Amine-functionalised SBA-15 of tailored pore size for heavy metal adsorption
[Display omitted] ► Synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment. ► Adsorption of Pb and Cd ions from wastewater. ► Slower thermal treatment increases metal ion adsorption. ► Regeneration was achieved using HCl with little adverse effect on the material. This stu...
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Published in | Journal of colloid and interface science Vol. 369; no. 1; pp. 330 - 337 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Amsterdam
Elsevier Inc
01.03.2012
Elsevier |
Subjects | |
Online Access | Get full text |
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Abstract | [Display omitted]
► Synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment. ► Adsorption of Pb and Cd ions from wastewater. ► Slower thermal treatment increases metal ion adsorption. ► Regeneration was achieved using HCl with little adverse effect on the material.
This study examines the synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment for the adsorption of Pb and Cd ions. The aim is to produce a material that can adsorb heavy metals at both high and low concentrations. The materials were characterised by means of N2 physisorption, powder X-ray diffraction (PXRD), diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS), microanalysis and transmission electron microscopy (TEM). The surface areas ranged from 410 to 871m2g−1, and pore diameter was increased from 5.9 to 10.8nm. This method allows for maximum adsorption of metal ions at very low concentrations. Metal ion adsorption was determined using an Atomic Absorption Spectrophotometer. The effects of pH were found to play a major role in the precipitation and, therefore, adsorption of metal ions. This method proved to be efficient at adsorbing large quantities of both metals (39 and 41mgg−1 for Pb and Cd, respectively). |
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AbstractList | This study examines the synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment for the adsorption of Pb and Cd ions. The aim is to produce a material that can adsorb heavy metals at both high and low concentrations. The materials were characterised by means of N2 physisorption, powder X-ray diffraction (PXRD), diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS), microanalysis and transmission electron microscopy (TEM). The surface areas ranged from 410 to 871 m2 g-1, and pore diameter was increased from 5.9 to 10.8 nm. This method allows for maximum adsorption of metal ions at very low concentrations. Metal ion adsorption was determined using an Atomic Absorption Spectrophotometer. The effects of pH were found to play a major role in the precipitation and, therefore, adsorption of metal ions. This method proved to be efficient at adsorbing large quantities of both metals (39 and 41 mg g-1 for Pb and Cd, respectively). This study examines the synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment for the adsorption of Pb and Cd ions. The aim is to produce a material that can adsorb heavy metals at both high and low concentrations. The materials were characterised by means of N(2) physisorption, powder X-ray diffraction (PXRD), diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS), microanalysis and transmission electron microscopy (TEM). The surface areas ranged from 410 to 871 m(2)g(-1), and pore diameter was increased from 5.9 to 10.8 nm. This method allows for maximum adsorption of metal ions at very low concentrations. Metal ion adsorption was determined using an Atomic Absorption Spectrophotometer. The effects of pH were found to play a major role in the precipitation and, therefore, adsorption of metal ions. This method proved to be efficient at adsorbing large quantities of both metals (39 and 41 mg g(-1) for Pb and Cd, respectively). [Display omitted] ► Synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment. ► Adsorption of Pb and Cd ions from wastewater. ► Slower thermal treatment increases metal ion adsorption. ► Regeneration was achieved using HCl with little adverse effect on the material. This study examines the synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment for the adsorption of Pb and Cd ions. The aim is to produce a material that can adsorb heavy metals at both high and low concentrations. The materials were characterised by means of N2 physisorption, powder X-ray diffraction (PXRD), diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS), microanalysis and transmission electron microscopy (TEM). The surface areas ranged from 410 to 871m2g−1, and pore diameter was increased from 5.9 to 10.8nm. This method allows for maximum adsorption of metal ions at very low concentrations. Metal ion adsorption was determined using an Atomic Absorption Spectrophotometer. The effects of pH were found to play a major role in the precipitation and, therefore, adsorption of metal ions. This method proved to be efficient at adsorbing large quantities of both metals (39 and 41mgg−1 for Pb and Cd, respectively). |
Author | McManamon, Colm Holmes, Justin D. Burke, Aoife M. Morris, Michael A. |
Author_xml | – sequence: 1 givenname: Colm surname: McManamon fullname: McManamon, Colm organization: Department of Chemistry, Supercritical Fluid Centre and Materials Section, University College Cork, Cork, Ireland – sequence: 2 givenname: Aoife M. surname: Burke fullname: Burke, Aoife M. organization: Department of Chemistry, Supercritical Fluid Centre and Materials Section, University College Cork, Cork, Ireland – sequence: 3 givenname: Justin D. surname: Holmes fullname: Holmes, Justin D. organization: Department of Chemistry, Supercritical Fluid Centre and Materials Section, University College Cork, Cork, Ireland – sequence: 4 givenname: Michael A. surname: Morris fullname: Morris, Michael A. email: m.morris@ucc.ie organization: Department of Chemistry, Supercritical Fluid Centre and Materials Section, University College Cork, Cork, Ireland |
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Keywords | Metal ion adsorption Pore size expansion Functionalisation Heat treatment Microanalysis Metal ion Porous material X ray diffraction Physisorption Mesoporosity Powder Heavy metal Infrared spectrometry Pore size Precipitation Amine Transmission electron microscopy Synthesis Adsorption pH Surface area Reflectance |
Language | English |
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► Synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment. ► Adsorption of Pb and Cd ions from wastewater. ► Slower... This study examines the synthesis of SBA-15 with tailored pore sizes through controlled thermal treatment for the adsorption of Pb and Cd ions. The aim is to... |
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SubjectTerms | Adsorption Amines - chemistry Cadmium Cadmium - isolation & purification Chemistry Colloidal state and disperse state Exact sciences and technology Functionalisation General and physical chemistry Lead (metal) Lead - isolation & purification Low concentrations Metal ion adsorption Metal ions Pore size Pore size expansion Porosity Porous materials Silicon Dioxide - chemical synthesis Silicon Dioxide - chemistry Surface chemistry Surface physical chemistry |
Title | Amine-functionalised SBA-15 of tailored pore size for heavy metal adsorption |
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