Influence of Calcination Temperature on Activity and Selectivity of Ni–CeO2 and Ni–Ce0.8Zr0.2O2 Catalysts for CO2 Methanation

Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO 2 and Ni/Ce 0.8 Zr 0.2 O 2 catalysts on the specific surface area, pore volume, crystalline size, lattice parameter, chemical bonding and oxidation states, nickel dispersion and CH 4 /CO production rate in CO 2 methan...

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Published in	Topics in catalysis Vol. 61; no. 15-17; pp. 1514 - 1527
Main Authors	Yu, Yang, Bian, Zhoufeng, Song, Fujiao, Wang, Juan, Zhong, Qin, Kawi, Sibudjing
Format	Journal Article
Language	English
Published	New York Springer US 01.10.2018 Springer Nature B.V
Subjects	Carbon dioxide Catalysis Catalysts Cerium oxides Characterization and Evaluation of Materials Chemical bonds Chemistry Chemistry and Materials Science Dispersion Industrial Chemistry/Chemical Engineering Methanation Methane Nickel Organic chemistry OriginalPaper Oxidation Pharmacy Physical Chemistry Roasting Zirconium Ni/CeO Zr In-situ DRIFTS methanation CO Ni/Ce Calcination temperature O
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ISSN	1022-5528 1572-9028
DOI	10.1007/s11244-018-1010-6

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Abstract	Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO 2 and Ni/Ce 0.8 Zr 0.2 O 2 catalysts on the specific surface area, pore volume, crystalline size, lattice parameter, chemical bonding and oxidation states, nickel dispersion and CH 4 /CO production rate in CO 2 methanation. In general, the catalytic performance revealed that Zr doping catalysts could increase the CH 4 production rate. Combined with the production rate and the characterizations results, we found that the combination of nickel dispersion, peak area of CO 2 –TPD and O II /(O II + O I )) play the critical role in increasing the CH 4 production rate. It is well to be mentioned that the CO production rate is strongly influenced by the nickel dispersion. Furthermore, the in-situ DRIFTS confirmed that the CO originates from the decomposition of H-assisted formate species.
AbstractList	Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO 2 and Ni/Ce 0.8 Zr 0.2 O 2 catalysts on the specific surface area, pore volume, crystalline size, lattice parameter, chemical bonding and oxidation states, nickel dispersion and CH 4 /CO production rate in CO 2 methanation. In general, the catalytic performance revealed that Zr doping catalysts could increase the CH 4 production rate. Combined with the production rate and the characterizations results, we found that the combination of nickel dispersion, peak area of CO 2 –TPD and O II /(O II + O I )) play the critical role in increasing the CH 4 production rate. It is well to be mentioned that the CO production rate is strongly influenced by the nickel dispersion. Furthermore, the in-situ DRIFTS confirmed that the CO originates from the decomposition of H-assisted formate species. Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO2 and Ni/Ce0.8Zr0.2O2 catalysts on the specific surface area, pore volume, crystalline size, lattice parameter, chemical bonding and oxidation states, nickel dispersion and CH4/CO production rate in CO2 methanation. In general, the catalytic performance revealed that Zr doping catalysts could increase the CH4 production rate. Combined with the production rate and the characterizations results, we found that the combination of nickel dispersion, peak area of CO2–TPD and OII/(OII + OI)) play the critical role in increasing the CH4 production rate. It is well to be mentioned that the CO production rate is strongly influenced by the nickel dispersion. Furthermore, the in-situ DRIFTS confirmed that the CO originates from the decomposition of H-assisted formate species.
Author	Yu, Yang Kawi, Sibudjing Zhong, Qin Bian, Zhoufeng Wang, Juan Song, Fujiao
Author_xml	– sequence: 1 givenname: Yang surname: Yu fullname: Yu, Yang organization: Department of Chemical and Biomolecular Engineering, National University of Singapore, School of Chemical Engineering, Nanjing University of Science and Technology – sequence: 2 givenname: Zhoufeng surname: Bian fullname: Bian, Zhoufeng organization: Department of Chemical and Biomolecular Engineering, National University of Singapore – sequence: 3 givenname: Fujiao surname: Song fullname: Song, Fujiao organization: School of Environmental Science and Engineering, Yancheng Institute of Technology – sequence: 4 givenname: Juan surname: Wang fullname: Wang, Juan organization: Department of Chemical and Biomolecular Engineering, National University of Singapore, School of Chemical Engineering, Nanjing University of Science and Technology – sequence: 5 givenname: Qin surname: Zhong fullname: Zhong, Qin email: zq304@njust.edu.cn organization: School of Chemical Engineering, Nanjing University of Science and Technology – sequence: 6 givenname: Sibudjing surname: Kawi fullname: Kawi, Sibudjing email: chekawis@nus.edu.sg organization: Department of Chemical and Biomolecular Engineering, National University of Singapore
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Snippet	Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO 2 and Ni/Ce 0.8 Zr 0.2 O 2 catalysts on the specific surface area, pore... Herein, we studied the influence of calcination temperature (500–800 °C) of Ni/CeO2 and Ni/Ce0.8Zr0.2O2 catalysts on the specific surface area, pore volume,...
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StartPage	1514
SubjectTerms	Carbon dioxide Catalysis Catalysts Cerium oxides Characterization and Evaluation of Materials Chemical bonds Chemistry Chemistry and Materials Science Dispersion Industrial Chemistry/Chemical Engineering Methanation Methane Nickel Organic chemistry OriginalPaper Oxidation Pharmacy Physical Chemistry Roasting Zirconium
Title	Influence of Calcination Temperature on Activity and Selectivity of Ni–CeO2 and Ni–Ce0.8Zr0.2O2 Catalysts for CO2 Methanation
URI	https://link.springer.com/article/10.1007/s11244-018-1010-6 https://www.proquest.com/docview/2117175692
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