Green synthesis of zerovalent copper nanoparticles for efficient reduction of toxic azo dyes congo red and methyl orange

In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method accounts for the green chemistry approach using the fruit extract of for the first time. The UV-visible spectrum of the CuNPs solution showed...

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Published inGreen processing and synthesis Vol. 8; no. 1; pp. 135 - 143
Main Authors Ismail, Muhammad, Gul, Saima, Khan, M.I., Khan, Murad Ali, Asiri, Abdullah M., Khan, Sher Bahadar
Format Journal Article
LanguageEnglish
Published Berlin De Gruyter 28.01.2019
Walter de Gruyter GmbH
Subjects
azo dye effluents
Azo dyes
Carcinogens
Catalysis
Chemical reduction
Copper
copper nanoparticles
Diffraction patterns
Dyes
Emission analysis
Energy dispersive X ray spectroscopy
Field emission microscopy
Fourier transforms
Fruits
Green chemistry
Infrared spectroscopy
Morphology
Nanoparticles
Organic chemistry
Purification
Rate constants
Reducing agents
Scanning electron microscopy
Synthesis
Visible spectrum
Water purification
X-ray diffraction
X-ray spectroscopy
Online AccessGet full text
ISSN2191-9542
2191-9550
2191-9550
DOI10.1515/gps-2018-0038

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Abstract In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method accounts for the green chemistry approach using the fruit extract of for the first time. The UV-visible spectrum of the CuNPs solution showed a distinct absorption peak at 588 nm. Fourier transform infrared spectroscopy confirmed that the fruit extract is responsible for the reduction as well as the stabilization of CuNPs. X-ray diffraction patterns conform the crystalline nature of CuNPs. Energy-dispersive X-ray spectroscopy was performed for elemental analysis whereas field emission scanning electron microscopy was carried out for surface morphology. Prepared CuNPs were used for the reduction of carcinogenic azo dyes methyl orange (MO) and congo red (CR). CuNPs exhibit outstanding catalytic reduction for MO and CR in the presence of NaBH as reducing agents with the pseudo-first-order rate constants of 8.6×10 s and 5.07×10 s for MO and CR, respectively. Thus, natural plant materials act as cheap and environmentally friendly support for the synthesis of CuNPs and could be used for the purification of water from organic dye effluents.
AbstractList In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method accounts for the green chemistry approach using the fruit extract of for the first time. The UV-visible spectrum of the CuNPs solution showed a distinct absorption peak at 588 nm. Fourier transform infrared spectroscopy confirmed that the fruit extract is responsible for the reduction as well as the stabilization of CuNPs. X-ray diffraction patterns conform the crystalline nature of CuNPs. Energy-dispersive X-ray spectroscopy was performed for elemental analysis whereas field emission scanning electron microscopy was carried out for surface morphology. Prepared CuNPs were used for the reduction of carcinogenic azo dyes methyl orange (MO) and congo red (CR). CuNPs exhibit outstanding catalytic reduction for MO and CR in the presence of NaBH as reducing agents with the pseudo-first-order rate constants of 8.6×10 s and 5.07×10 s for MO and CR, respectively. Thus, natural plant materials act as cheap and environmentally friendly support for the synthesis of CuNPs and could be used for the purification of water from organic dye effluents.
In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method accounts for the green chemistry approach using the fruit extract of Duranta erecta for the first time. The UV-visible spectrum of the CuNPs solution showed a distinct absorption peak at 588 nm. Fourier transform infrared spectroscopy confirmed that the fruit extract is responsible for the reduction as well as the stabilization of CuNPs. X-ray diffraction patterns conform the crystalline nature of CuNPs. Energy-dispersive X-ray spectroscopy was performed for elemental analysis whereas field emission scanning electron microscopy was carried out for surface morphology. Prepared CuNPs were used for the reduction of carcinogenic azo dyes methyl orange (MO) and congo red (CR). CuNPs exhibit outstanding catalytic reduction for MO and CR in the presence of NaBH4 as reducing agents with the pseudo-first-order rate constants of 8.6×10−3 s−1 and 5.07×10−3 s−1 for MO and CR, respectively. Thus, natural plant materials act as cheap and environmentally friendly support for the synthesis of CuNPs and could be used for the purification of water from organic dye effluents.
In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method accounts for the green chemistry approach using the fruit extract of Duranta erecta for the first time. The UV-visible spectrum of the CuNPs solution showed a distinct absorption peak at 588 nm. Fourier transform infrared spectroscopy confirmed that the fruit extract is responsible for the reduction as well as the stabilization of CuNPs. X-ray diffraction patterns conform the crystalline nature of CuNPs. Energy-dispersive X-ray spectroscopy was performed for elemental analysis whereas field emission scanning electron microscopy was carried out for surface morphology. Prepared CuNPs were used for the reduction of carcinogenic azo dyes methyl orange (MO) and congo red (CR). CuNPs exhibit outstanding catalytic reduction for MO and CR in the presence of NaBH 4 as reducing agents with the pseudo-first-order rate constants of 8.6×10 −3 s −1 and 5.07×10 −3 s −1 for MO and CR, respectively. Thus, natural plant materials act as cheap and environmentally friendly support for the synthesis of CuNPs and could be used for the purification of water from organic dye effluents.
Author Khan, M.I.
Khan, Murad Ali
Ismail, Muhammad
Khan, Sher Bahadar
Asiri, Abdullah M.
Gul, Saima
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  fullname: Gul, Saima
  organization: Department of Chemistry, Kohat University of Science & Technology, Kohat 26000, Khyber Pakhtunkhwa, Pakistan
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  surname: Khan
  fullname: Khan, M.I.
  organization: Department of Chemistry, Kohat University of Science & Technology, Kohat 26000, Khyber Pakhtunkhwa, Pakistan
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  givenname: Murad Ali
  surname: Khan
  fullname: Khan, Murad Ali
  organization: Department of Chemistry, Kohat University of Science & Technology, Kohat 26000, Khyber Pakhtunkhwa, Pakistan
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  givenname: Abdullah M.
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  givenname: Sher Bahadar
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  fullname: Khan, Sher Bahadar
  email: sbkhan@kau.edu.sa
  organization: Chemistry Department, Faculty of Science, King Abdulaziz University, P.O. Box 80203, Jeddah 21589, Saudi Arabia
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Snippet In this study, plant-mediated copper nanoparticles (CuNPs) were synthesized. Due to its direct synthesis mechanism and eco-friendly nature, the current method...
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SubjectTerms azo dye effluents
Azo dyes
Carcinogens
Catalysis
Chemical reduction
Copper
copper nanoparticles
Diffraction patterns
Dyes
Emission analysis
Energy dispersive X ray spectroscopy
Field emission microscopy
Fourier transforms
Fruits
Green chemistry
Infrared spectroscopy
Morphology
Nanoparticles
Organic chemistry
Purification
Rate constants
Reducing agents
Scanning electron microscopy
Synthesis
Visible spectrum
Water purification
X-ray diffraction
X-ray spectroscopy
Title Green synthesis of zerovalent copper nanoparticles for efficient reduction of toxic azo dyes congo red and methyl orange
URI https://www.degruyter.com/doi/10.1515/gps-2018-0038
https://www.proquest.com/docview/2194246132
https://doaj.org/article/7e01544c89e1464fa06b0e2d6350ef13
Volume 8
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