Ultraviolet (UV) light-activated persulfate oxidation of sulfamethazine in water

► Effective SMT degradation can be achieved by UV/persulfate oxidation treatment. ► The degradation rate and mineralization degree of SMT were influenced by the S2O82- dose and pH. ► Mass spectrometry was applied for identification of intermediates and products. ► Degradation mechanisms were propose...

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Published inChemical engineering journal (Lausanne, Switzerland : 1996) Vol. 195-196; pp. 248 - 253
Main Authors Gao, Yu-qiong, Gao, Nai-yun, Deng, Yang, Yang, Yi-qiong, Ma, Yan
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.07.2012
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Abstract ► Effective SMT degradation can be achieved by UV/persulfate oxidation treatment. ► The degradation rate and mineralization degree of SMT were influenced by the S2O82- dose and pH. ► Mass spectrometry was applied for identification of intermediates and products. ► Degradation mechanisms were proposed according to the results of LC–MS analysis. Ultraviolet light (UV)/persulfate (S2O82-) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel photo-reactor. During the treatment, UV photolytic S2O82- activation to produce highly reactive sulfate radicals (SO4-) to decompose SMT in water. The treatment was advantageous over direct photolysis or persulfate oxidation alone and UV/H2O2 oxidation, suggesting that SO4- is a very effective agent to remove SMT from water. Under the experimental conditions, the SMT degradation exhibited a pseudo-first-order reaction pattern. The degradation rate was influenced by the S2O82- dose and solution pH. Typically, a high persulfate dose could achieve a high SMT removal. In contrast, both the highest SMT degradation rate and the lowest mineralization degree were observed at pH 6.5, while the highest mineralization extent was accomplished at pH 11. The complex pH effect may be associated with the fact that the total radical concentration and fractions of the different radicals were varied with pH. Finally, the major SMT degradation products were identified, and the primary reaction pathways were proposed. This study demonstrated that UV/persulfate is a viable option for controlling SMT pollution in water.
AbstractList Ultraviolet light (UV)/persulfate (S₂O₈ ²⁻) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel photo-reactor. During the treatment, UV photolytic S₂O₈ ²⁻ activation to produce highly reactive sulfate radicals (SO₄ ⁻) to decompose SMT in water. The treatment was advantageous over direct photolysis or persulfate oxidation alone and UV/H₂O₂ oxidation, suggesting that SO₄ ⁻ is a very effective agent to remove SMT from water. Under the experimental conditions, the SMT degradation exhibited a pseudo-first-order reaction pattern. The degradation rate was influenced by the S₂O₈ ²⁻ dose and solution pH. Typically, a high persulfate dose could achieve a high SMT removal. In contrast, both the highest SMT degradation rate and the lowest mineralization degree were observed at pH 6.5, while the highest mineralization extent was accomplished at pH 11. The complex pH effect may be associated with the fact that the total radical concentration and fractions of the different radicals were varied with pH. Finally, the major SMT degradation products were identified, and the primary reaction pathways were proposed. This study demonstrated that UV/persulfate is a viable option for controlling SMT pollution in water.
► Effective SMT degradation can be achieved by UV/persulfate oxidation treatment. ► The degradation rate and mineralization degree of SMT were influenced by the S2O82- dose and pH. ► Mass spectrometry was applied for identification of intermediates and products. ► Degradation mechanisms were proposed according to the results of LC–MS analysis. Ultraviolet light (UV)/persulfate (S2O82-) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel photo-reactor. During the treatment, UV photolytic S2O82- activation to produce highly reactive sulfate radicals (SO4-) to decompose SMT in water. The treatment was advantageous over direct photolysis or persulfate oxidation alone and UV/H2O2 oxidation, suggesting that SO4- is a very effective agent to remove SMT from water. Under the experimental conditions, the SMT degradation exhibited a pseudo-first-order reaction pattern. The degradation rate was influenced by the S2O82- dose and solution pH. Typically, a high persulfate dose could achieve a high SMT removal. In contrast, both the highest SMT degradation rate and the lowest mineralization degree were observed at pH 6.5, while the highest mineralization extent was accomplished at pH 11. The complex pH effect may be associated with the fact that the total radical concentration and fractions of the different radicals were varied with pH. Finally, the major SMT degradation products were identified, and the primary reaction pathways were proposed. This study demonstrated that UV/persulfate is a viable option for controlling SMT pollution in water.
Ultraviolet light (UV)/persulfate ( S 2 O 8 2 - ) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel photo-reactor. During the treatment, UV photolytic S 2 O 8 2 - activation to produce highly reactive sulfate radicals ( SO 4 - ) to decompose SMT in water. The treatment was advantageous over direct photolysis or persulfate oxidation alone and UV/H2O2 oxidation, suggesting that SO 4 - is a very effective agent to remove SMT from water. Under the experimental conditions, the SMT degradation exhibited a pseudo-first-order reaction pattern. The degradation rate was influenced by the S 2 O 8 2 - dose and solution pH. Typically, a high persulfate dose could achieve a high SMT removal. In contrast, both the highest SMT degradation rate and the lowest mineralization degree were observed at pH 6.5, while the highest mineralization extent was accomplished at pH 11. The complex pH effect may be associated with the fact that the total radical concentration and fractions of the different radicals were varied with pH. Finally, the major SMT degradation products were identified, and the primary reaction pathways were proposed. This study demonstrated that UV/persulfate is a viable option for controlling SMT pollution in water.
Author Deng, Yang
Yang, Yi-qiong
Gao, Yu-qiong
Gao, Nai-yun
Ma, Yan
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  surname: Gao
  fullname: Gao, Yu-qiong
  organization: State Key Laboratory of Pollution Control and Resources Reuse, Ministry of Education, College of Environmental Science and Engineering, Tongji University, Shanghai 200092, PR China
– sequence: 2
  givenname: Nai-yun
  surname: Gao
  fullname: Gao, Nai-yun
  email: gaonaiyun2011@yahoo.com.cn
  organization: State Key Laboratory of Pollution Control and Resources Reuse, Ministry of Education, College of Environmental Science and Engineering, Tongji University, Shanghai 200092, PR China
– sequence: 3
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  surname: Deng
  fullname: Deng, Yang
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– sequence: 4
  givenname: Yi-qiong
  surname: Yang
  fullname: Yang, Yi-qiong
  organization: State Key Laboratory of Pollution Control and Resources Reuse, Ministry of Education, College of Environmental Science and Engineering, Tongji University, Shanghai 200092, PR China
– sequence: 5
  givenname: Yan
  surname: Ma
  fullname: Ma, Yan
  organization: State Key Laboratory of Pollution Control and Resources Reuse, Ministry of Education, College of Environmental Science and Engineering, Tongji University, Shanghai 200092, PR China
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Snippet ► Effective SMT degradation can be achieved by UV/persulfate oxidation treatment. ► The degradation rate and mineralization degree of SMT were influenced by...
Ultraviolet light (UV)/persulfate (S₂O₈ ²⁻) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel...
Ultraviolet light (UV)/persulfate ( S 2 O 8 2 - ) oxidation of a pharmaceutically active compound, sulfamethazine (SMT), was studied in a stainless steel...
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StartPage 248
SubjectTerms chemical engineering
Degradation
free radicals
Intermediates
mineralization
oxidation
photolysis
stainless steel
Sulfamethazine
Sulfate radicals
ultraviolet radiation
water pollution
Title Ultraviolet (UV) light-activated persulfate oxidation of sulfamethazine in water
URI https://dx.doi.org/10.1016/j.cej.2012.04.084
https://search.proquest.com/docview/1038611928
Volume 195-196
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