Enhancing photocatalytic activity on gas-phase heavy metal oxidation with self-assembled BiOI/BiOCl microflowers
[Display omitted] A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM),...
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| Published in | Journal of colloid and interface science Vol. 546; pp. 32 - 42 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier Inc
15.06.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), scanning electron microscopy (SEM). The composition information and bonding energy structure of the BiOI/BiOCl microflowers were studied by X-ray diffraction (XRD) and high-resolution X-ray photoelectron spectra (XPS), Fourier Transform Infrared Spectroscopy (FTIR), UV–vis diffuse reflectance spectroscopy (DRS) analysis and photoluminescence (PL) spectra. The photocatalytic performance of as-prepared BiOI/BiOCl microflowers was tested through photocatalytic oxidation of gas-phase mercury, as a useful catalyst (or additive) in wet electrostatistic precipitator (WESP) to capture heavy metals including mercury. The results show that the prepared BiOI/BiOCl samples demonstrate higher photocatalytic efficiency than pure BiOI or BiOCl. By optimizing the component ratio of the BiOI and BiOCl, up to 72.2% oxidation efficiency can be achieved in BiOI/BiOCl microflowers. Finally, the photocatalytic influence of BiOI/BiOCl microflowers on gas-phase mercury oxidation had been proposed. |
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| AbstractList | A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), scanning electron microscopy (SEM). The composition information and bonding energy structure of the BiOI/BiOCl microflowers were studied by X-ray diffraction (XRD) and high-resolution X-ray photoelectron spectra (XPS), Fourier Transform Infrared Spectroscopy (FTIR), UV-vis diffuse reflectance spectroscopy (DRS) analysis and photoluminescence (PL) spectra. The photocatalytic performance of as-prepared BiOI/BiOCl microflowers was tested through photocatalytic oxidation of gas-phase mercury, as a useful catalyst (or additive) in wet electrostatistic precipitator (WESP) to capture heavy metals including mercury. The results show that the prepared BiOI/BiOCl samples demonstrate higher photocatalytic efficiency than pure BiOI or BiOCl. By optimizing the component ratio of the BiOI and BiOCl, up to 72.2% oxidation efficiency can be achieved in BiOI/BiOCl microflowers. Finally, the photocatalytic influence of BiOI/BiOCl microflowers on gas-phase mercury oxidation had been proposed.A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), scanning electron microscopy (SEM). The composition information and bonding energy structure of the BiOI/BiOCl microflowers were studied by X-ray diffraction (XRD) and high-resolution X-ray photoelectron spectra (XPS), Fourier Transform Infrared Spectroscopy (FTIR), UV-vis diffuse reflectance spectroscopy (DRS) analysis and photoluminescence (PL) spectra. The photocatalytic performance of as-prepared BiOI/BiOCl microflowers was tested through photocatalytic oxidation of gas-phase mercury, as a useful catalyst (or additive) in wet electrostatistic precipitator (WESP) to capture heavy metals including mercury. The results show that the prepared BiOI/BiOCl samples demonstrate higher photocatalytic efficiency than pure BiOI or BiOCl. By optimizing the component ratio of the BiOI and BiOCl, up to 72.2% oxidation efficiency can be achieved in BiOI/BiOCl microflowers. Finally, the photocatalytic influence of BiOI/BiOCl microflowers on gas-phase mercury oxidation had been proposed. A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), scanning electron microscopy (SEM). The composition information and bonding energy structure of the BiOI/BiOCl microflowers were studied by X-ray diffraction (XRD) and high-resolution X-ray photoelectron spectra (XPS), Fourier Transform Infrared Spectroscopy (FTIR), UV–vis diffuse reflectance spectroscopy (DRS) analysis and photoluminescence (PL) spectra. The photocatalytic performance of as-prepared BiOI/BiOCl microflowers was tested through photocatalytic oxidation of gas-phase mercury, as a useful catalyst (or additive) in wet electrostatistic precipitator (WESP) to capture heavy metals including mercury. The results show that the prepared BiOI/BiOCl samples demonstrate higher photocatalytic efficiency than pure BiOI or BiOCl. By optimizing the component ratio of the BiOI and BiOCl, up to 72.2% oxidation efficiency can be achieved in BiOI/BiOCl microflowers. Finally, the photocatalytic influence of BiOI/BiOCl microflowers on gas-phase mercury oxidation had been proposed. [Display omitted] A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been developed. The physicochemical structure of BiOI/BiOCl microflowers were characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), scanning electron microscopy (SEM). The composition information and bonding energy structure of the BiOI/BiOCl microflowers were studied by X-ray diffraction (XRD) and high-resolution X-ray photoelectron spectra (XPS), Fourier Transform Infrared Spectroscopy (FTIR), UV–vis diffuse reflectance spectroscopy (DRS) analysis and photoluminescence (PL) spectra. The photocatalytic performance of as-prepared BiOI/BiOCl microflowers was tested through photocatalytic oxidation of gas-phase mercury, as a useful catalyst (or additive) in wet electrostatistic precipitator (WESP) to capture heavy metals including mercury. The results show that the prepared BiOI/BiOCl samples demonstrate higher photocatalytic efficiency than pure BiOI or BiOCl. By optimizing the component ratio of the BiOI and BiOCl, up to 72.2% oxidation efficiency can be achieved in BiOI/BiOCl microflowers. Finally, the photocatalytic influence of BiOI/BiOCl microflowers on gas-phase mercury oxidation had been proposed. |
| Author | Guan, Dayong Lu, Jia Yan, Naiqiang Liu, Qizhen Sun, Xiaoming Wu, Jiang |
| Author_xml | – sequence: 1 givenname: Xiaoming surname: Sun fullname: Sun, Xiaoming organization: College of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China – sequence: 2 givenname: Jia surname: Lu fullname: Lu, Jia organization: College of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China – sequence: 3 givenname: Jiang surname: Wu fullname: Wu, Jiang email: wjcfd2002@163.com organization: College of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China – sequence: 4 givenname: Dayong surname: Guan fullname: Guan, Dayong organization: College of Electric and Information Engineering, Tongji University, Shanghai 200092, China – sequence: 5 givenname: Qizhen surname: Liu fullname: Liu, Qizhen organization: Shanghai Environment Monitoring Center, Shanghai 200030, China – sequence: 6 givenname: Naiqiang surname: Yan fullname: Yan, Naiqiang organization: Environmental Science and Engineering College, Shanghai Jiao Tong University, Shanghai 200240, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30901690$$D View this record in MEDLINE/PubMed |
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| Keywords | BiOI/BiOCl Template-free coprecipitation Wet electrostatistic precipitator Microflower heterostructure Heavy metal |
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28 Yan (10.1016/j.jcis.2019.03.049_b0180) 2015; 634 Ye (10.1016/j.jcis.2019.03.049_b0210) 2011; 21 Huang (10.1016/j.jcis.2019.03.049_b0245) 2015; 7 Xu (10.1016/j.jcis.2019.03.049_b0055) 2017; 51 Ma (10.1016/j.jcis.2019.03.049_b0035) 2018; 219 Sun (10.1016/j.jcis.2019.03.049_b0165) 2017; 218 Huang (10.1016/j.jcis.2019.03.049_b0005) 2016 Huang (10.1016/j.jcis.2019.03.049_b0075) 2016; 5 Xiang (10.1016/j.jcis.2019.03.049_b0125) 2016; 71 Bao (10.1016/j.jcis.2019.03.049_b0140) 2011; 40 Yang (10.1016/j.jcis.2019.03.049_b0145) 2016; 423 Mehraj (10.1016/j.jcis.2019.03.049_b0105) 2016; 387 Sun (10.1016/j.jcis.2019.03.049_b0120) 2015; 5 Yu (10.1016/j.jcis.2019.03.049_b0070) 2019 Zhang (10.1016/j.jcis.2019.03.049_b0190) 2016; 686 Bai (10.1016/j.jcis.2019.03.049_b0175) 2016; 194 Xu (10.1016/j.jcis.2019.03.049_b0060) 2017; 51 Chai (10.1016/j.jcis.2019.03.049_b0205) 2009; 262 Zhang (10.1016/j.jcis.2019.03.049_b0100) 2006; 68 |
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A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature... A one-pot synthetic approach to prepare self-assembled BiOI/BiOCl microflowers by a template-free coprecipitation method at room temperature has been... |
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| SubjectTerms | ambient temperature BiOI/BiOCl catalysts coprecipitation energy Fourier transform infrared spectroscopy gases Heavy metal heavy metals mercury Microflower heterostructure oxidation photocatalysis photoluminescence reflectance spectroscopy scanning electron microscopy Template-free coprecipitation transmission electron microscopy Wet electrostatistic precipitator X-ray diffraction X-ray photoelectron spectroscopy |
| Title | Enhancing photocatalytic activity on gas-phase heavy metal oxidation with self-assembled BiOI/BiOCl microflowers |
| URI | https://dx.doi.org/10.1016/j.jcis.2019.03.049 https://www.ncbi.nlm.nih.gov/pubmed/30901690 https://www.proquest.com/docview/2196517152 https://www.proquest.com/docview/2221008677 |
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