different grafting content of 4,4′‐methlenebis(phenyl isocyanate)‐modified attapulgite (ATT‐MDI) on thermal and mechanical properties of segmented polyurethane (PU) elastomers were investigated. The ATT‐MDI nanorods with different grafting content were prepared by treating ATT with heat and acid followed by grafting with MDI molecules. MDI‐modified ATT were characterized by transmission electron microscopy (TEM), thermogravimetric analysis (TGA), and Fourier transform infrared spectroscopy. TGA analysis revealed that at least 30 wt % of MDI was grafted/adsorbed on the surface of ATT following the modification. Three PU/ATT‐MDI nanocomposites were in situ synthesized using ATT with different grafting contents, and the materials were characterized by TEM, thermal analysis, and mechanical testing. The tensile strength and modulus increased with increasing grafting content of MDI molecules, and the crystallinity of soft and hard segments was increased by ATT‐MDI. POLYM. COMPOS., 31:1890–1898, 2010. © 2010 Society of Plastics Engineers.
Author	Nutt, Steven Shieh, Yeong-Tarng Guo, Gangjian Wang, Chia-Hao
Author_xml	– sequence: 1 givenname: Chia-Hao surname: Wang fullname: Wang, Chia-Hao email: chiahaow@usc.edu organization: M.C. Gill Composites Center, Mork Family Department of Chemical Engineering and Matrials Science, University of Southern California, Los Angeles 90089-0241 – sequence: 2 givenname: Yeong-Tarng surname: Shieh fullname: Shieh, Yeong-Tarng organization: Department of Chemical and Materials Engineering, National University of Kaohsiung, Kaohsiung 811, Taiwan – sequence: 3 givenname: Gangjian surname: Guo fullname: Guo, Gangjian organization: M.C. Gill Composites Center, Mork Family Department of Chemical Engineering and Matrials Science, University of Southern California, Los Angeles 90089-0241 – sequence: 4 givenname: Steven surname: Nutt fullname: Nutt, Steven organization: M.C. Gill Composites Center, Mork Family Department of Chemical Engineering and Matrials Science, University of Southern California, Los Angeles 90089-0241
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Keywords	Clay Organic isocyanate Organic clay Mechanical properties Thermoplastic rubber Attapulgite Dispersion reinforced material Crystallinity Experimental study Composite material Tensile strength Thermal stability Surface treatment Coupling agent Polyurethane elastomer Thermal properties Morphology Concentration effect Nanocomposite
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Snippet	The effects of different grafting content of 4,4′‐methlenebis(phenyl isocyanate)‐modified attapulgite (ATT‐MDI) on thermal and mechanical properties of...
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SubjectTerms	Applied sciences Composites Elastomers Exact sciences and technology Forms of application and semi-finished materials Nanorods Polymer industry, paints, wood Polymer matrix composites Polyurethane resins Technology of polymers
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Title	Effects of organophilic-modified attapulgite nanorods on thermal and mechanical behavior of segmented polyurethane elastomers
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