An Itaconic Acid‐Based Phosphorus‐Containing Oligomer Endowing Epoxy Resins with Good Flame Retardancy and Toughness

With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP system...

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Published inMacromolecular materials and engineering Vol. 308; no. 4
Main Authors Zhao, Huijuan, Duan, Huajun, Zhang, Junjun, Chen, Lu, Wan, Chao, Zhang, Chenhao, Liu, Chentao, Ma, Huiru
Format Journal Article
LanguageEnglish
Published Weinheim John Wiley & Sons, Inc 01.04.2023
Wiley-VCH
Subjects
Acids
anhydride
Bisphenol A
Calorimetry
Chromatography
Curing
Data analysis
epoxy resin
Epoxy resins
flame retardancy
Flame retardants
Flammability
Fourier transforms
Glass transition temperature
Itaconic acid
Mechanical properties
Methyltetrahydrophthalic anhydride
Molecular structure
Nitrogen
NMR
Nuclear magnetic resonance
Oligomers
Phosphorus
Reagents
Sample size
Solvents
Tensile strength
toughening
Vapor phases
United States > US
Online AccessGet full text
ISSN1438-7492
1439-2054
DOI10.1002/mame.202200550

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Abstract With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP systems. Compared with EP/MeTHPA, the glass transition temperature (Tg) declines after introducing BID. But the addition of BID endows EP/MeTHPA with good flame retardancy. When the dosage is only 19.2 wt.%, the limiting oxygen index (LOI) of EP/BID/MeTHPA increases by 77% to 36% (P content: 1.5 wt.%) compared with EP and reaches the vertical combustion (UL‐94) V‐0 rating. Cone calorimetry (CC) results reveal that PHRR and THR drop by 40% and 31%. The pyrolytic process and char residue data analysis show that BID plays flame‐retardant role in gas phase and condensed phase. In addition, impact and flexural and tensile strength improve by 84%, 19% and 54% individually, proving that BID holds a potential on enhancing mechanical performance of EP/MeTHPA. Phosphorus oligomer BID is applied in the EP system of methyl tetrahydrophthalic anhydride (MeTHPA) cured epoxy resin. The addition of BID not only improves the flame retardancy of EP, but also improves the mechanical properties.
AbstractList With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP systems. Compared with EP/MeTHPA, the glass transition temperature (Tg) declines after introducing BID. But the addition of BID endows EP/MeTHPA with good flame retardancy. When the dosage is only 19.2 wt.%, the limiting oxygen index (LOI) of EP/BID/MeTHPA increases by 77% to 36% (P content: 1.5 wt.%) compared with EP and reaches the vertical combustion (UL‐94) V‐0 rating. Cone calorimetry (CC) results reveal that PHRR and THR drop by 40% and 31%. The pyrolytic process and char residue data analysis show that BID plays flame‐retardant role in gas phase and condensed phase. In addition, impact and flexural and tensile strength improve by 84%, 19% and 54% individually, proving that BID holds a potential on enhancing mechanical performance of EP/MeTHPA.
With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP systems. Compared with EP/MeTHPA, the glass transition temperature ( T g ) declines after introducing BID. But the addition of BID endows EP/MeTHPA with good flame retardancy. When the dosage is only 19.2 wt.%, the limiting oxygen index (LOI) of EP/BID/MeTHPA increases by 77% to 36% (P content: 1.5 wt.%) compared with EP and reaches the vertical combustion (UL‐94) V‐0 rating. Cone calorimetry (CC) results reveal that PHRR and THR drop by 40% and 31%. The pyrolytic process and char residue data analysis show that BID plays flame‐retardant role in gas phase and condensed phase. In addition, impact and flexural and tensile strength improve by 84%, 19% and 54% individually, proving that BID holds a potential on enhancing mechanical performance of EP/MeTHPA.
With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP systems. Compared with EP/MeTHPA, the glass transition temperature (Tg) declines after introducing BID. But the addition of BID endows EP/MeTHPA with good flame retardancy. When the dosage is only 19.2 wt.%, the limiting oxygen index (LOI) of EP/BID/MeTHPA increases by 77% to 36% (P content: 1.5 wt.%) compared with EP and reaches the vertical combustion (UL‐94) V‐0 rating. Cone calorimetry (CC) results reveal that PHRR and THR drop by 40% and 31%. The pyrolytic process and char residue data analysis show that BID plays flame‐retardant role in gas phase and condensed phase. In addition, impact and flexural and tensile strength improve by 84%, 19% and 54% individually, proving that BID holds a potential on enhancing mechanical performance of EP/MeTHPA. Phosphorus oligomer BID is applied in the EP system of methyl tetrahydrophthalic anhydride (MeTHPA) cured epoxy resin. The addition of BID not only improves the flame retardancy of EP, but also improves the mechanical properties.
Abstract With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing phosphophenanthrene group and flexible chain segment is designed and applied to methyltetrahydrophthalic anhydride (MeTHPA) curing EP systems. Compared with EP/MeTHPA, the glass transition temperature (Tg) declines after introducing BID. But the addition of BID endows EP/MeTHPA with good flame retardancy. When the dosage is only 19.2 wt.%, the limiting oxygen index (LOI) of EP/BID/MeTHPA increases by 77% to 36% (P content: 1.5 wt.%) compared with EP and reaches the vertical combustion (UL‐94) V‐0 rating. Cone calorimetry (CC) results reveal that PHRR and THR drop by 40% and 31%. The pyrolytic process and char residue data analysis show that BID plays flame‐retardant role in gas phase and condensed phase. In addition, impact and flexural and tensile strength improve by 84%, 19% and 54% individually, proving that BID holds a potential on enhancing mechanical performance of EP/MeTHPA.
Author Zhang, Junjun
Zhao, Huijuan
Zhang, Chenhao
Wan, Chao
Ma, Huiru
Duan, Huajun
Liu, Chentao
Chen, Lu
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Snippet With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID) containing...
Abstract With the aim to reduce the influence of flammability and brittleness of epoxy resin (EP) on its applications, a phosphorus‐containing oligomer (BID)...
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SubjectTerms Acids
anhydride
Bisphenol A
Calorimetry
Chromatography
Curing
Data analysis
epoxy resin
Epoxy resins
flame retardancy
Flame retardants
Flammability
Fourier transforms
Glass transition temperature
Itaconic acid
Mechanical properties
Methyltetrahydrophthalic anhydride
Molecular structure
Nitrogen
NMR
Nuclear magnetic resonance
Oligomers
Phosphorus
Reagents
Sample size
Solvents
Tensile strength
toughening
Vapor phases
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Title An Itaconic Acid‐Based Phosphorus‐Containing Oligomer Endowing Epoxy Resins with Good Flame Retardancy and Toughness
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fmame.202200550
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https://doaj.org/article/7c604ad29ffd46dea7bc14e7443ae7a2
Volume 308
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