The construction of double type II heterostructure from CdS and Ni-MOF-74 with two structures and enhanced mechanism of photocatalytic water splitting

Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized b...

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Published inJournal of materials science Vol. 57; no. 10; pp. 5768 - 5787
Main Authors Niu, Lu, Zhang, Wang-gang, Li, Hao-tian, Wang, Hong-xia, Wang, Jian, Liu, Yi-ming
Format Journal Article
LanguageEnglish
Published New York Springer US 01.03.2022
Springer
Springer Nature B.V
Subjects
Analysis
Characterization and Evaluation of Materials
Chemical Routes to Materials
Chemistry and Materials Science
Classical Mechanics
Composite materials
Conduction bands
Crystallography and Scattering Methods
Heterostructures
Hydrogen
Hydrogen evolution
Hydrogen production
irradiation
light
Light irradiation
Materials Science
Morphology
Nanoparticles
Optical properties
Photocatalysis
Polymer Sciences
Povidone
Solid Mechanics
Water splitting
X ray photoelectron spectroscopy
Online AccessGet full text

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Abstract Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized by controlling the amount (X mL) of added water. Then, various CdS/Ni-MOF-74 composites were prepared by simple mechanical mixing of Ni-MOF-74(X) and CdS nanoparticles. The morphology and structures of CdS, Ni-MOF-74(X), and CdS/Ni-MOF-74(X) were analyzed by SEM, TEM, XRD, FT-IR, BET, and XPS. The optical properties of the composites were analyzed by UV–visible DRS, PL, TRPL, and photoelectrochemical experiments. The results show that Ni-MOF-74 is formed with a Ni 3 (OH) 2 (H 2 O) 2 (tp) 2 structure (tp: terephthalate) at low water amounts and with a [Ni 3 (OH) 2 (H 2 O) 4 (tp) 2 ]·2H 2 O structure when sufficient water was present to promote its formation. Mixed structures of Ni-MOF-74 containing Ni 3 (OH) 2 (H 2 O) 2 (tp) 2 and [Ni 3 (OH) 2 (H 2 O) 4 (tp) 2 ]·2H 2 O are formed when the water amount is between 5 and 40 mL. The CdS/Ni-MOF-74(15) composite has the best photocatalytic hydrogen evolution performance under visible light irradiation, and the maximum produced hydrogen amount is 3117.9 μmol after 3 h, which is 12.8 times that of pure CdS nanoparticles. The composite of CdS and Ni-MOF-74 with a mixed structure exhibits better photocatalytic hydrogen production performance than the composite based on Ni-MOF-74 with a single structure. As an explanation for the superior activity, a double type II heterostructure is formed by CdS and Ni-MOF-74 with two structures. The photogenerated electrons in the conduction band (CB) of CdS spontaneously transfer to the CB of Ni-MOF-74, which is beneficial to the improvement in the separation of photogenerated carriers in hydrogen evolution.
AbstractList Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized by controlling the amount (X mL) of added water. Then, various CdS/Ni-MOF-74 composites were prepared by simple mechanical mixing of Ni-MOF-74(X) and CdS nanoparticles. The morphology and structures of CdS, Ni-MOF-74(X), and CdS/Ni-MOF-74(X) were analyzed by SEM, TEM, XRD, FT-IR, BET, and XPS. The optical properties of the composites were analyzed by UV–visible DRS, PL, TRPL, and photoelectrochemical experiments. The results show that Ni-MOF-74 is formed with a Ni3(OH)2(H2O)2(tp)2 structure (tp: terephthalate) at low water amounts and with a [Ni3(OH)2(H2O)4(tp)2]·2H2O structure when sufficient water was present to promote its formation. Mixed structures of Ni-MOF-74 containing Ni3(OH)2(H2O)2(tp)2 and [Ni3(OH)2(H2O)4(tp)2]·2H2O are formed when the water amount is between 5 and 40 mL. The CdS/Ni-MOF-74(15) composite has the best photocatalytic hydrogen evolution performance under visible light irradiation, and the maximum produced hydrogen amount is 3117.9 μmol after 3 h, which is 12.8 times that of pure CdS nanoparticles. The composite of CdS and Ni-MOF-74 with a mixed structure exhibits better photocatalytic hydrogen production performance than the composite based on Ni-MOF-74 with a single structure. As an explanation for the superior activity, a double type II heterostructure is formed by CdS and Ni-MOF-74 with two structures. The photogenerated electrons in the conduction band (CB) of CdS spontaneously transfer to the CB of Ni-MOF-74, which is beneficial to the improvement in the separation of photogenerated carriers in hydrogen evolution.
Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized by controlling the amount (X mL) of added water. Then, various CdS/Ni-MOF-74 composites were prepared by simple mechanical mixing of Ni-MOF-74(X) and CdS nanoparticles. The morphology and structures of CdS, Ni-MOF-74(X), and CdS/Ni-MOF-74(X) were analyzed by SEM, TEM, XRD, FT-IR, BET, and XPS. The optical properties of the composites were analyzed by UV–visible DRS, PL, TRPL, and photoelectrochemical experiments. The results show that Ni-MOF-74 is formed with a Ni₃(OH)₂(H₂O)₂(tp)₂ structure (tp: terephthalate) at low water amounts and with a [Ni₃(OH)₂(H₂O)₄(tp)₂]·2H₂O structure when sufficient water was present to promote its formation. Mixed structures of Ni-MOF-74 containing Ni₃(OH)₂(H₂O)₂(tp)₂ and [Ni₃(OH)₂(H₂O)₄(tp)₂]·2H₂O are formed when the water amount is between 5 and 40 mL. The CdS/Ni-MOF-74(15) composite has the best photocatalytic hydrogen evolution performance under visible light irradiation, and the maximum produced hydrogen amount is 3117.9 μmol after 3 h, which is 12.8 times that of pure CdS nanoparticles. The composite of CdS and Ni-MOF-74 with a mixed structure exhibits better photocatalytic hydrogen production performance than the composite based on Ni-MOF-74 with a single structure. As an explanation for the superior activity, a double type II heterostructure is formed by CdS and Ni-MOF-74 with two structures. The photogenerated electrons in the conduction band (CB) of CdS spontaneously transfer to the CB of Ni-MOF-74, which is beneficial to the improvement in the separation of photogenerated carriers in hydrogen evolution.
Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized by controlling the amount (X mL) of added water. Then, various CdS/Ni-MOF-74 composites were prepared by simple mechanical mixing of Ni-MOF-74(X) and CdS nanoparticles. The morphology and structures of CdS, Ni-MOF-74(X), and CdS/Ni-MOF-74(X) were analyzed by SEM, TEM, XRD, FT-IR, BET, and XPS. The optical properties of the composites were analyzed by UV-visible DRS, PL, TRPL, and photoelectrochemical experiments. The results show that Ni-MOF-74 is formed with a Ni.sub.3(OH).sub.2(H.sub.2O).sub.2(tp).sub.2 structure (tp: terephthalate) at low water amounts and with a [Ni.sub.3(OH).sub.2(H.sub.2O).sub.4(tp).sub.2]·2H.sub.2O structure when sufficient water was present to promote its formation. Mixed structures of Ni-MOF-74 containing Ni.sub.3(OH).sub.2(H.sub.2O).sub.2(tp).sub.2 and [Ni.sub.3(OH).sub.2(H.sub.2O).sub.4(tp).sub.2]·2H.sub.2O are formed when the water amount is between 5 and 40 mL. The CdS/Ni-MOF-74(15) composite has the best photocatalytic hydrogen evolution performance under visible light irradiation, and the maximum produced hydrogen amount is 3117.9 [mu]mol after 3 h, which is 12.8 times that of pure CdS nanoparticles. The composite of CdS and Ni-MOF-74 with a mixed structure exhibits better photocatalytic hydrogen production performance than the composite based on Ni-MOF-74 with a single structure. As an explanation for the superior activity, a double type II heterostructure is formed by CdS and Ni-MOF-74 with two structures. The photogenerated electrons in the conduction band (CB) of CdS spontaneously transfer to the CB of Ni-MOF-74, which is beneficial to the improvement in the separation of photogenerated carriers in hydrogen evolution.
Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and environmental friendliness. In this paper, a series of Ni-MOF-74 materials, Ni-MOF-74(X), with different morphologies and structures were synthesized by controlling the amount (X mL) of added water. Then, various CdS/Ni-MOF-74 composites were prepared by simple mechanical mixing of Ni-MOF-74(X) and CdS nanoparticles. The morphology and structures of CdS, Ni-MOF-74(X), and CdS/Ni-MOF-74(X) were analyzed by SEM, TEM, XRD, FT-IR, BET, and XPS. The optical properties of the composites were analyzed by UV–visible DRS, PL, TRPL, and photoelectrochemical experiments. The results show that Ni-MOF-74 is formed with a Ni 3 (OH) 2 (H 2 O) 2 (tp) 2 structure (tp: terephthalate) at low water amounts and with a [Ni 3 (OH) 2 (H 2 O) 4 (tp) 2 ]·2H 2 O structure when sufficient water was present to promote its formation. Mixed structures of Ni-MOF-74 containing Ni 3 (OH) 2 (H 2 O) 2 (tp) 2 and [Ni 3 (OH) 2 (H 2 O) 4 (tp) 2 ]·2H 2 O are formed when the water amount is between 5 and 40 mL. The CdS/Ni-MOF-74(15) composite has the best photocatalytic hydrogen evolution performance under visible light irradiation, and the maximum produced hydrogen amount is 3117.9 μmol after 3 h, which is 12.8 times that of pure CdS nanoparticles. The composite of CdS and Ni-MOF-74 with a mixed structure exhibits better photocatalytic hydrogen production performance than the composite based on Ni-MOF-74 with a single structure. As an explanation for the superior activity, a double type II heterostructure is formed by CdS and Ni-MOF-74 with two structures. The photogenerated electrons in the conduction band (CB) of CdS spontaneously transfer to the CB of Ni-MOF-74, which is beneficial to the improvement in the separation of photogenerated carriers in hydrogen evolution.
Audience Academic
Author Wang, Hong-xia
Wang, Jian
Li, Hao-tian
Zhang, Wang-gang
Liu, Yi-ming
Niu, Lu
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Snippet Visible light-driven hydrogen production by water splitting has attracted much attention because of its advantages of low cost, relative safety, and...
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SubjectTerms Analysis
Characterization and Evaluation of Materials
Chemical Routes to Materials
Chemistry and Materials Science
Classical Mechanics
Composite materials
Conduction bands
Crystallography and Scattering Methods
Heterostructures
Hydrogen
Hydrogen evolution
Hydrogen production
irradiation
light
Light irradiation
Materials Science
Morphology
Nanoparticles
Optical properties
Photocatalysis
Polymer Sciences
Povidone
Solid Mechanics
Water splitting
X ray photoelectron spectroscopy
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Title The construction of double type II heterostructure from CdS and Ni-MOF-74 with two structures and enhanced mechanism of photocatalytic water splitting
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