Chitin-Based Magnesium Oxide Biocomposite for the Removal of Methyl Orange from Water

In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt...

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Published inInternational journal of environmental research and public health Vol. 20; no. 1; p. 831
Main Authors Majdoubi, Hicham, Alqadami, Ayoub Abdullah, Billah, Rachid El Kaim, Otero, Marta, Jeon, Byong-Hun, Hannache, Hassan, Tamraoui, Youssef, Khan, Moonis Ali
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 01.01.2023
MDPI
Subjects
Adsorbents
Adsorption
Aqueous solutions
Biomedical materials
Carbon
Chitin
Color removal
Composite materials
Dyes
Hydrogen-Ion Concentration
Kinetics
Magnesium
Magnesium Oxide
Membrane separation
Monomolecular films
Spectroscopy, Fourier Transform Infrared
Superconductors (materials)
Water
Water Pollutants, Chemical - analysis
United States > US
adsorption
anionic dye
regeneration
waste management
sea food waste
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Abstract In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration ( ). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity ( ) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle.
AbstractList In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration (Co). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity (qm) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle.
In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration ( C o ). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity ( q m ) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle.
In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration ( ). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity ( ) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle.
Author Majdoubi, Hicham
Billah, Rachid El Kaim
Alqadami, Ayoub Abdullah
Otero, Marta
Jeon, Byong-Hun
Hannache, Hassan
Tamraoui, Youssef
Khan, Moonis Ali
AuthorAffiliation 5 Department of Earth Resources & Environmental Engineering, Hanyang University, 222 Wangsimni-ro, Seongdong-gu, Seoul 04763, Republic of Korea
2 Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia
6 Laboratory of Engineering and Materials LIMAT, Faculty of Science Ben M’Sik, Hassan II University, Casablanca 2600, Morocco
4 Departmento de Química y Física Aplicadas, Universidad de León, Campus de Vegazana s/n, 24071 León, Spain
3 Laboratory of Coordination and Analytical Chemistry, Department of Chemistry, Faculty of Sciences, University of Chouaib Doukkali, Avenue Jabran Khalil Jabran, B.P 299, El Jadida 24000, Morocco
1 Materials Science Energy and Nanoengineering Department (MSN), Mohammed VI Polytechnic University (UM6P), Lot 660-Hay Moulay Rachid, Benguerir 43150, Morocco
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Issue 1
Keywords adsorption
anionic dye
regeneration
waste management
sea food waste
Language English
License Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
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SSID ssj0038469
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Snippet In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water...
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proquest
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pubmed
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StartPage 831
SubjectTerms Adsorbents
Adsorption
Aqueous solutions
Biomedical materials
Carbon
Chitin
Color removal
Composite materials
Dyes
Hydrogen-Ion Concentration
Kinetics
Magnesium
Magnesium Oxide
Membrane separation
Monomolecular films
Spectroscopy, Fourier Transform Infrared
Superconductors (materials)
Water
Water Pollutants, Chemical - analysis
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Title Chitin-Based Magnesium Oxide Biocomposite for the Removal of Methyl Orange from Water
URI https://www.ncbi.nlm.nih.gov/pubmed/36613153
https://www.proquest.com/docview/2761185958
https://pubmed.ncbi.nlm.nih.gov/PMC9819834
Volume 20
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