Innovative sequential combination of fixed bed adsorption/desorption and photocatalysis cost-effective process to remove antibiotics in solution
[Display omitted] •Biocomposite beads as adsorbent were simply prepared from Reed plant.•Sequential combination of photocatalysis and adsorption was first time used to remove antibiotics.•Surface characterization confirm the success of adsorption and photodegradation process.•Ciprofloxacin photodegr...
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| Published in | Progress in organic coatings Vol. 151; p. 106014 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Lausanne
Elsevier B.V
01.02.2021
Elsevier BV Elsevier |
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| Abstract | [Display omitted]
•Biocomposite beads as adsorbent were simply prepared from Reed plant.•Sequential combination of photocatalysis and adsorption was first time used to remove antibiotics.•Surface characterization confirm the success of adsorption and photodegradation process.•Ciprofloxacin photodegradation mechanism was discussed.
In this paper, a Reed-based composite (R) beads, combined with photocatalysis, for the oxidative degradation of fluoroquinolones ciprofloxacin (CIP) in simulated hospital wastewater was developed. It is well known that hospital effluents present very diluted pollution (less than 5 mg/L), The first purpose, which concerns the first step to treat CIP solution (4 mg/L) via adsorption on (R) beads in continuous column system. The second aim was to regenerate the material for the simultaneous R reuse and CIP desorption in a low volume of a highly concentrated solution (≈30 mg/L). The third purpose was to degrade the concentrated solution of antibiotic using continuous and batch photocatalytic reactors. After CIP uptake on R-beads, two acid solutions were investigated for the regeneration step. Indeed desorption process was investigated using acetic acid (0.1 M) and hydrochloric acid (0.1 M) as eluents, leading to a highly concentrated CIP solution (≈30 mg/L) compared to the feed solution (4 mg/L). Consequently, these results provide new study into the application of sequential combination to effectively mineralize antibiotics with continuous treatment. |
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| AbstractList | [Display omitted]
•Biocomposite beads as adsorbent were simply prepared from Reed plant.•Sequential combination of photocatalysis and adsorption was first time used to remove antibiotics.•Surface characterization confirm the success of adsorption and photodegradation process.•Ciprofloxacin photodegradation mechanism was discussed.
In this paper, a Reed-based composite (R) beads, combined with photocatalysis, for the oxidative degradation of fluoroquinolones ciprofloxacin (CIP) in simulated hospital wastewater was developed. It is well known that hospital effluents present very diluted pollution (less than 5 mg/L), The first purpose, which concerns the first step to treat CIP solution (4 mg/L) via adsorption on (R) beads in continuous column system. The second aim was to regenerate the material for the simultaneous R reuse and CIP desorption in a low volume of a highly concentrated solution (≈30 mg/L). The third purpose was to degrade the concentrated solution of antibiotic using continuous and batch photocatalytic reactors. After CIP uptake on R-beads, two acid solutions were investigated for the regeneration step. Indeed desorption process was investigated using acetic acid (0.1 M) and hydrochloric acid (0.1 M) as eluents, leading to a highly concentrated CIP solution (≈30 mg/L) compared to the feed solution (4 mg/L). Consequently, these results provide new study into the application of sequential combination to effectively mineralize antibiotics with continuous treatment. In this paper, a Reed-based composite (R) beads, combined with photocatalysis, for the oxidative degradation of fluoroquinolones ciprofloxacin (CIP) in simulated hospital wastewater was developed. It is well known that hospital effluents present very diluted pollution (less than 5 mg/L), The first purpose, which concerns the first step to treat CIP solution (4 mg/L) via adsorption on (R) beads in continuous column system. The second aim was to regenerate the material for the simultaneous R reuse and CIP desorption in a low volume of a highly concentrated solution (≈30 mg/L). The third purpose was to degrade the concentrated solution of antibiotic using continuous and batch photocatalytic reactors. After CIP uptake on R-beads, two acid solutions were investigated for the regeneration step. Indeed desorption process was investigated using acetic acid (0.1 M) and hydrochloric acid (0.1 M) as eluents, leading to a highly concentrated CIP solution (≈30 mg/L) compared to the feed solution (4 mg/L). Consequently, these results provide new study into the application of sequential combination to effectively mineralize antibiotics with continuous treatment. In this paper, a Reed-based composite (R) beads, combined with photocatalysis, for the oxidative degradation of fluoroquinolones ciprofloxacin (CIP) in simulated hospital wastewater was developed. It is well known that hospital effluents present very diluted pollution (less than 5 mg/L), The first purpose, which concerns the first step to treat CIP solution (4 mg/L) via adsorption on (R) beads in continuous column system. The second aim was to regenerate the material for the simultaneous R reuse and CIP desorption in a low volume of a highly concentrated solution (≈30 mg/L). The third purpose was to degrade the concentrated solution of antibiotic using continuous and batch photocatalytic reactors. After CIP uptake on R-beads, two acid solutions were investigated for the regeneration step. Indeed desorption process was investigated using acetic acid (0.1 M) and hydrochloric acid (0.1 M) as eluents, leading to a highly concentrated CIP solution (≈30 mg/L) compared to the feed solution (4 mg/L). Consequently, these results provide new study into the application of sequential combination to effectively mineralize antibiotics with continuous treatment. © 2020 Elsevier B.V. |
| ArticleNumber | 106014 |
| Author | Karoui, Sarra Arfi, Rim Ben Amrane, Abdeltif Assadi, Aymen Amine Ghorbal, Achraf |
| Author_xml | – sequence: 1 givenname: Sarra surname: Karoui fullname: Karoui, Sarra organization: Research Laboratory LR18ES33, National Engineering School of Gabes, University of Gabes, Tunisia – sequence: 2 givenname: Rim Ben surname: Arfi fullname: Arfi, Rim Ben organization: Research Laboratory LR18ES33, National Engineering School of Gabes, University of Gabes, Tunisia – sequence: 3 givenname: Achraf surname: Ghorbal fullname: Ghorbal, Achraf organization: Research Laboratory LR18ES33, National Engineering School of Gabes, University of Gabes, Tunisia – sequence: 4 givenname: Abdeltif surname: Amrane fullname: Amrane, Abdeltif organization: Univ Rennes, École Nationale Supérieure de Chimie de Rennes, CNRS, ISCR, UMR 6226, F-35000 Rennes, France – sequence: 5 givenname: Aymen Amine surname: Assadi fullname: Assadi, Aymen Amine email: aymen.assadi@ensc-rennes.fr organization: Univ Rennes, École Nationale Supérieure de Chimie de Rennes, CNRS, ISCR, UMR 6226, F-35000 Rennes, France |
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| Keywords | Regeneration Adsorption Reed-based composite (R) beads Photocatalysis Antibiotic removal |
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•Biocomposite beads as adsorbent were simply prepared from Reed plant.•Sequential combination of photocatalysis and adsorption was first time... In this paper, a Reed-based composite (R) beads, combined with photocatalysis, for the oxidative degradation of fluoroquinolones ciprofloxacin (CIP) in... |
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| SubjectTerms | Acetic acid Adsorption Antibiotic removal Antibiotics Beads Chemical Sciences Desorption Fixed beds Hydrochloric acid Photocatalysis Reed-based composite (R) beads Regeneration Wastewater |
| Title | Innovative sequential combination of fixed bed adsorption/desorption and photocatalysis cost-effective process to remove antibiotics in solution |
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