Novel BiOBr by compositing low-cost biochar for efficient ciprofloxacin removal: the synergy of adsorption and photocatalysis on the degradation kinetics and mechanism insight
C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis...
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| Published in | RSC advances Vol. 11; no. 25; pp. 15369 - 15379 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
26.04.2021
The Royal Society of Chemistry |
| Subjects | |
| Online Access | Get full text |
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| Abstract | C/BiOBr composite materials were synthesized
via
a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi-O-C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, &z.rad;O
2
−
and h
+
played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis.
1. The C-loaded BiOBr was synthesized
via
a one-step solvothermal method. 2. C/BiOBr showed an obvious synergistic effect of adsorption and photocatalysis on the degradation of ciprofloxacin. |
|---|---|
| AbstractList | C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi-O-C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, ˙O2 - and h+ played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi-O-C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, &z.rad;O 2 − and h + played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. 1. The C-loaded BiOBr was synthesized via a one-step solvothermal method. 2. C/BiOBr showed an obvious synergistic effect of adsorption and photocatalysis on the degradation of ciprofloxacin. C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi–O–C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, ·O2− and h+ played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. C/BiOBr composite materials were synthesized a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi-O-C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, ˙O and h played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi–O–C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, ˙O 2 − and h + played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw. The samples were characterized by SEM, XRD, XPS and PL. The 2% C/BiOBr composite material showed a noticeable adsorption and photocatalysis synergistic effect to remove CIP. The adsorption rate and degradation rate were 1.45 times and 1.8 times that of BiOBr. The adsorption kinetics and isotherms of CIP on C/BiOBr were analyzed with the pseudo-second-order kinetic and Langmuir models. The degradation efficiency was 96.8% after 60 min of irradiation. High stability and degradability were still maintained after four cycles. The Bi–O–C bond accelerated electron transition and inhibited the rapid photogenerated electron pair recombination. In the degradation process of CIP, ˙O 2 − and h + played a significant role. Experiments proved that C/BiOBr is practical and feasible for the degradation of CIP under the synergistic effect of adsorption and photocatalysis. 1. The C-loaded BiOBr was synthesized via a one-step solvothermal method. 2. C/BiOBr showed an obvious synergistic effect of adsorption and photocatalysis on the degradation of ciprofloxacin. |
| Author | Song, Wandi Wang, Chengyu Liu, Shuxia Liu, Wang Chang, Haibo Zhao, Jianghua Xie, Xiuhong |
| AuthorAffiliation | Changchun University College of Resources and Environment Jilin Agricultural University College of Landscape Architecture |
| AuthorAffiliation_xml | – name: Changchun University – name: Jilin Agricultural University – name: College of Landscape Architecture – name: College of Resources and Environment |
| Author_xml | – sequence: 1 givenname: Wandi surname: Song fullname: Song, Wandi – sequence: 2 givenname: Jianghua surname: Zhao fullname: Zhao, Jianghua – sequence: 3 givenname: Xiuhong surname: Xie fullname: Xie, Xiuhong – sequence: 4 givenname: Wang surname: Liu fullname: Liu, Wang – sequence: 5 givenname: Shuxia surname: Liu fullname: Liu, Shuxia – sequence: 6 givenname: Haibo surname: Chang fullname: Chang, Haibo – sequence: 7 givenname: Chengyu surname: Wang fullname: Wang, Chengyu |
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| Snippet | C/BiOBr composite materials were synthesized
via
a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost... C/BiOBr composite materials were synthesized a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost straw.... C/BiOBr composite materials were synthesized via a simple one-step solvothermal method, with C derived from biochar, which was prepared from the low-cost... |
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| SubjectTerms | Adsorption Chemistry Composite materials Degradation Electron transitions Kinetics Low cost Photocatalysis Synergistic effect X ray photoelectron spectroscopy |
| Title | Novel BiOBr by compositing low-cost biochar for efficient ciprofloxacin removal: the synergy of adsorption and photocatalysis on the degradation kinetics and mechanism insight |
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