Recyclable thermosetting polymers for digital light processing 3D printing

3D printing of various polymers has attracted great attention and developed rapidly in recent years. Digital light processing (DLP) has recently emerged as a fast growing 3D printing technique due to its high resolution and high speed. However, the lack of printable high-performance materials limits...

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Published inMaterials & design Vol. 197; p. 109189
Main Authors Chen, Zhiqiang, Yang, Meng, Ji, Mengke, Kuang, Xiao, Qi, H. Jerry, Wang, Tiejun
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.01.2021
Elsevier
Subjects
3D printing
Bond exchange reactions (BERs)
Recycle
Reprint
Bond exchange reactions (BERs)
Reprint
3D printing
Recycle
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Abstract 3D printing of various polymers has attracted great attention and developed rapidly in recent years. Digital light processing (DLP) has recently emerged as a fast growing 3D printing technique due to its high resolution and high speed. However, the lack of printable high-performance materials limits its broad applications. In addition, with the increasing adoption of DLP 3D printing, the efficient recycling of printed thermosetting materials is highly desired. Herein, we proposed a two-stage curing approach involving dynamic reactions by using the acrylate-epoxy hybrid resin for the recyclable DLP 3D printing of high-performance thermosetting polymers. Bond exchange reactions (BERs) could establish covalent bonds between the acrylate network and the epoxy network, thus partially triggering the copolymerization. The resulting new polymers exhibited excellent mechanical properties. A small-molecule assisted BER method was then used to efficiently depolymerize the thermosetting printed parts into soluble oligomers, which were formulated with fresh photopolymers for the next round of printing. The reprinted samples still showed good mechanical properties comparable to the virgin ones. In addition, the new polymers demonstrated potential applications in 4D printing of smart actuators. This work opens a novel avenue for green manufacturing technologies. [Display omitted] •Digital light processing 3D printing of recyclable thermosetting polymers.•A two-stage curing approach involving dynamic reactions to improve performance.•Recycle printed parts by using small-molecule assisted bond exchange reactions.•Reprinted polymers exhibit comparable mechanical properties to the virgin ones.•4D printing of smart actuators by using the shape memory effect.
AbstractList 3D printing of various polymers has attracted great attention and developed rapidly in recent years. Digital light processing (DLP) has recently emerged as a fast growing 3D printing technique due to its high resolution and high speed. However, the lack of printable high-performance materials limits its broad applications. In addition, with the increasing adoption of DLP 3D printing, the efficient recycling of printed thermosetting materials is highly desired. Herein, we proposed a two-stage curing approach involving dynamic reactions by using the acrylate-epoxy hybrid resin for the recyclable DLP 3D printing of high-performance thermosetting polymers. Bond exchange reactions (BERs) could establish covalent bonds between the acrylate network and the epoxy network, thus partially triggering the copolymerization. The resulting new polymers exhibited excellent mechanical properties. A small-molecule assisted BER method was then used to efficiently depolymerize the thermosetting printed parts into soluble oligomers, which were formulated with fresh photopolymers for the next round of printing. The reprinted samples still showed good mechanical properties comparable to the virgin ones. In addition, the new polymers demonstrated potential applications in 4D printing of smart actuators. This work opens a novel avenue for green manufacturing technologies.
3D printing of various polymers has attracted great attention and developed rapidly in recent years. Digital light processing (DLP) has recently emerged as a fast growing 3D printing technique due to its high resolution and high speed. However, the lack of printable high-performance materials limits its broad applications. In addition, with the increasing adoption of DLP 3D printing, the efficient recycling of printed thermosetting materials is highly desired. Herein, we proposed a two-stage curing approach involving dynamic reactions by using the acrylate-epoxy hybrid resin for the recyclable DLP 3D printing of high-performance thermosetting polymers. Bond exchange reactions (BERs) could establish covalent bonds between the acrylate network and the epoxy network, thus partially triggering the copolymerization. The resulting new polymers exhibited excellent mechanical properties. A small-molecule assisted BER method was then used to efficiently depolymerize the thermosetting printed parts into soluble oligomers, which were formulated with fresh photopolymers for the next round of printing. The reprinted samples still showed good mechanical properties comparable to the virgin ones. In addition, the new polymers demonstrated potential applications in 4D printing of smart actuators. This work opens a novel avenue for green manufacturing technologies. [Display omitted] •Digital light processing 3D printing of recyclable thermosetting polymers.•A two-stage curing approach involving dynamic reactions to improve performance.•Recycle printed parts by using small-molecule assisted bond exchange reactions.•Reprinted polymers exhibit comparable mechanical properties to the virgin ones.•4D printing of smart actuators by using the shape memory effect.
ArticleNumber 109189
Author Yang, Meng
Qi, H. Jerry
Ji, Mengke
Wang, Tiejun
Chen, Zhiqiang
Kuang, Xiao
Author_xml – sequence: 1
  givenname: Zhiqiang
  surname: Chen
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  organization: State Key Lab for Strength and Vibration of Mechanical Structures, Department of Engineering Mechanics, Xi'an Jiaotong University, Xi'an 710049, China
– sequence: 2
  givenname: Meng
  surname: Yang
  fullname: Yang, Meng
  organization: State Key Lab for Strength and Vibration of Mechanical Structures, Department of Engineering Mechanics, Xi'an Jiaotong University, Xi'an 710049, China
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  givenname: Mengke
  surname: Ji
  fullname: Ji, Mengke
  organization: State Key Lab for Strength and Vibration of Mechanical Structures, Department of Engineering Mechanics, Xi'an Jiaotong University, Xi'an 710049, China
– sequence: 4
  givenname: Xiao
  surname: Kuang
  fullname: Kuang, Xiao
  organization: The George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA 30332, USA
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  givenname: H. Jerry
  surname: Qi
  fullname: Qi, H. Jerry
  email: qih@me.gatech.edu
  organization: The George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA 30332, USA
– sequence: 6
  givenname: Tiejun
  surname: Wang
  fullname: Wang, Tiejun
  email: wangtj@mail.xjtu.edu.cn
  organization: State Key Lab for Strength and Vibration of Mechanical Structures, Department of Engineering Mechanics, Xi'an Jiaotong University, Xi'an 710049, China
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Keywords Bond exchange reactions (BERs)
Reprint
3D printing
Recycle
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Snippet 3D printing of various polymers has attracted great attention and developed rapidly in recent years. Digital light processing (DLP) has recently emerged as a...
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SubjectTerms 3D printing
Bond exchange reactions (BERs)
Recycle
Reprint
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Title Recyclable thermosetting polymers for digital light processing 3D printing
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