Pd Loaded TiO2 Nanotubes for the Effective Catalytic Reduction of p-Nitrophenol
Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectr...
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| Published in | Catalysis letters Vol. 146; no. 2; pp. 474 - 482 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.02.2016
Springer Nature B.V |
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| Abstract | Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO
2
) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of
p
-nitrophenol to
p
-aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min
−1
) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity.
Graphical Abstract |
|---|---|
| AbstractList | Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO
2
) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of
p
-nitrophenol to
p
-aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min
−1
) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity.
Graphical Abstract Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate the anatase to rutile crystalline phase transformation as well as in collapse of the morphology as revealed by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. The presence of metallic as well as the oxidized form (PdO2) of surface metal ions was characterized by using XPS. The catalytic activity of the Pd loaded titania nanotubes has been demonstrated by studying the reduction of p-nitrophenol to p-aminophenol. The 1.0 mol% Pd loaded titania nanotubes has been found to exhibit optimum catalytic activity (rate constant of 0.7072 min−1) while those with higher amounts of Pd loading showed lower catalytic activity. It is observed that retention of tubular morphology and higher anatase content play significant roles in their catalytic activity.Graphical Abstract |
| Author | Wunderlich, W. Pillai, Suresh C. Vijayan, Baiju K. Kalarivalappil, Vijila Hinder, Steven J. Divya, C. M. Kumar, V. Nageri, Manoj |
| Author_xml | – sequence: 1 givenname: Vijila surname: Kalarivalappil fullname: Kalarivalappil, Vijila organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India – sequence: 2 givenname: C. M. surname: Divya fullname: Divya, C. M. organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India – sequence: 3 givenname: W. surname: Wunderlich fullname: Wunderlich, W. organization: Material Science Department, Faculty of Engineering, Tokai University – sequence: 4 givenname: Suresh C. surname: Pillai fullname: Pillai, Suresh C. organization: Nanotechnology Research Group, Department of Environmental Sciences, Institute of Technology Sligo, Centre for Precision Engineering, Materials and Manufacturing Research, Institute of Technology Sligo – sequence: 5 givenname: Steven J. surname: Hinder fullname: Hinder, Steven J. organization: The Surface Analysis Laboratory, Department of Mechanical Engineering Sciences, University of Surrey – sequence: 6 givenname: Manoj surname: Nageri fullname: Nageri, Manoj organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India – sequence: 7 givenname: V. surname: Kumar fullname: Kumar, V. organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India – sequence: 8 givenname: Baiju K. surname: Vijayan fullname: Vijayan, Baiju K. email: baijuvijayan@gmail.com, baiju@cmet.gov.in organization: Department of Electronics and Information Technology, Centre for Materials for Electronics Technology (C-MET), Government of India |
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| Keywords | Palladium Anatase Rutile Morphology Catalysis and reduction Titania nanotubes |
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| Snippet | Titania nanotubes decorated with Pd nanoparticles were synthesised by a hydrothermal method. The increased amounts of Pd concentration is found to facilitate... |
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| SubjectTerms | Aminophenol Anatase Catalysis Catalytic activity Chemical reduction Chemistry Chemistry and Materials Science Collapse Industrial Chemistry/Chemical Engineering Morphology Nanoparticles Nanotubes Nitrophenol Organometallic Chemistry Palladium Phase transitions Physical Chemistry Raman spectroscopy Scanning electron microscopy Titanium dioxide Transmission electron microscopy X ray photoelectron spectroscopy X-ray diffraction |
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| Title | Pd Loaded TiO2 Nanotubes for the Effective Catalytic Reduction of p-Nitrophenol |
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