Plasma-Assisted Synthesis of TiO2 Nanorods by Gliding Arc Discharge Processing at Atmospheric Pressure for Photocatalytic Applications
The present study explores a new method of synthesis of TiO 2 nano-particles in an aqueous medium from TiCl 3 precursor by non-thermal plasma in humid air as feeding gas obtained at atmospheric pressure. The precursor solution, TiCl 3 is oxidized by strongly reactive species generated by gliding arc...
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Published in | Plasma chemistry and plasma processing Vol. 33; no. 4; pp. 725 - 735 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
Published |
Boston
Springer US
01.08.2013
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Abstract | The present study explores a new method of synthesis of TiO
2
nano-particles in an aqueous medium from TiCl
3
precursor by non-thermal plasma in humid air as feeding gas obtained at atmospheric pressure. The precursor solution, TiCl
3
is oxidized by strongly reactive species generated by gliding arc plasma (HO
·
= 2.85 V/SHE) to produce titanium oxide powders. The synthesized powder was characterised by X-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, FTIR spectroscopy, nitrogen physisorption, and UV–Vis spectroscopy. The results obtained showed that the material consists of rod-shaped nanoparticles of rutile and anatase phases. The presence of TiO
2
phases was confirmed by FTIR spectrum and textural analyses showed that the material is mesoporous with specific surface area of 158 m
2
g
−1
. UV–Visible spectrum of the plasma-synthesized TiO
2
sample showed that it absorbs in the UV–A region leading to effective use as a photocatalyst under visible light. |
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AbstractList | The present study explores a new method of synthesis of TiO
2
nano-particles in an aqueous medium from TiCl
3
precursor by non-thermal plasma in humid air as feeding gas obtained at atmospheric pressure. The precursor solution, TiCl
3
is oxidized by strongly reactive species generated by gliding arc plasma (HO
·
= 2.85 V/SHE) to produce titanium oxide powders. The synthesized powder was characterised by X-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, FTIR spectroscopy, nitrogen physisorption, and UV–Vis spectroscopy. The results obtained showed that the material consists of rod-shaped nanoparticles of rutile and anatase phases. The presence of TiO
2
phases was confirmed by FTIR spectrum and textural analyses showed that the material is mesoporous with specific surface area of 158 m
2
g
−1
. UV–Visible spectrum of the plasma-synthesized TiO
2
sample showed that it absorbs in the UV–A region leading to effective use as a photocatalyst under visible light. The present study explores a new method of synthesis of TiO2 nano-particles in an aqueous medium from TiCl3 precursor by non-thermal plasma in humid air as feeding gas obtained at atmospheric pressure. The precursor solution, TiCl3 is oxidized by strongly reactive species generated by gliding arc plasma (HOADT = 2.85 V/SHE) to produce titanium oxide powders. The synthesized powder was characterised by X-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, FTIR spectroscopy, nitrogen physisorption, and UV-Vis spectroscopy. The results obtained showed that the material consists of rod-shaped nanoparticles of rutile and anatase phases. The presence of TiO2 phases was confirmed by FTIR spectrum and textural analyses showed that the material is mesoporous with specific surface area of 158 m2 g super(-1). UV-Visible spectrum of the plasma-synthesized TiO2 sample showed that it absorbs in the UVaA region leading to effective use as a photocatalyst under visible light. |
Author | Gaigneaux, E. M. Acayanka, E. Tiya Djowe, A. Tchoumkwé, C. C. Laminsi, S. Nzali, S. Poupi Mbouopda, A. Ndifon, P. T. |
Author_xml | – sequence: 1 givenname: E. surname: Acayanka fullname: Acayanka, E. organization: Inorganic Chemistry Department, University of Yaoundé I, Instituto de Química, Universidade Federal do Rio Grande do Sul – sequence: 2 givenname: A. surname: Tiya Djowe fullname: Tiya Djowe, A. organization: Inorganic Chemistry Department, University of Yaoundé I, Institute of Condensed Matter and Nanosciences (IMCN), Division “Molecules, Solids and reactiviTy” (MOST), Université catholique de Louvain – sequence: 3 givenname: S. surname: Laminsi fullname: Laminsi, S. email: s.laminsi@yahoo.fr organization: Inorganic Chemistry Department, University of Yaoundé I – sequence: 4 givenname: C. C. surname: Tchoumkwé fullname: Tchoumkwé, C. C. organization: Inorganic Chemistry Department, University of Yaoundé I – sequence: 5 givenname: S. surname: Nzali fullname: Nzali, S. organization: School of Wood, Water and Natural Resources, Faculty of Agronomy and Agricultural Sciences, University of Dschang (Ebolowa campus) – sequence: 6 givenname: A. surname: Poupi Mbouopda fullname: Poupi Mbouopda, A. organization: Inorganic Chemistry Department, University of Yaoundé I – sequence: 7 givenname: P. T. surname: Ndifon fullname: Ndifon, P. T. organization: Inorganic Chemistry Department, University of Yaoundé I – sequence: 8 givenname: E. M. surname: Gaigneaux fullname: Gaigneaux, E. M. organization: Institute of Condensed Matter and Nanosciences (IMCN), Division “Molecules, Solids and reactiviTy” (MOST), Université catholique de Louvain |
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Keywords | Gliding arc discharge Non-thermal plasma Titanium dioxide Photocatalyst Nanorods |
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Snippet | The present study explores a new method of synthesis of TiO
2
nano-particles in an aqueous medium from TiCl
3
precursor by non-thermal plasma in humid air as... The present study explores a new method of synthesis of TiO2 nano-particles in an aqueous medium from TiCl3 precursor by non-thermal plasma in humid air as... |
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SubjectTerms | Atmospheric pressure Barometric pressure Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Classical Mechanics Gliding Inorganic Chemistry Mechanical Engineering Nanorods Nanostructure Original Paper Spectroscopy Synthesis Titanium dioxide |
Title | Plasma-Assisted Synthesis of TiO2 Nanorods by Gliding Arc Discharge Processing at Atmospheric Pressure for Photocatalytic Applications |
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