A copper(I) phosphine complex with 5,7-dinitro-2-methylquinolin-8-ol as co-ligand
5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO 2 ligand and its complex were characterized by IR, NMR, and UV–Vis spectra. The structure of the [Cu(2-MequinNO 2 )(PPh 3 ) 2 ] complex has been determined by single-crystal...
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| Published in | Transition metal chemistry (Weinheim) Vol. 39; no. 7; pp. 755 - 762 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cham
Springer International Publishing
01.10.2014
Springer Nature B.V |
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| Abstract | 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO
2
ligand and its complex were characterized by IR, NMR, and UV–Vis spectra. The structure of the [Cu(2-MequinNO
2
)(PPh
3
)
2
] complex has been determined by single-crystal X-ray analysis. The free 2-MequinNO
2
ligand reveals luminescence in contrast to the complex. For 2-MequinNO
2
, the quantum yield, lifetime of the excited state, and the rate constants of both radiative and non-radiative decay have been determined. The lack of luminescence for the complex has been explained with the use of a quantum chemical study. |
|---|---|
| AbstractList | 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO sub(2) ligand and its complex were characterized by IR, NMR, and UV-Vis spectra. The structure of the [Cu(2-MequinNO sub(2))(PPh sub(3) ) sub(2)] complex has been determined by single-crystal X-ray analysis. The free 2-MequinNO sub(2) ligand reveals luminescence in contrast to the complex. For 2-MequinNO sub(2), the quantum yield, lifetime of the excited state, and the rate constants of both radiative and non-radiative decay have been determined. The lack of luminescence for the complex has been explained with the use of a quantum chemical study. 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO 2 ligand and its complex were characterized by IR, NMR, and UV–Vis spectra. The structure of the [Cu(2-MequinNO 2 )(PPh 3 ) 2 ] complex has been determined by single-crystal X-ray analysis. The free 2-MequinNO 2 ligand reveals luminescence in contrast to the complex. For 2-MequinNO 2 , the quantum yield, lifetime of the excited state, and the rate constants of both radiative and non-radiative decay have been determined. The lack of luminescence for the complex has been explained with the use of a quantum chemical study. 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO2 ligand and its complex were characterized by IR, NMR, and UV-Vis spectra. The structure of the [Cu(2-MequinNO2)(PPh^sub 3^)^sub 2^] complex has been determined by single-crystal X-ray analysis. The free 2-MequinNO2 ligand reveals luminescence in contrast to the complex. For 2-MequinNO2, the quantum yield, lifetime of the excited state, and the rate constants of both radiative and non-radiative decay have been determined. The lack of luminescence for the complex has been explained with the use of a quantum chemical study.[PUBLICATION ABSTRACT] |
| Author | Palion, Joanna Małecki, Jan G. Maroń, Anna Szala, Marcin Nycz, Jacek E. |
| Author_xml | – sequence: 1 givenname: Jan G. surname: Małecki fullname: Małecki, Jan G. email: gmalecki@us.edu.pl organization: Department of Crystallography, Institute of Chemistry, University of Silesia – sequence: 2 givenname: Anna surname: Maroń fullname: Maroń, Anna organization: Department of Crystallography, Institute of Chemistry, University of Silesia – sequence: 3 givenname: Joanna surname: Palion fullname: Palion, Joanna organization: Department of Crystallography, Institute of Chemistry, University of Silesia – sequence: 4 givenname: Jacek E. surname: Nycz fullname: Nycz, Jacek E. organization: Department of Organic, Organometallic Chemistry and Catalysis, Institute of Chemistry, University of Silesia – sequence: 5 givenname: Marcin surname: Szala fullname: Szala, Marcin organization: Department of Organic, Organometallic Chemistry and Catalysis, Institute of Chemistry, University of Silesia |
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| Keywords | Differential Pulse Voltammetry High Occupied Molecular Orbital Quinoline Ring PPh3 Quantum Chemical Study |
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| Snippet | 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO
2
ligand and its complex were... 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO2 ligand and its complex were... 5,7-Dinitro-2-methylquinolin-8-ol has been synthesized, and its copper(I) complex has been prepared. Both the free 2-MequinNO sub(2) ligand and its complex... |
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| SubjectTerms | Catalysis Chemistry Chemistry and Materials Science Decay rate Inorganic Chemistry Ligands Luminescence Organometallic Chemistry Phosphines Physical Chemistry Quantum chemistry Rate constants Spectra X-rays |
| Title | A copper(I) phosphine complex with 5,7-dinitro-2-methylquinolin-8-ol as co-ligand |
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