Simple one-pot synthesis of a mesoporous superacidic catalyst for the dehydration of glycerol to acrolein
Mesoporous silica containing a ZrO 2 /SO 4 2− superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO 2 /SO 4 2− (SZ) was introduced during the synthesis of the SBA-15. When the molar ratio of Zr to Si was less than 0.37 : 1, a 2D-hexagonal pore structure was maintained. The super...
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| Published in | The Korean journal of chemical engineering Vol. 27; no. 6; pp. 1695 - 1699 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Boston
Springer US
01.11.2010
한국화학공학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0256-1115 1975-7220 |
| DOI | 10.1007/s11814-010-0256-x |
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| Abstract | Mesoporous silica containing a ZrO
2
/SO
4
2−
superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO
2
/SO
4
2−
(SZ) was introduced during the synthesis of the SBA-15. When the molar ratio of Zr to Si was less than 0.37 : 1, a 2D-hexagonal pore structure was maintained. The superacidic SZ was successfully supported on mesoporous silica resulting in superacidity. The prepared SZS catalysts were applied to the conversion of glycerol to acrolein by dehydration and had considerable catalytic activity. The present study describes the first attempt to utilize mesoporous silica-supported superacid catalysts in the dehydration of glycerol to produce acrolein. |
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| AbstractList | Mesoporous silica containing a ZrO2/SO42− superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO2/SO42− (SZ) was introduced during the synthesis of the SBA-15. When the molar ratio of Zr to Si was less than 0.37 : 1, a 2D-hexagonal pore structure was maintained. The superacidic SZ was successfully supported on mesoporous silica resulting in superacidity. The prepared SZS catalysts were applied to the conversion of glycerol to acrolein by dehydration and had considerable catalytic activity. The present study describes the first attempt to utilize mesoporous silica-supported superacid catalysts in the dehydration of glycerol to produce acrolein. KCI Citation Count: 13 Mesoporous silica containing a ZrO 2 /SO 4 2− superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO 2 /SO 4 2− (SZ) was introduced during the synthesis of the SBA-15. When the molar ratio of Zr to Si was less than 0.37 : 1, a 2D-hexagonal pore structure was maintained. The superacidic SZ was successfully supported on mesoporous silica resulting in superacidity. The prepared SZS catalysts were applied to the conversion of glycerol to acrolein by dehydration and had considerable catalytic activity. The present study describes the first attempt to utilize mesoporous silica-supported superacid catalysts in the dehydration of glycerol to produce acrolein. |
| Author | Yang, Lina Jung, Kwang Seop Joo, Ji Bong Yi, Jongheop Kim, Nam Dong |
| Author_xml | – sequence: 1 givenname: Lina surname: Yang fullname: Yang, Lina organization: Department of Petrochemical Engineering, Liaoning Shihua University – sequence: 2 givenname: Ji Bong surname: Joo fullname: Joo, Ji Bong organization: School of Chemical and Biological Engineering, Institute of Chemical Processes, Seoul National University – sequence: 3 givenname: Nam Dong surname: Kim fullname: Kim, Nam Dong organization: School of Chemical and Biological Engineering, Institute of Chemical Processes, Seoul National University – sequence: 4 givenname: Kwang Seop surname: Jung fullname: Jung, Kwang Seop organization: GS Caltex Corporation – sequence: 5 givenname: Jongheop surname: Yi fullname: Yi, Jongheop email: jyi@snu.ac.kr organization: School of Chemical and Biological Engineering, Institute of Chemical Processes, Seoul National University |
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| CitedBy_id | crossref_primary_10_1007_s11814_012_0039_7 crossref_primary_10_1016_j_apcatb_2015_02_032 crossref_primary_10_1016_j_apcatb_2017_09_016 crossref_primary_10_1016_j_cej_2015_03_018 crossref_primary_10_1002_cssc_201300416 crossref_primary_10_1016_j_apcata_2016_02_016 crossref_primary_10_1016_j_cattod_2014_12_024 crossref_primary_10_1007_s11814_024_00176_4 crossref_primary_10_1016_j_rser_2014_07_168 crossref_primary_10_1080_01614940_2013_816610 crossref_primary_10_1021_cs400354p crossref_primary_10_1016_S1872_2067_16_62564_0 crossref_primary_10_1002_cssc_201402925 |
| Cites_doi | 10.1016/j.micromeso.2006.12.018 10.1021/j100411a018 10.1016/0926-860X(94)80286-6 10.1039/c39950000203 10.1016/S1387-1811(99)00147-X 10.1007/s11814-007-5006-3 10.1016/S0254-0584(97)80177-0 10.1039/B506285C 10.1016/S0926-860X(02)00133-3 10.1016/j.jcat.2004.02.021 10.1039/b006051h 10.1021/jp984378j 10.1016/S0926-860X(00)00698-0 10.1016/S0360-0564(08)60365-X 10.1016/j.micromeso.2005.01.007 10.1016/j.catcom.2006.12.006 10.1016/j.jcat.2007.06.016 10.1039/a904783b 10.1039/C39800000851 10.1006/jcat.1993.1304 10.1021/ja00515a051 10.1016/S1005-9040(06)60119-0 10.1016/S1381-1169(01)00063-2 10.1016/S0022-4596(03)00218-4 10.1016/j.jssc.2008.04.009 10.1016/S0926-860X(01)00504-X 10.1016/j.apcata.2003.07.010 10.1016/j.cattod.2009.03.006 10.1016/S0926-860X(99)00404-4 |
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| Keywords | Superacid Acrolein Mesoporous Silica SO ZrO One-pot Synthesis |
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| Snippet | Mesoporous silica containing a ZrO
2
/SO
4
2−
superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO
2
/SO
4
2−
(SZ) was introduced during... Mesoporous silica containing a ZrO2/SO42− superacid catalyst (SZS) was synthesized via a simple one-pot process. ZrO2/SO42− (SZ) was introduced during the... |
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| SubjectTerms | Biotechnology Catalysis Chemistry Chemistry and Materials Science Industrial Chemistry/Chemical Engineering Materials Science 화학공학 |
| Title | Simple one-pot synthesis of a mesoporous superacidic catalyst for the dehydration of glycerol to acrolein |
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