Electrochemical synthesis of NiCo layered double hydroxide nanosheets decorated on moderately oxidized graphene films for energy storage
The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remain...
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| Published in | Nanoscale Vol. 11; no. 6; pp. 2812 - 2822 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
01.01.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO)
via
an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π–π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed
via
electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm
−3
), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles). |
|---|---|
| AbstractList | The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO) via an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π–π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed via electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm−3), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles). The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO) via an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π-π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed via electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm-3), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles).The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO) via an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π-π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed via electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm-3), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles). The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO) via an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π-π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed via electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm-3), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles). The introduction of oxygenous functional groups onto graphene can provide additional pseudocapacitance for supercapacitors. However, how to balance the amount of introduced oxygenous functional groups and the reduced electrical conductivity arising from the disruption of the conjugated system remains a big challenge. Here, a controllable strategy is reported to prepare moderately oxidized reduced graphene oxide (MORGO) via an electrochemical oxidation process. The MORGO not only has oxygenous groups with appropriate quantities, but also preserves the highly crystalline structure of the π–π conjugated carbon framework. As a result, the MORGO films showed superior electrochemical properties to the pristine RGO films and other previously reported RGO films. Furthermore, the oxygenous groups and the conductivity of MORGO films can be easily adjusted by controlling the oxidation time. A hierarchical composite of NiCo-layered double hydroxide nanosheet arrays on MORGO films (MORGO/NiCo-LDH) was also constructed via electrochemical deposition to combine the advantages of electric double-layer electrode materials and faradaic electrode materials. The flexible solid-state supercapacitor fabricated with MORGO/NiCo-LDH film electrodes exhibits a high energy density (0.51 mW h cm −3 ), as well as a long cycle life (88.2% capacitance retention after 10 000 cycles). |
| Author | Tan, Hua Cao, Xueying Liu, Jingquan Jia, Dedong Yue, Lijun Zheng, Yiwei Jiang, Degang Liu, Fang Sun, Yuanyuan |
| Author_xml | – sequence: 1 givenname: Dedong surname: Jia fullname: Jia, Dedong organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 2 givenname: Degang surname: Jiang fullname: Jiang, Degang organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 3 givenname: Yiwei surname: Zheng fullname: Zheng, Yiwei organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 4 givenname: Hua surname: Tan fullname: Tan, Hua organization: School of Physical and Mathematical Sciences, Nanyang Technological University, Singapore 637371, Singapore – sequence: 5 givenname: Xueying surname: Cao fullname: Cao, Xueying organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 6 givenname: Fang surname: Liu fullname: Liu, Fang organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 7 givenname: Lijun surname: Yue fullname: Yue, Lijun organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 8 givenname: Yuanyuan surname: Sun fullname: Sun, Yuanyuan organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China – sequence: 9 givenname: Jingquan orcidid: 0000-0001-6178-8661 surname: Liu fullname: Liu, Jingquan organization: College of Material Science and Engineering, Institute for Graphene Applied Technology Innovation, Qingdao University, Qingdao 266071, China |
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| SubjectTerms | Disruption Electrical resistivity Electrochemical analysis Electrochemical oxidation Electrode materials Electrodes Energy storage Flux density Functional groups Graphene Hydroxides Nanosheets Oxidation Stability Supercapacitors |
| Title | Electrochemical synthesis of NiCo layered double hydroxide nanosheets decorated on moderately oxidized graphene films for energy storage |
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