Chitin-Based Magnesium Oxide Biocomposite for the Removal of Methyl Orange from Water
In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt...
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Published in | International journal of environmental research and public health Vol. 20; no. 1; p. 831 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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01.01.2023
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Abstract | In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration (
). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity (
) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle. |
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AbstractList | In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration (Co). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity (qm) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle. In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration ( C o ). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity ( q m ) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle. In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water was developed. The CHt@MgO biocomposite was characterized by FT-IR, XRD, SEM-EDX, and TGA/DTG. Results proved the successful synthesis of CHt@MgO biocomposite. Adsorption of MO on the CHt@MgO biocomposite was optimized by varying experimental conditions such as pH, amount of adsorbent (m), contact time (t), temperature (T), and initial MO concentration ( ). The optimized parameters for MO removal by CHt@MgO biocomposite were as follows: pH, 6; m, 2 g/L; t, 120 min. Two common isotherm models (Langmuir and Freundlich) and three kinetic models (pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD)) were tested for experimental data fitting. Results showed that Langmuir and PFO were the most suitable to respectively describe equilibrium and kinetic results on the adsorption of MO adsorption on CHt@MgO biocomposite. The maximum Langmuir monolayer adsorption capacity ( ) on CHt@MgO biocomposite toward MO dye was 252 mg/g at 60 °C. The reusability tests revealed that CHt@MgO biocomposite possessed high (90.7%) removal efficiency after the fifth regeneration cycle. |
Author | Majdoubi, Hicham Billah, Rachid El Kaim Alqadami, Ayoub Abdullah Otero, Marta Jeon, Byong-Hun Hannache, Hassan Tamraoui, Youssef Khan, Moonis Ali |
AuthorAffiliation | 5 Department of Earth Resources & Environmental Engineering, Hanyang University, 222 Wangsimni-ro, Seongdong-gu, Seoul 04763, Republic of Korea 2 Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia 6 Laboratory of Engineering and Materials LIMAT, Faculty of Science Ben M’Sik, Hassan II University, Casablanca 2600, Morocco 4 Departmento de Química y Física Aplicadas, Universidad de León, Campus de Vegazana s/n, 24071 León, Spain 3 Laboratory of Coordination and Analytical Chemistry, Department of Chemistry, Faculty of Sciences, University of Chouaib Doukkali, Avenue Jabran Khalil Jabran, B.P 299, El Jadida 24000, Morocco 1 Materials Science Energy and Nanoengineering Department (MSN), Mohammed VI Polytechnic University (UM6P), Lot 660-Hay Moulay Rachid, Benguerir 43150, Morocco |
AuthorAffiliation_xml | – name: 2 Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia – name: 1 Materials Science Energy and Nanoengineering Department (MSN), Mohammed VI Polytechnic University (UM6P), Lot 660-Hay Moulay Rachid, Benguerir 43150, Morocco – name: 3 Laboratory of Coordination and Analytical Chemistry, Department of Chemistry, Faculty of Sciences, University of Chouaib Doukkali, Avenue Jabran Khalil Jabran, B.P 299, El Jadida 24000, Morocco – name: 5 Department of Earth Resources & Environmental Engineering, Hanyang University, 222 Wangsimni-ro, Seongdong-gu, Seoul 04763, Republic of Korea – name: 6 Laboratory of Engineering and Materials LIMAT, Faculty of Science Ben M’Sik, Hassan II University, Casablanca 2600, Morocco – name: 4 Departmento de Química y Física Aplicadas, Universidad de León, Campus de Vegazana s/n, 24071 León, Spain |
Author_xml | – sequence: 1 givenname: Hicham orcidid: 0000-0001-6587-5148 surname: Majdoubi fullname: Majdoubi, Hicham organization: Materials Science Energy and Nanoengineering Department (MSN), Mohammed VI Polytechnic University (UM6P), Lot 660-Hay Moulay Rachid, Benguerir 43150, Morocco – sequence: 2 givenname: Ayoub Abdullah surname: Alqadami fullname: Alqadami, Ayoub Abdullah organization: Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia – sequence: 3 givenname: Rachid El Kaim orcidid: 0000-0002-6320-0814 surname: Billah fullname: Billah, Rachid El Kaim organization: Laboratory of Coordination and Analytical Chemistry, Department of Chemistry, Faculty of Sciences, University of Chouaib Doukkali, Avenue Jabran Khalil Jabran, B.P 299, El Jadida 24000, Morocco – sequence: 4 givenname: Marta orcidid: 0000-0001-5218-0726 surname: Otero fullname: Otero, Marta organization: Departmento de Química y Física Aplicadas, Universidad de León, Campus de Vegazana s/n, 24071 León, Spain – sequence: 5 givenname: Byong-Hun orcidid: 0000-0002-5478-765X surname: Jeon fullname: Jeon, Byong-Hun organization: Department of Earth Resources & Environmental Engineering, Hanyang University, 222 Wangsimni-ro, Seongdong-gu, Seoul 04763, Republic of Korea – sequence: 6 givenname: Hassan surname: Hannache fullname: Hannache, Hassan organization: Laboratory of Engineering and Materials LIMAT, Faculty of Science Ben M'Sik, Hassan II University, Casablanca 2600, Morocco – sequence: 7 givenname: Youssef surname: Tamraoui fullname: Tamraoui, Youssef organization: Materials Science Energy and Nanoengineering Department (MSN), Mohammed VI Polytechnic University (UM6P), Lot 660-Hay Moulay Rachid, Benguerir 43150, Morocco – sequence: 8 givenname: Moonis Ali orcidid: 0000-0002-0548-8581 surname: Khan fullname: Khan, Moonis Ali organization: Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia |
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Keywords | adsorption anionic dye regeneration waste management sea food waste |
Language | English |
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Notes | These authors contributed equally to this work. |
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Snippet | In this work, a cost-effective chitin-based magnesium oxide (CHt@MgO) biocomposite with excellent anionic methyl orange (MO) dye removal efficiency from water... |
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SubjectTerms | Adsorbents Adsorption Aqueous solutions Biomedical materials Carbon Chitin Color removal Composite materials Dyes Hydrogen-Ion Concentration Kinetics Magnesium Magnesium Oxide Membrane separation Monomolecular films Spectroscopy, Fourier Transform Infrared Superconductors (materials) Water Water Pollutants, Chemical - analysis |
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Title | Chitin-Based Magnesium Oxide Biocomposite for the Removal of Methyl Orange from Water |
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