Structural Control of Mesoporous 1,4-Phenylene-silica Using the Mixture of CTAB/SDS
The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium bromide （CTAB） and sodium dodecylsulfate （SDS）. When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4-phenyle...
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| Published in | Chinese journal of chemistry Vol. 29; no. 5; pp. 883 - 887 |
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| Format | Journal Article |
| Language | English |
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WILEY-VCH Verlag
01.05.2011
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| Abstract | The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium bromide （CTAB） and sodium dodecylsulfate （SDS）. When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4-phenylene-silicas changed in a sequence of sphere, hexagonal short rod, worm-like, bent flake and flower-like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4-phenylene-silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod-like micelles during the reaction process. |
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| AbstractList | The morphology, pore architecture and crystallinity of the mesoporous 1,4‐phenylene‐silicas were controlled using the mixtures of cetyltrimethylammonium bromide (CTAB) and sodium dodecylsulfate (SDS). When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4‐phenylene‐silicas changed in a sequence of sphere, hexagonal short rod, worm‐like, bent flake and flower‐like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4‐phenylene‐silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod‐like micelles during the reaction process.
The morphology, pore architecture and crystallinity of the mesoporous 1,4‐phenylene‐silicas were controlled using the mixtures of cetyltrimethylammonium bromide (CTAB) and sodium dodecylsulfate (SDS). The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium bromide (CTAB) and sodium dodecylsulfate (SDS). When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4-phenylene-silicas changed in a sequence of sphere, hexagonal short rod, worm-like, bent flake and flower-like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4-phenylene-silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod-like micelles during the reaction process. The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium bromide （CTAB） and sodium dodecylsulfate （SDS）. When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4-phenylene-silicas changed in a sequence of sphere, hexagonal short rod, worm-like, bent flake and flower-like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4-phenylene-silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod-like micelles during the reaction process. Abstract The morphology, pore architecture and crystallinity of the mesoporous 1,4‐phenylene‐silicas were controlled using the mixtures of cetyltrimethylammonium bromide (CTAB) and sodium dodecylsulfate (SDS). When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4‐phenylene‐silicas changed in a sequence of sphere, hexagonal short rod, worm‐like, bent flake and flower‐like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4‐phenylene‐silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod‐like micelles during the reaction process. |
| Author | Bi, Lifeng Yang, Yonggang Zhuang, Wei Wang, Sibing Li, Yi Li, Baozong Zhang, Ming |
| AuthorAffiliation | Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou, Jiangsu 215123, China |
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| CitedBy_id | crossref_primary_10_1002_slct_202400483 crossref_primary_10_1002_cjoc_201280026 crossref_primary_10_1016_j_polymer_2021_123862 crossref_primary_10_1007_s00396_014_3191_2 crossref_primary_10_1177_15280837221077129 |
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| Copyright | Copyright © 2011 SIOC, CAS, Shanghai & WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2011 SIOC, CAS, Shanghai & WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim |
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| Notes | 31-1547/O6 The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium bromide （CTAB） and sodium dodecylsulfate （SDS）. When the SDS/CTAB molar ratio increased from 0 to 1.0, the morphology of the mesoporous 1,4-phenylene-silicas changed in a sequence of sphere, hexagonal short rod, worm-like, bent flake and flower-like structure; the pore architecture of them changed from a hexagonal arranged tubular structure to a lamellar one; and the organization of the smallest repeat units within the wall changed from a random structure to a crystalline structure. At the SDS/CTAB molar ratios of 0.3 and 0.5, 1,4-phenylene-silica nanofibers with lamellar mesopores outside and tubular pore channels inside were obtained. The lamellar mesopores should be formed by merging the rod-like micelles during the reaction process. Zhuang Wei, Bi Lifeng, Zhang, Ming, Wang Sibing, Li Yi, Li Baozong, Yang Yonggang（ Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou, Jiangsu 215123, China） mesoporous, 1,4-phenylene-silica, surfactants, sol-gel processes, self-assembly istex:DBC919ECA989DC0A75C236ADAEA29BCDA42D57F1 the National Natural Science Foundation of China - No. 20871087 ArticleID:CJOC201190183 the Program of Innovative Research Team of Soochow University, Program for New Century Excellent Talents in University - No. NCET-08-0698 ark:/67375/WNG-B55XP2VC-4 |
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| Snippet | The morphology, pore architecture and crystallinity of the mesoporous 1,4-phenylene-silicas were controlled using the mixtures of cetyltrimethylammonium... The morphology, pore architecture and crystallinity of the mesoporous 1,4‐phenylene‐silicas were controlled using the mixtures of cetyltrimethylammonium... Abstract The morphology, pore architecture and crystallinity of the mesoporous 1,4‐phenylene‐silicas were controlled using the mixtures of... |
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| SubjectTerms | 1,4‐phenylene‐silica 4-phenylene-silica CTAB mesoporous Morphology SDS self-assembly Silica sol-gel processes surfactants 二氧化硅 介孔 十二烷基硫酸钠 十六烷基三甲基溴化铵 混合使用 结构控制 |
| Title | Structural Control of Mesoporous 1,4-Phenylene-silica Using the Mixture of CTAB/SDS |
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