Synthesis of hierarchical porous zinc oxide (ZnO) microspheres with highly efficient adsorption of Congo red
[Display omitted] Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption–desorption, and Fou...
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| Published in | Journal of colloid and interface science Vol. 490; pp. 242 - 251 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier Inc
15.03.2017
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption–desorption, and Fourier transform infrared spectroscopy analyses. The as-prepared porous ZnO exhibits microsphere morphologies with diameters of 6–8μm, which are assembled from two-dimensional nanosheets. The as-prepared hierarchical porous ZnO microspheres possessed high specific surface areas (57m2/g), and were evaluated for adsorption of Congo red (CR) in aqueous solution. The adsorption kinetics data were described by the pseudo-second-order kinetics and intraparticle diffusion models, while the equilibrium adsorption data were well fitted to the Langmuir model, with a maximum adsorption amount of 334mg/g. The as-prepared hierarchical porous ZnO exhibited higher CR adsorption capacity than commercial ZnO and various other materials, and thus could be an effective adsorbent for removal of anionic organic dyes from wastewater. |
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| AbstractList | Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption, and Fourier transform infrared spectroscopy analyses. The as-prepared porous ZnO exhibits microsphere morphologies with diameters of 6-8μm, which are assembled from two-dimensional nanosheets. The as-prepared hierarchical porous ZnO microspheres possessed high specific surface areas (57m
/g), and were evaluated for adsorption of Congo red (CR) in aqueous solution. The adsorption kinetics data were described by the pseudo-second-order kinetics and intraparticle diffusion models, while the equilibrium adsorption data were well fitted to the Langmuir model, with a maximum adsorption amount of 334mg/g. The as-prepared hierarchical porous ZnO exhibited higher CR adsorption capacity than commercial ZnO and various other materials, and thus could be an effective adsorbent for removal of anionic organic dyes from wastewater. [Display omitted] Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption–desorption, and Fourier transform infrared spectroscopy analyses. The as-prepared porous ZnO exhibits microsphere morphologies with diameters of 6–8μm, which are assembled from two-dimensional nanosheets. The as-prepared hierarchical porous ZnO microspheres possessed high specific surface areas (57m2/g), and were evaluated for adsorption of Congo red (CR) in aqueous solution. The adsorption kinetics data were described by the pseudo-second-order kinetics and intraparticle diffusion models, while the equilibrium adsorption data were well fitted to the Langmuir model, with a maximum adsorption amount of 334mg/g. The as-prepared hierarchical porous ZnO exhibited higher CR adsorption capacity than commercial ZnO and various other materials, and thus could be an effective adsorbent for removal of anionic organic dyes from wastewater. Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption–desorption, and Fourier transform infrared spectroscopy analyses. The as-prepared porous ZnO exhibits microsphere morphologies with diameters of 6–8μm, which are assembled from two-dimensional nanosheets. The as-prepared hierarchical porous ZnO microspheres possessed high specific surface areas (57m²/g), and were evaluated for adsorption of Congo red (CR) in aqueous solution. The adsorption kinetics data were described by the pseudo-second-order kinetics and intraparticle diffusion models, while the equilibrium adsorption data were well fitted to the Langmuir model, with a maximum adsorption amount of 334mg/g. The as-prepared hierarchical porous ZnO exhibited higher CR adsorption capacity than commercial ZnO and various other materials, and thus could be an effective adsorbent for removal of anionic organic dyes from wastewater. Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption, and Fourier transform infrared spectroscopy analyses. The as-prepared porous ZnO exhibits microsphere morphologies with diameters of 6-8μm, which are assembled from two-dimensional nanosheets. The as-prepared hierarchical porous ZnO microspheres possessed high specific surface areas (57m2/g), and were evaluated for adsorption of Congo red (CR) in aqueous solution. The adsorption kinetics data were described by the pseudo-second-order kinetics and intraparticle diffusion models, while the equilibrium adsorption data were well fitted to the Langmuir model, with a maximum adsorption amount of 334mg/g. The as-prepared hierarchical porous ZnO exhibited higher CR adsorption capacity than commercial ZnO and various other materials, and thus could be an effective adsorbent for removal of anionic organic dyes from wastewater. |
| Author | Cheng, Bei Yu, Jiaguo Jiang, Chuanjia Lei, Chunsheng Pi, Meng |
| Author_xml | – sequence: 1 givenname: Chunsheng surname: Lei fullname: Lei, Chunsheng organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, PR China – sequence: 2 givenname: Meng surname: Pi fullname: Pi, Meng organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, PR China – sequence: 3 givenname: Chuanjia surname: Jiang fullname: Jiang, Chuanjia organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, PR China – sequence: 4 givenname: Bei surname: Cheng fullname: Cheng, Bei organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, PR China – sequence: 5 givenname: Jiaguo surname: Yu fullname: Yu, Jiaguo email: jiaguoyu@yahoo.com organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, PR China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/27912123$$D View this record in MEDLINE/PubMed |
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Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized... Hierarchical porous zinc oxide (ZnO) was successfully synthesized via a facile hydrothermal method followed by calcination, and characterized by X-ray... |
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| SubjectTerms | adsorbents adsorption Adsorption isotherm Anionic dye aqueous solutions Congo red dyes Fourier transform infrared spectroscopy Hierarchical porous structure hot water treatment microparticles nanosheets nitrogen scanning electron microscopy sorption isotherms transmission electron microscopy wastewater X-ray diffraction Zinc oxide |
| Title | Synthesis of hierarchical porous zinc oxide (ZnO) microspheres with highly efficient adsorption of Congo red |
| URI | https://dx.doi.org/10.1016/j.jcis.2016.11.049 https://www.ncbi.nlm.nih.gov/pubmed/27912123 https://www.proquest.com/docview/1845836982 https://www.proquest.com/docview/2116873105 |
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