Controlled synthesis of KCu7S4/rGO nanocomposites for electrochemical energy storage
Aqueous rechargeable batteries present desired properties of considerable energy density, low-cost and high safety for large-scale energy storage systems. However, the scarcity of available negative electrode materials with high capacity and satisfying cycling life still hinders their development. H...
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| Published in | Materials & design Vol. 195; p. 108992 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2020
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Aqueous rechargeable batteries present desired properties of considerable energy density, low-cost and high safety for large-scale energy storage systems. However, the scarcity of available negative electrode materials with high capacity and satisfying cycling life still hinders their development. Here, we report a novel tunnel structured KCu7S4 negative electrode material for aqueous rechargeable batteries. The structural evolution and charge storage mechanism of the KCu7S4 is successfully studied by using ex-situ XPS and XRD. The charge storage can be attributed to the deep oxidation of Cu+ into Cu2+/Cu3+ and the good reversible reaction. The electrochemical induced irreversible phase transformation of Cu7S4 into Cu1.96S is mainly responsible for the capacity degradation of the KCu7S4 electrode. Fortunately, the optimized KCu7S4/rGO composite electrode shows good electrochemical performance and the fabricated full cell delivers good energy storage capability. These findings can broaden the horizon of negative elctrode materials and endow new opportunities for the fabrication of advanced rechargeable batteries.
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•The structural evolution and energy storage mechanism of KCu7S4 are successfully understood.•The KCu7S4/rGO composite delivers high capacity and good rate capability.•The fabricated Ni(OH)2//KCu7S4/rGO battery exhibits good energy storage capability. |
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| AbstractList | Aqueous rechargeable batteries present desired properties of considerable energy density, low-cost and high safety for large-scale energy storage systems. However, the scarcity of available negative electrode materials with high capacity and satisfying cycling life still hinders their development. Here, we report a novel tunnel structured KCu7S4 negative electrode material for aqueous rechargeable batteries. The structural evolution and charge storage mechanism of the KCu7S4 is successfully studied by using ex-situ XPS and XRD. The charge storage can be attributed to the deep oxidation of Cu+ into Cu2+/Cu3+ and the good reversible reaction. The electrochemical induced irreversible phase transformation of Cu7S4 into Cu1.96S is mainly responsible for the capacity degradation of the KCu7S4 electrode. Fortunately, the optimized KCu7S4/rGO composite electrode shows good electrochemical performance and the fabricated full cell delivers good energy storage capability. These findings can broaden the horizon of negative elctrode materials and endow new opportunities for the fabrication of advanced rechargeable batteries. Aqueous rechargeable batteries present desired properties of considerable energy density, low-cost and high safety for large-scale energy storage systems. However, the scarcity of available negative electrode materials with high capacity and satisfying cycling life still hinders their development. Here, we report a novel tunnel structured KCu7S4 negative electrode material for aqueous rechargeable batteries. The structural evolution and charge storage mechanism of the KCu7S4 is successfully studied by using ex-situ XPS and XRD. The charge storage can be attributed to the deep oxidation of Cu+ into Cu2+/Cu3+ and the good reversible reaction. The electrochemical induced irreversible phase transformation of Cu7S4 into Cu1.96S is mainly responsible for the capacity degradation of the KCu7S4 electrode. Fortunately, the optimized KCu7S4/rGO composite electrode shows good electrochemical performance and the fabricated full cell delivers good energy storage capability. These findings can broaden the horizon of negative elctrode materials and endow new opportunities for the fabrication of advanced rechargeable batteries. [Display omitted] •The structural evolution and energy storage mechanism of KCu7S4 are successfully understood.•The KCu7S4/rGO composite delivers high capacity and good rate capability.•The fabricated Ni(OH)2//KCu7S4/rGO battery exhibits good energy storage capability. |
| ArticleNumber | 108992 |
| Author | Shen, Weixia Dai, Shuge Hu, Hao Yan, Ruiqiang Zhang, Zhuangfei Zang, Jinhao Xu, Junmin |
| Author_xml | – sequence: 1 givenname: Weixia surname: Shen fullname: Shen, Weixia organization: Key Laboratory of Material Physics of Ministry of Education, School of Physics and Microelectronics, Zhengzhou University, 75 Daxue Road, Zhengzhou 450052, PR China – sequence: 2 givenname: Jinhao surname: Zang fullname: Zang, Jinhao organization: Key Laboratory of Material Physics of Ministry of Education, School of Physics and Microelectronics, Zhengzhou University, 75 Daxue Road, Zhengzhou 450052, PR China – sequence: 3 givenname: Hao surname: Hu fullname: Hu, Hao organization: School of Material Science and Engineering, Henan University of Science and Technology, Luoyang, Henan 471023, PR China – sequence: 4 givenname: Junmin surname: Xu fullname: Xu, Junmin organization: Key Laboratory of Material Physics of Ministry of Education, School of Physics and Microelectronics, Zhengzhou University, 75 Daxue Road, Zhengzhou 450052, PR China – sequence: 5 givenname: Zhuangfei surname: Zhang fullname: Zhang, Zhuangfei organization: Key Laboratory of Material Physics of Ministry of Education, School of Physics and Microelectronics, Zhengzhou University, 75 Daxue Road, Zhengzhou 450052, PR China – sequence: 6 givenname: Ruiqiang surname: Yan fullname: Yan, Ruiqiang organization: School of Pharmaceutical and Materials Engineering, Taizhou Univiersity, Taizhou 318000, Zhejiang Province, PR China – sequence: 7 givenname: Shuge surname: Dai fullname: Dai, Shuge email: shugedai@zzu.edu.cn organization: Key Laboratory of Material Physics of Ministry of Education, School of Physics and Microelectronics, Zhengzhou University, 75 Daxue Road, Zhengzhou 450052, PR China |
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| Keywords | Tunnel structure Ni/Cu batteries Energy storage mechanism KCu7S4/rGO nanocomposites |
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| Title | Controlled synthesis of KCu7S4/rGO nanocomposites for electrochemical energy storage |
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