Rapid synthesis of mesoporous ceria–zirconia solid solutions via a novel salt-assisted combustion process

Mesoporous ceria–zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant. The effects of various operating conditions such as the fuel-to-oxidant ratio and the nature and amount of added salt on the characteristics...

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Published inMaterials research bulletin Vol. 41; no. 12; pp. 2318 - 2324
Main Authors Chen, Weifan, Li, Fengsheng, Yu, Jiyi, Liu, Leili, Gao, Hailian
Format Journal Article
LanguageEnglish
Published United States Elsevier Ltd 14.12.2006
Subjects
A. Oxides
ADSORPTION
AGGLOMERATION
B. Chemical synthesis
D. Microstructure
FRACTALS
GLYCOLS
MATERIALS SCIENCE
MICROSTRUCTURE
NANOSTRUCTURES
NITRATES
OXIDES
PRECURSOR
SALTS
SPECIFIC SURFACE AREA
SYNTHESIS
TRANSMISSION ELECTRON MICROSCOPY
X-RAY DIFFRACTION
B. Chemical synthesis
D. Microstructure
A. Oxides
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Abstract Mesoporous ceria–zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant. The effects of various operating conditions such as the fuel-to-oxidant ratio and the nature and amount of added salt on the characteristics of the products were investigated by X-ray diffraction (XRD) and nitrogen adsorption analysis. Results from transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM) showed that the introduction of leachable inert inorganic salt as a hard agglomeration inhibitor into the redox mixture precursor led to the breakup of fractal nanocrystallite agglomerates and the mesoporous structure formed by the loose agglomeration of monodispersed nanoparticles, which was also confirmed by small-angle XRD and nitrogen adsorption analysis. The presence of salt was found to result in a more than 10-fold increase in the specific surface area of the products from 17.34 to 208.17 m 2/g at a given molar ratio of ethylene glycol–nitrate. A mechanism scheme was proposed to illustrate the possible formation processes and discuss the role of the salt additives.
AbstractList Mesoporous ceria–zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant. The effects of various operating conditions such as the fuel-to-oxidant ratio and the nature and amount of added salt on the characteristics of the products were investigated by X-ray diffraction (XRD) and nitrogen adsorption analysis. Results from transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM) showed that the introduction of leachable inert inorganic salt as a hard agglomeration inhibitor into the redox mixture precursor led to the breakup of fractal nanocrystallite agglomerates and the mesoporous structure formed by the loose agglomeration of monodispersed nanoparticles, which was also confirmed by small-angle XRD and nitrogen adsorption analysis. The presence of salt was found to result in a more than 10-fold increase in the specific surface area of the products from 17.34 to 208.17 m 2/g at a given molar ratio of ethylene glycol–nitrate. A mechanism scheme was proposed to illustrate the possible formation processes and discuss the role of the salt additives.
Mesoporous ceria-zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant. The effects of various operating conditions such as the fuel-to-oxidant ratio and the nature and amount of added salt on the characteristics of the products were investigated by X-ray diffraction (XRD) and nitrogen adsorption analysis. Results from transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM) showed that the introduction of leachable inert inorganic salt as a hard agglomeration inhibitor into the redox mixture precursor led to the breakup of fractal nanocrystallite agglomerates and the mesoporous structure formed by the loose agglomeration of monodispersed nanoparticles, which was also confirmed by small-angle XRD and nitrogen adsorption analysis. The presence of salt was found to result in a more than 10-fold increase in the specific surface area of the products from 17.34 to 208.17 m{sup 2}/g at a given molar ratio of ethylene glycol-nitrate. A mechanism scheme was proposed to illustrate the possible formation processes and discuss the role of the salt additives.
Author Li, Fengsheng
Yu, Jiyi
Chen, Weifan
Liu, Leili
Gao, Hailian
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BackLink https://www.osti.gov/biblio/20895206$$D View this record in Osti.gov
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  publication-title: J. Colloid Interf. Sci.
  doi: 10.1016/S0021-9797(02)00168-6
  contributor:
    fullname: Yu
– volume: 15
  start-page: 4796
  year: 1999
  ident: 10.1016/j.materresbull.2006.04.024_bib4
  publication-title: Langmuir
  doi: 10.1021/la981537h
  contributor:
    fullname: Martínez-Arias
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Snippet Mesoporous ceria–zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant....
Mesoporous ceria-zirconia solid solutions were prepared by a novel salt-assisted combustion process using ethylene glycol as a fuel and nitrate as an oxidant....
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elsevier
SourceType Open Access Repository
Aggregation Database
Publisher
StartPage 2318
SubjectTerms A. Oxides
ADSORPTION
AGGLOMERATION
B. Chemical synthesis
D. Microstructure
FRACTALS
GLYCOLS
MATERIALS SCIENCE
MICROSTRUCTURE
NANOSTRUCTURES
NITRATES
OXIDES
PRECURSOR
SALTS
SPECIFIC SURFACE AREA
SYNTHESIS
TRANSMISSION ELECTRON MICROSCOPY
X-RAY DIFFRACTION
Title Rapid synthesis of mesoporous ceria–zirconia solid solutions via a novel salt-assisted combustion process
URI https://dx.doi.org/10.1016/j.materresbull.2006.04.024
https://www.osti.gov/biblio/20895206
Volume 41
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