Triflic Acid-Functionalized Silica-Coated Magnetic Nanoparticles as a Magnetically Separable Catalyst for Synthesis of gem-Dihydroperoxides
Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe2O3@SiO2‐TfOH] were readily prepared and identified as an effictive catalyst for the transformation of aldehydes or ketones into their corresponding gem‐dihydroperoxides with 30% aqueous hydrogen peroxide. The catalyst was easily...
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| Published in | Advanced synthesis & catalysis Vol. 354; no. 2-3; pp. 441 - 447 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.02.2012
WILEY‐VCH Verlag Wiley Wiley-VCH |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1615-4150 1615-4169 |
| DOI | 10.1002/adsc.201100561 |
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| Abstract | Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe2O3@SiO2‐TfOH] were readily prepared and identified as an effictive catalyst for the transformation of aldehydes or ketones into their corresponding gem‐dihydroperoxides with 30% aqueous hydrogen peroxide. The catalyst was easily separated by magnetic decantation and the recovered catalyst was reused for seven cycles without significant loss of catalytic activity. |
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| AbstractList | Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe
2
O
3
@SiO
2
‐TfOH] were readily prepared and identified as an effictive catalyst for the transformation of aldehydes or ketones into their corresponding
gem
‐dihydroperoxides with 30% aqueous hydrogen peroxide. The catalyst was easily separated by magnetic decantation and the recovered catalyst was reused for seven cycles without significant loss of catalytic activity. Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe2O3@SiO2‐TfOH] were readily prepared and identified as an effictive catalyst for the transformation of aldehydes or ketones into their corresponding gem‐dihydroperoxides with 30% aqueous hydrogen peroxide. The catalyst was easily separated by magnetic decantation and the recovered catalyst was reused for seven cycles without significant loss of catalytic activity. Triflic acid-functionalized silica-coated magnetic nanoparticles [?-Fe2O3@SiO2-TfOH] were readily prepared and identified as an effictive catalyst for the transformation of aldehydes or ketones into their corresponding gem-dihydroperoxides with 30% aqueous hydrogen peroxide. The catalyst was easily separated by magnetic decantation and the recovered catalyst was reused for seven cycles without significant loss of catalytic activity. |
| Author | Liu, Yong-Hui Deng, Jia Gao, Jian-Wu Zhang, Zhan-Hui |
| Author_xml | – sequence: 1 givenname: Yong-Hui surname: Liu fullname: Liu, Yong-Hui organization: Key Laboratory of Inorganic Nanomaterial of Hebei Province, College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024, People's Republic of China, Fax: (+86)-311-8963-2795 – sequence: 2 givenname: Jia surname: Deng fullname: Deng, Jia organization: Key Laboratory of Inorganic Nanomaterial of Hebei Province, College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024, People's Republic of China, Fax: (+86)-311-8963-2795 – sequence: 3 givenname: Jian-Wu surname: Gao fullname: Gao, Jian-Wu organization: Key Laboratory of Inorganic Nanomaterial of Hebei Province, College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024, People's Republic of China, Fax: (+86)-311-8963-2795 – sequence: 4 givenname: Zhan-Hui surname: Zhang fullname: Zhang, Zhan-Hui email: zhanhui@mail.nankai.edu.cn organization: Key Laboratory of Inorganic Nanomaterial of Hebei Province, College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024, People's Republic of China, Fax: (+86)-311-8963-2795 |
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| Keywords | magnetic catalysts FE3O4 NANOPARTICLES AQUEOUS HYDROGEN-PEROXIDE GEMINAL BISHYDROPEROXIDES EFFICIENT SYNTHESIS CARBONYL-COMPOUNDS gem-dihydroperoxides HETEROGENEOUS CATALYSIS ketones LIGHT IRRADIATION aldehydes functionalized silica-coated magnetic nanoparticles ANTIMALARIAL ACTIVITY RECYCLABLE CATALYST MOLECULAR-OXYGEN Hydrogen peroxide Nanoparticle Reuse Trifluoromethanesulfonic acid Aldehyde Ketone Silica Magnetic particles Functionalization Magnetic separation Aqueous solution Iron III Oxides Chemical synthesis Catalyst activity Catalyst Maghemite Organic peroxide |
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| Snippet | Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe2O3@SiO2‐TfOH] were readily prepared and identified as an effictive catalyst for the... Triflic acid‐functionalized silica‐coated magnetic nanoparticles [γ‐Fe 2 O 3 @SiO 2 ‐TfOH] were readily prepared and identified as an effictive catalyst for... Triflic acid-functionalized silica-coated magnetic nanoparticles [?-Fe2O3@SiO2-TfOH] were readily prepared and identified as an effictive catalyst for the... |
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| SubjectTerms | aldehydes Aliphatic compounds Catalysis Catalysts: preparations and properties Chemistry Chemistry, Applied Chemistry, Organic Exact sciences and technology functionalized silica-coated magnetic nanoparticles gem-dihydroperoxides General and physical chemistry ketones magnetic catalysts Organic chemistry Physical Sciences Preparations and properties Science & Technology Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry |
| Title | Triflic Acid-Functionalized Silica-Coated Magnetic Nanoparticles as a Magnetically Separable Catalyst for Synthesis of gem-Dihydroperoxides |
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