Study of thermal ageing effects on Rh coating's mechanical performance upon CuCrZr substrate through modeling and experimental methods
Rhodium (Rh) coating on CuCrZr substrate is a promising material option for optical, structural and electrical applications on nuclear fusion reactors. For these applications, Rh coated CuCrZr components subject to long time of thermal ageing due to pre-treatment or normal operation condition. In th...
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| Published in | Vacuum Vol. 154; pp. 227 - 234 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.08.2018
Elsevier |
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| Online Access | Get full text |
| ISSN | 0042-207X |
| DOI | 10.1016/j.vacuum.2018.05.018 |
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| Abstract | Rhodium (Rh) coating on CuCrZr substrate is a promising material option for optical, structural and electrical applications on nuclear fusion reactors. For these applications, Rh coated CuCrZr components subject to long time of thermal ageing due to pre-treatment or normal operation condition. In this paper, both finite element method (FEM) and experimental method were applied to investigate the effects of thermal ageing on mechanical performance of Rh coating after 250 °C, 500 h baking in vacuum. Based on FEM analysis, thermal stresses which concentrate at Rh coating interface is the main source of cracking, and such stresses can be minimized efficiently by introducing a 0.5 μm Au interlayer into the coating layer structure. According to thermal ageing experiments, through-thickness cracking in the Rh coating due to thermal stress releasing and voids generated at the Rh bonding interface caused by Kirkendall effect were the main micro-structure changes in the coating system. The solid-solution hardening caused by significant Cu diffusion into Rh is the dominant factor that affected the Rh coating's hardness. The existing of large amount of cracks in the Rh coating and voids at the Rh coating interface deteriorated the adhesion performance of Rh on CuCrZr substrate by 30%.
•Applying of Au interlayer to decrease Rh coating's thermal stress was modeled.•Electroplated Rh showed good thermal stability in hardness and crystallite size.•Diffusion phenomenon at Rh/Cu interface impaired the Rh adhesion significantly. |
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| AbstractList | Rhodium (Rh) coating on CuCrZr substrate is a promising material option for optical, structural and electrical applications on nuclear fusion reactors. For these applications, Rh coated CuCrZr components subject to long time of thermal ageing due to pre-treatment or normal operation condition. In this paper, both finite element method (FEM) and experimental method were applied to investigate the effects of thermal ageing on mechanical performance of Rh coating after 250 °C, 500 h baking in vacuum. Based on FEM analysis, thermal stresses which concentrate at Rh coating interface is the main source of cracking, and such stresses can be minimized efficiently by introducing a 0.5 μm Au interlayer into the coating layer structure. According to thermal ageing experiments, through-thickness cracking in the Rh coating due to thermal stress releasing and voids generated at the Rh bonding interface caused by Kirkendall effect were the main micro-structure changes in the coating system. The solid-solution hardening caused by significant Cu diffusion into Rh is the dominant factor that affected the Rh coating's hardness. The existing of large amount of cracks in the Rh coating and voids at the Rh coating interface deteriorated the adhesion performance of Rh on CuCrZr substrate by 30%.
•Applying of Au interlayer to decrease Rh coating's thermal stress was modeled.•Electroplated Rh showed good thermal stability in hardness and crystallite size.•Diffusion phenomenon at Rh/Cu interface impaired the Rh adhesion significantly. Rhodium (Rh) coating on CuCrZr substrate is a promising material option for optical, structural and electrical applications on nuclear fusion reactors. For these applications, Rh coated CuCrZr components subject to long time of thermal ageing due to pre-treatment or normal operation condition. In this paper, both finite element method (FEM) and experimental method were applied to investigate the effects of thermal ageing on mechanical performance of Rh coating after 250 °C, 500 h baking in vacuum. Based on FEM analysis, thermal stresses which concentrate at Rh coating interface is the main source of cracking, and such stresses can be minimized efficiently by introducing a 0.5 μm Au interlayer into the coating layer structure. According to thermal ageing experiments, through-thickness cracking in the Rh coating due to thermal stress releasing and voids generated at the Rh bonding interface caused by Kirkendall effect were the main micro-structure changes in the coating system. The solid-solution hardening caused by significant Cu diffusion into Rh is the dominant factor that affected the Rh coating's hardness. The existing of large amount of cracks in the Rh coating and voids at the Rh coating interface deteriorated the adhesion performance of Rh on CuCrZr substrate by 30%. |
| Author | Vulliez, K. Chen, Z.X. Song, Y.T. Laloo, R. Hernandez, C. Bernard, J.M. Ferreira, L. Turq, V. Fesquet, F. Hillairet, J. Yang, Q.X. |
| Author_xml | – sequence: 1 givenname: Z.X. surname: Chen fullname: Chen, Z.X. email: zhaoxi.chen@cea.fr organization: CEA, IRFM, F-13108, Saint-Paul-Lez-Durance, France – sequence: 2 givenname: J. surname: Hillairet fullname: Hillairet, J. organization: CEA, IRFM, F-13108, Saint-Paul-Lez-Durance, France – sequence: 3 givenname: V. surname: Turq fullname: Turq, V. organization: Institut Carnot CIRIMAT, UMR CNRS-UPS-INP 5085, Université Paul-Sabatier, 118 Route de Narbonne, 31062, Toulouse Cedex 9, France – sequence: 4 givenname: Y.T. surname: Song fullname: Song, Y.T. organization: Institute of Plasma Physics, CAS, Hefei, Anhui, 230031, China – sequence: 5 givenname: R. surname: Laloo fullname: Laloo, R. organization: Institut Carnot CIRIMAT, UMR CNRS-UPS-INP 5085, Université Paul-Sabatier, 118 Route de Narbonne, 31062, Toulouse Cedex 9, France – sequence: 6 givenname: K. surname: Vulliez fullname: Vulliez, K. organization: Laboratoire d’étanchéité, DEN/DTEC/SDTC, CEA, 2 Rue James Watt, 26700, Pierrelatte, France – sequence: 7 givenname: J.M. surname: Bernard fullname: Bernard, J.M. organization: CEA, IRFM, F-13108, Saint-Paul-Lez-Durance, France – sequence: 8 givenname: Q.X. surname: Yang fullname: Yang, Q.X. organization: Institute of Plasma Physics, CAS, Hefei, Anhui, 230031, China – sequence: 9 givenname: C. surname: Hernandez fullname: Hernandez, C. organization: CEA, IRFM, F-13108, Saint-Paul-Lez-Durance, France – sequence: 10 givenname: L. surname: Ferreira fullname: Ferreira, L. organization: CERN, Geneva, Switzerland – sequence: 11 givenname: F. surname: Fesquet fullname: Fesquet, F. organization: CERN, Geneva, Switzerland |
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| Cites_doi | 10.1016/j.msea.2012.02.027 10.1016/S0040-6090(01)01043-4 10.1016/j.apsusc.2008.04.003 10.1016/j.msea.2005.07.010 10.1016/j.fusengdes.2010.12.038 10.1088/0029-5515/49/3/035007 10.1016/j.jnucmat.2007.01.281 10.1016/S0921-5093(02)00251-4 10.1016/j.fusengdes.2015.04.005 10.1016/j.msea.2015.09.082 10.1016/j.surfcoat.2007.10.014 10.1016/S1359-6462(02)00633-4 10.1063/1.2800779 10.1088/1742-6596/114/1/012013 10.1016/S0167-577X(02)00570-0 10.1007/BF00618901 10.1016/S0921-5093(99)00565-1 10.1063/1.4864566 10.1002/adma.200602398 10.1016/j.vacuum.2009.05.015 10.1016/j.fusengdes.2013.03.050 10.4236/wjnse.2012.23020 10.1016/j.jmatprotec.2007.03.115 10.1016/j.jmatprotec.2004.09.093 10.1016/S0040-6090(03)00427-9 10.1016/j.tsf.2008.04.087 |
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| Keywords | Rh coating Thermal stress Cracking CuCrZr Hardness Adhesion |
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| Snippet | Rhodium (Rh) coating on CuCrZr substrate is a promising material option for optical, structural and electrical applications on nuclear fusion reactors. For... |
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| SubjectTerms | Adhesion Cracking CuCrZr Electromagnetism Engineering Sciences Hardness Physics Plasma Physics Plasmas Rh coating Thermal stress |
| Title | Study of thermal ageing effects on Rh coating's mechanical performance upon CuCrZr substrate through modeling and experimental methods |
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