Surface relief gratings inscription in linear and crosslinked azo modified epoxy‐isocyanate polymers
This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'‐metilen‐bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and ge...
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| Published in | Journal of polymer science. Part B, Polymer physics Vol. 53; no. 8; pp. 587 - 594 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Hoboken
Wiley
15.04.2015
Blackwell Publishing Ltd Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0887-6266 1099-0488 |
| DOI | 10.1002/polb.23674 |
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| Abstract | This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'‐metilen‐bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 °C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the Tgof the bulk sample. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015, 53, 587–594 |
|---|---|
| AbstractList | This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'-metilen-bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 °C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the Tg of the bulk sample. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015, 53, 587-594 ABSTRACT This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'‐metilen‐bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 °C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the Tg of the bulk sample. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015, 53, 587–594 The photoisomerization of azobenzenes gives different motions in those materials where they are incorporated. The scale range of these movements goes from little reorientations of the azobenzene groups to massive motion of polymeric material. At a macroscopic level, involve large amounts of polymeric material, which produces deformations on the surface of an azopolymer film. In this work, crosslinked azobenzene‐containing epoxy‐isocyanate polymers are prepared and even though the mobility of the azochromophores was restrained in the crosslinked network, enough of the azochromophores maintained high mobility to generate gratings of remarkable depth. This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'-metilen-bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 degree C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the T sub(g) of the bulk sample. copyright 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015, 53, 587-594 The photoisomerization of azobenzenes gives different motions in those materials where they are incorporated. The scale range of these movements goes from little reorientations of the azobenzene groups to massive motion of polymeric material. At a macroscopic level, involve large amounts of polymeric material, which produces deformations on the surface of an azopolymer film. In this work, crosslinked azobenzene-containing epoxy-isocyanate polymers are prepared and even though the mobility of the azochromophores was restrained in the crosslinked network, enough of the azochromophores maintained high mobility to generate gratings of remarkable depth. This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'‐metilen‐bis(cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 °C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the Tgof the bulk sample. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015, 53, 587–594 This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and diisocyanate (4,4'‐metilen‐ bis (cyclohexyl isocyanate), DI) with similar glass transition temperature values. The effect of the experimental and geometrical parameters (such as beams polarization direction and interference pattern spacing) on the surface modulation process was examined as well. The absence of photodegradation or bleaching was corroborated by comparing Raman spectra inside and outside the SRG zone. Being a very important subject matter, the influence of crosslinking on the inscription rates and thermal stability of SRGs was investigated. Crosslinked films with an interesting modulation and good grating stability, even at high temperatures (160 °C), were obtained. Gratings shape was retained, and significant diffraction was still observed even well above the T g of the bulk sample. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015 , 53 , 587–594 |
| Author | Galante, María J. Ainchil, Paula Zucchi, Ileana A. Sáiz, Luciana M. Oyanguren, Patricia A. |
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| Cites_doi | 10.1063/1.371393 10.1021/jp001715r 10.1021/jp953300p 10.1021/ma991803d 10.1364/AO.38.003714 10.1002/macp.200290006 10.1063/1.117292 10.1063/1.1629800 10.1557/JMR.1996.0107 10.1002/marc.201300763 10.1002/1099-1581(200008/12)11:8/12<570::AID-PAT7>3.0.CO;2-K 10.1364/AO.38.005418 10.1002/9780470439098.ch1 10.1002/macp.200500147 10.1021/ma990753 10.1021/ma00130a017 10.1016/j.polymer.2003.09.035 10.1002/adma.200305535 10.1016/j.reactfunctpolym.2012.04.010 10.1002/(SICI)1099-0518(19980130)36:2<283::AID-POLA11>3.0.CO;2-K 10.1063/1.119710 10.1039/C4TC01236D 10.1039/b900146h 10.1088/0957-4484/23/48/485309 10.1063/1.124113 10.1366/0003702021954656 10.1063/1.113541 10.1039/a902424g 10.1021/ma048804c 10.1063/1.116200 10.1021/ma980160j |
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| References_xml | – reference: D. Y. Kim, L. Li, X. L. Jiang, V. Shivshankar, J. Kumar, S. K. Tripathy, Macromolecules 1995, 28, 8835-8839. – reference: X. L. Jiang, J. Kumar, D. Y. Kim, V. Shivshankar, S. K. Tripathy, Appl. Phys. Lett. 1996, 68, 2618-2620. – reference: S. Tripathy, N. Viswanathan, S. Balasubramanian, J. Kumar, Polym. Adv. Technol. 2000, 11, 570-574. – reference: J. P. Chen, F. L. Labarthet, A. Natansohn, P. Rochon, Macromolecules 1999, 32, 8572-8579. – reference: P. Rochon, E. Batalla, A. Natanshon, Appl. Phys. Lett. 1995, 66, 136-138. – reference: T. Kimura, J. Y. Kim, T. Fukuda, H. Matsuda, Macromol. Chem. Phys. 2002, 203, 2344-2350. – reference: C. J. L. Constantino, R. F. Aroca, V. Zucolotto, L. Li, O. N. Oliveira Jr., J. Kumar, S. K. Tripathy, Appl. Spectrosc. 2002, 56, 187-191. – reference: T. S. Lee, D. Kim, X. Jiang, L. Li, J. Kumar, S. Triphathy, J. Polym. Sci. Part A: Polym Chem. 1998, 36, 283-289. – reference: A. Priimagi, C. J. Barret, A. Shishido, J. 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| Snippet | This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and... ABSTRACT This work analyses the SRG forming ability of a linear and a crosslinked polymer, both based on the same azo chromophore (Disperse Red 19, DR19) and... |
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| SubjectTerms | Azo azo polymers azobenzene Beams (radiation) bleaching Crosslinking crosslinling Diffraction gratings Diisocyanates epoxy-isocyanate polymer glass transition temperature Gratings (spectra) Modulation Networks photolysis Polarization polymers surface relief grating thermal stability thermoplastics thermosets |
| Title | Surface relief gratings inscription in linear and crosslinked azo modified epoxy‐isocyanate polymers |
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