Pd Loaded TiO2 Nanotubes for the Effective Catalytic Reduction of p-Nitrophenol

Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectr...

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Published inCatalysis letters Vol. 146; no. 2; pp. 474 - 482
Main Authors Kalarivalappil, Vijila, Divya, C. M., Wunderlich, W., Pillai, Suresh C., Hinder, Steven J., Nageri, Manoj, Kumar, V., Vijayan, Baiju K.
Format Journal Article
LanguageEnglish
Published New York Springer US 01.02.2016
Springer Nature B.V
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Abstract Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO 2 ) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of p -nitrophenol to p -aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min −1 ) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity. Graphical Abstract
AbstractList Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO 2 ) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of p -nitrophenol to p -aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min −1 ) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity. Graphical Abstract
Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO2) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of p-nitrophenol to p-aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min−1) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity.Graphical Abstract
Author Wunderlich, W.
Pillai, Suresh C.
Vijayan, Baiju K.
Kalarivalappil, Vijila
Hinder, Steven J.
Divya, C. M.
Kumar, V.
Nageri, Manoj
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  surname: Wunderlich
  fullname: Wunderlich, W.
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  surname: Pillai
  fullname: Pillai, Suresh C.
  organization: Nanotechnology Research Group, Department of Environmental Sciences, Institute of Technology Sligo, Centre for Precision Engineering, Materials and Manufacturing Research, Institute of Technology Sligo
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  givenname: Steven J.
  surname: Hinder
  fullname: Hinder, Steven J.
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  surname: Kumar
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  organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India
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  givenname: Baiju K.
  surname: Vijayan
  fullname: Vijayan, Baiju K.
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  organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India
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Issue 2
Keywords Palladium
Anatase
Rutile
Morphology
Catalysis and reduction
Titania nanotubes
Language English
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PublicationTitle Catalysis letters
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Snippet Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate...
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springer
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Publisher
StartPage 474
SubjectTerms Aminophenol
Anatase
Catalysis
Catalytic activity
Chemical reduction
Chemistry
Chemistry and Materials Science
Collapse
Industrial Chemistry/Chemical Engineering
Morphology
Nanoparticles
Nanotubes
Nitrophenol
Organometallic Chemistry
Palladium
Phase transitions
Physical Chemistry
Raman spectroscopy
Scanning electron microscopy
Titanium dioxide
Transmission electron microscopy
X ray photoelectron spectroscopy
X-ray diffraction
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Title Pd Loaded TiO2 Nanotubes for the Effective Catalytic Reduction of p-Nitrophenol
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