Polyoxometalate-based ionic liquids as catalysts for deep desulfurization of fuels
In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction and catalytic oxidation desulfurization (ECODS) system is one of the most promising desulfurization processes. A series of Keggin-type POM-base...
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| Published in | Fuel processing technology Vol. 92; no. 10; pp. 1842 - 1848 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.10.2011
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0378-3820 1873-7188 |
| DOI | 10.1016/j.fuproc.2011.04.030 |
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| Abstract | In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction and catalytic oxidation desulfurization (ECODS) system is one of the most promising desulfurization processes. A series of Keggin-type POM-based ionic liquids hybrid materials [MIMPS]
3PW
12O
40·2H
2O (1-(3-sulfonic group) propyl-3-methyl imidazolium phosphotungstate), [Bmim]
3PW
12O
40 (1-butyl 3-methyl imidazolium phosphotungstate), [Bmim]
3PMo
12O
40 (1-butyl 3-methyl imidazolium phosphomolybdate) and [Bmim]
4SiW
12O
40 (1-butyl-3-methyl imidazolium silicotungstate) have been developed in this study, and the reaction has performed using the POM-ILs materials as catalysts, H
2O
2 as oxidant, and ionic liquid (IL) as solvent. Through experimental evaluations, [MIMPS]
3PW
12O
40·2H
2O was found to be the best catalyst, with an S-removal of 100% at 30
°C for 1
h. The main factors affecting the process including temperature, catalyst dosage, and O/S (H
2O
2/DBT) molar ratio were investigated in detail. Under the optimal conditions, DBT (dibenzothiophene) and 4,6-DMDBT (4,6-dimethyl-dibenzothiophene) could achieve high desulfurization efficiency. Moreover, the reaction system also exhibited high activity in actual diesel oil, which could be reduced from 1113
ppm to 198
ppm. The reaction system could recycle 8-times with a slight decrease in activity.
[Display omitted]
► Several POM-based ILs were synthesized and characterized. ► New attempt with POM-based ILs as catalysts in removing DBT in fuels. ► High desulfurization was achieved in water-immiscible IL. ► Desulfurization differences among different POM-ILs catalysts have been explained. |
|---|---|
| AbstractList | In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction and catalytic oxidation desulfurization (ECODS) system is one of the most promising desulfurization processes. A series of Keggin-type POM-based ionic liquids hybrid materials [MIMPS]
3PW
12O
40·2H
2O (1-(3-sulfonic group) propyl-3-methyl imidazolium phosphotungstate), [Bmim]
3PW
12O
40 (1-butyl 3-methyl imidazolium phosphotungstate), [Bmim]
3PMo
12O
40 (1-butyl 3-methyl imidazolium phosphomolybdate) and [Bmim]
4SiW
12O
40 (1-butyl-3-methyl imidazolium silicotungstate) have been developed in this study, and the reaction has performed using the POM-ILs materials as catalysts, H
2O
2 as oxidant, and ionic liquid (IL) as solvent. Through experimental evaluations, [MIMPS]
3PW
12O
40·2H
2O was found to be the best catalyst, with an S-removal of 100% at 30
°C for 1
h. The main factors affecting the process including temperature, catalyst dosage, and O/S (H
2O
2/DBT) molar ratio were investigated in detail. Under the optimal conditions, DBT (dibenzothiophene) and 4,6-DMDBT (4,6-dimethyl-dibenzothiophene) could achieve high desulfurization efficiency. Moreover, the reaction system also exhibited high activity in actual diesel oil, which could be reduced from 1113
ppm to 198
ppm. The reaction system could recycle 8-times with a slight decrease in activity.
[Display omitted]
► Several POM-based ILs were synthesized and characterized. ► New attempt with POM-based ILs as catalysts in removing DBT in fuels. ► High desulfurization was achieved in water-immiscible IL. ► Desulfurization differences among different POM-ILs catalysts have been explained. In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction and catalytic oxidation desulfurization (ECODS) system is one of the most promising desulfurization processes. A series of Keggin-type POM-based ionic liquids hybrid materials [MIMPS]₃PW₁₂O₄₀·2H₂O (1-(3-sulfonic group) propyl-3-methyl imidazolium phosphotungstate), [Bmim]₃PW₁₂O₄₀ (1-butyl 3-methyl imidazolium phosphotungstate), [Bmim]₃PMo₁₂O₄₀ (1-butyl 3-methyl imidazolium phosphomolybdate) and [Bmim]₄SiW₁₂O₄₀ (1-butyl-3-methyl imidazolium silicotungstate) have been developed in this study, and the reaction has performed using the POM-ILs materials as catalysts, H₂O₂ as oxidant, and ionic liquid (IL) as solvent. Through experimental evaluations, [MIMPS]₃PW₁₂O₄₀·2H₂O was found to be the best catalyst, with an S-removal of 100% at 30°C for 1h. The main factors affecting the process including temperature, catalyst dosage, and O/S (H₂O₂/DBT) molar ratio were investigated in detail. Under the optimal conditions, DBT (dibenzothiophene) and 4,6-DMDBT (4,6-dimethyl-dibenzothiophene) could achieve high desulfurization efficiency. Moreover, the reaction system also exhibited high activity in actual diesel oil, which could be reduced from 1113ppm to 198ppm. The reaction system could recycle 8-times with a slight decrease in activity. In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction and catalytic oxidation desulfurization (ECODS) system is one of the most promising desulfurization processes. A series of Keggin-type POM-based ionic liquids hybrid materials [MIMPS] sub(3)PW sub(12)O sub(4)0 times 2H sub(2)O (1-(3-sulfonic group) propyl-3-methyl imidazolium phosphotungstate), [Bmim] sub(3)PW sub(12)O sub(4)0 (1-butyl 3-methyl imidazolium phosphotungstate), [Bmim] sub(3)PMo sub(12)O sub(40) (1-butyl 3-methyl imidazolium phosphomolybdate) and [Bmim] sub(4)SiW sub(12)O sub(40) (1-butyl-3-methyl imidazolium silicotungstate) have been developed in this study, and the reaction has performed using the POM-ILs materials as catalysts, H sub(2)O sub(2) as oxidant, and ionic liquid (IL) as solvent. Through experimental evaluations, [MIMPS] sub(3)PW sub(12)O sub(4)0 times 2H sub(2)O was found to be the best catalyst, with an S-removal of 100% at 30 degree C for 1 h. The main factors affecting the process including temperature, catalyst dosage, and O/S (H sub(2)O sub(2)/DBT) molar ratio were investigated in detail. Under the optimal conditions, DBT (dibenzothiophene) and 4,6-DMDBT (4,6-dimethyl-dibenzothiophene) could achieve high desulfurization efficiency. Moreover, the reaction system also exhibited high activity in actual diesel oil, which could be reduced from 1113 ppm to 198 ppm. The reaction system could recycle 8-times with a slight decrease in activity. |
| Author | Huang, Wangli Li, Huaming Jiang, Wei Zhu, Wenshuai Chen, Guangying Han, Changri Zhang, Ming |
| Author_xml | – sequence: 1 givenname: Wenshuai surname: Zhu fullname: Zhu, Wenshuai organization: School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, PR China – sequence: 2 givenname: Wangli surname: Huang fullname: Huang, Wangli organization: School of the Environment, Jiangsu University, Zhenjiang 212013, PR China – sequence: 3 givenname: Huaming surname: Li fullname: Li, Huaming email: lihm@ujs.edu.cn organization: School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, PR China – sequence: 4 givenname: Ming surname: Zhang fullname: Zhang, Ming organization: School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, PR China – sequence: 5 givenname: Wei surname: Jiang fullname: Jiang, Wei organization: School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, PR China – sequence: 6 givenname: Guangying surname: Chen fullname: Chen, Guangying organization: School of Chemistry and Chemical Engineering, Hainan Normal University, Haikou 571158, PR China – sequence: 7 givenname: Changri surname: Han fullname: Han, Changri organization: School of Chemistry and Chemical Engineering, Hainan Normal University, Haikou 571158, PR China |
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| Keywords | Characterization Oxidative desulfurization Polyoxometalate-based ionic liquids Catalysis Evaluation Diesel fuel Reaction time Oxidation Fuel desulfurization Catalyst Ionic liquid |
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| PublicationPlace_xml | – name: Amsterdam |
| PublicationTitle | Fuel processing technology |
| PublicationYear | 2011 |
| Publisher | Elsevier B.V Elsevier |
| Publisher_xml | – name: Elsevier B.V – name: Elsevier |
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| Snippet | In order to obtain the ultra low-sulfur diesel, deep desulfurization of diesel oil has become a vital subject of environmental catalysis studies. Extraction... |
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| SubjectTerms | Applied sciences Catalysis catalysts catalytic activity Characterization diesel fuel Energy Energy. Thermal use of fuels Exact sciences and technology Fuels hydrogen peroxide ionic liquids oxidants oxidation Oxidative desulfurization Polyoxometalate-based ionic liquids recycling temperature |
| Title | Polyoxometalate-based ionic liquids as catalysts for deep desulfurization of fuels |
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