Application of ZnO nanorods as an adsorbent material for the removal of As(III) from aqueous solution: kinetics, isotherms and thermodynamic studies

Removal of metals from wastewaters causes a big concern from the environmental point of view due to their extreme toxicity towards aquatic life and humans. Application of As(III) from aqueous solution by ZnO nanorods as adsorbent has been investigated in the present study. The synthesized nanorods w...

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Published inInternational journal of industrial chemistry Vol. 9; no. 1; pp. 17 - 25
Main Authors Yuvaraja, Gutha, Prasad, Cheera, Vijaya, Yarramuthi, Subbaiah, Munagapati Venkata
Format Journal Article
LanguageEnglish
Published Berlin/Heidelberg Springer Berlin Heidelberg 01.03.2018
Springer Nature B.V
Subjects
Adsorbents
Aqueous solutions
Arsenic
Chemistry
Chemistry and Materials Science
Environmental Chemistry
Fourier transforms
Industrial Chemistry/Chemical Engineering
Infrared spectroscopy
Isotherms
Kinetics
Nanochemistry
Nanorods
Polymer Sciences
Sorption
Thermogravimetric analysis
Toxicity
Zinc oxide
ZnO nanorods
Thermodynamics
Kinetics
Isotherms
As(III)
Online AccessGet full text
ISSN2228-5970
2228-5547
DOI10.1007/s40090-018-0136-5

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Abstract Removal of metals from wastewaters causes a big concern from the environmental point of view due to their extreme toxicity towards aquatic life and humans. Application of As(III) from aqueous solution by ZnO nanorods as adsorbent has been investigated in the present study. The synthesized nanorods were characterized by XRD, FT-IR spectroscopy, SEM, and thermogravimetric analysis. Optimum biosorption conditions were determined with respect to pH, adsorbent dose, contact time, and temperature. The experimental data were examined using the Lagergren’s first-order, pseudo-second-order and intraparticle diffusion kinetic models. The results revealed that the pseudo-second-order kinetic model provided the best description of the data. Langmuir and Freundlich isotherm models were applied to the equilibrium data. The maximum As(III) sorption capacity of ZnO nanorods was found to be 52.63 mg/g at pH 7, adsorbent dose 0.4 g, contact time 105 min, and temperature 323 K. The calculated thermodynamic parameters, Δ G o (between − 5.741, − 5.342 and − 4.538 kJ/mol at 303–323 K), ∆ H o (13.75 kJ/mol) and ∆ S o (0.0616 J/mol K) showed that the sorption of As(III) onto ZnO nanorods was feasible, spontaneous and exothermic, respectively.
AbstractList Removal of metals from wastewaters causes a big concern from the environmental point of view due to their extreme toxicity towards aquatic life and humans. Application of As(III) from aqueous solution by ZnO nanorods as adsorbent has been investigated in the present study. The synthesized nanorods were characterized by XRD, FT-IR spectroscopy, SEM, and thermogravimetric analysis. Optimum biosorption conditions were determined with respect to pH, adsorbent dose, contact time, and temperature. The experimental data were examined using the Lagergren’s first-order, pseudo-second-order and intraparticle diffusion kinetic models. The results revealed that the pseudo-second-order kinetic model provided the best description of the data. Langmuir and Freundlich isotherm models were applied to the equilibrium data. The maximum As(III) sorption capacity of ZnO nanorods was found to be 52.63 mg/g at pH 7, adsorbent dose 0.4 g, contact time 105 min, and temperature 323 K. The calculated thermodynamic parameters, ΔGo (between − 5.741, − 5.342 and − 4.538 kJ/mol at 303–323 K), ∆Ho (13.75 kJ/mol) and ∆So (0.0616 J/mol K) showed that the sorption of As(III) onto ZnO nanorods was feasible, spontaneous and exothermic, respectively.
Removal of metals from wastewaters causes a big concern from the environmental point of view due to their extreme toxicity towards aquatic life and humans. Application of As(III) from aqueous solution by ZnO nanorods as adsorbent has been investigated in the present study. The synthesized nanorods were characterized by XRD, FT-IR spectroscopy, SEM, and thermogravimetric analysis. Optimum biosorption conditions were determined with respect to pH, adsorbent dose, contact time, and temperature. The experimental data were examined using the Lagergren’s first-order, pseudo-second-order and intraparticle diffusion kinetic models. The results revealed that the pseudo-second-order kinetic model provided the best description of the data. Langmuir and Freundlich isotherm models were applied to the equilibrium data. The maximum As(III) sorption capacity of ZnO nanorods was found to be 52.63 mg/g at pH 7, adsorbent dose 0.4 g, contact time 105 min, and temperature 323 K. The calculated thermodynamic parameters, Δ G o (between − 5.741, − 5.342 and − 4.538 kJ/mol at 303–323 K), ∆ H o (13.75 kJ/mol) and ∆ S o (0.0616 J/mol K) showed that the sorption of As(III) onto ZnO nanorods was feasible, spontaneous and exothermic, respectively.
Author Subbaiah, Munagapati Venkata
Prasad, Cheera
Vijaya, Yarramuthi
Yuvaraja, Gutha
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  givenname: Cheera
  surname: Prasad
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  surname: Vijaya
  fullname: Vijaya, Yarramuthi
  organization: Department of Chemistry, Vikrama Simhapuri University
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  givenname: Munagapati Venkata
  surname: Subbaiah
  fullname: Subbaiah, Munagapati Venkata
  organization: Department of Environmental Science and Engineering, Ewha Womans University
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Keywords ZnO nanorods
Thermodynamics
Kinetics
Isotherms
As(III)
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Snippet Removal of metals from wastewaters causes a big concern from the environmental point of view due to their extreme toxicity towards aquatic life and humans....
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SubjectTerms Adsorbents
Aqueous solutions
Arsenic
Chemistry
Chemistry and Materials Science
Environmental Chemistry
Fourier transforms
Industrial Chemistry/Chemical Engineering
Infrared spectroscopy
Isotherms
Kinetics
Nanochemistry
Nanorods
Polymer Sciences
Sorption
Thermogravimetric analysis
Toxicity
Zinc oxide
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Title Application of ZnO nanorods as an adsorbent material for the removal of As(III) from aqueous solution: kinetics, isotherms and thermodynamic studies
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