Crystal structure of [4-(chloro-meth-yl)phen-yl](4-hy-droxy-piperidin-1-yl)methanone
The title compound, C13H16ClNO2, crystallized with two independent mol-ecules in the asymmetric unit (A and B). The piperidinol ring in mol-ecule B is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both mol-ecules these rings have a chair conformation, including...
Saved in:
| Published in | Acta crystallographica. Section E, Crystallographic communications Vol. 71; no. Pt 10; pp. o703 - o704 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
International Union of Crystallography
01.10.2015
|
| Subjects | |
| Online Access | Get full text |
Cover
Loading…
| Abstract | The title compound, C13H16ClNO2, crystallized with two independent mol-ecules in the asymmetric unit (A and B). The piperidinol ring in mol-ecule B is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both mol-ecules these rings have a chair conformation, including the minor component in mol-ecule B. Their mean planes are inclined to the benzene ring by 45.57 (13)° in mol-ecule A, and by 50.5 (4)° for the major component of the piperidine ring in mol-ecule B. In the crystal, the individual mol-ecules are linked by O-H⋯O hydrogen bonds, forming chains of A and B mol-ecules along the [100] direction. The chains are inter-linked by C-H⋯O hydrogen bonds, forming ribbons. |
|---|---|
| AbstractList | The title compound, C
13
H
16
ClNO
2
, crystallized with two independent molecules in the asymmetric unit (
A
and
B
). The piperidinol ring in molecule
B
is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both molecules these rings have a chair conformation, including the minor component in molecule
B
. Their mean planes are inclined to the benzene ring by 45.57 (13)° in molecule
A
, and by 50.5 (4)° for the major component of the piperidine ring in molecule
B
. In the crystal, the individual molecules are linked by O—H⋯O hydrogen bonds, forming chains of
A
and
B
molecules along the [100] direction. The chains are interlinked by C—H⋯O hydrogen bonds, forming ribbons. The title compound, C13H16ClNO2, crystallized with two independent mol-ecules in the asymmetric unit (A and B). The piperidinol ring in mol-ecule B is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both mol-ecules these rings have a chair conformation, including the minor component in mol-ecule B. Their mean planes are inclined to the benzene ring by 45.57 (13)° in mol-ecule A, and by 50.5 (4)° for the major component of the piperidine ring in mol-ecule B. In the crystal, the individual mol-ecules are linked by O-H⋯O hydrogen bonds, forming chains of A and B mol-ecules along the [100] direction. The chains are inter-linked by C-H⋯O hydrogen bonds, forming ribbons. The title compound, C13H16ClNO2, crystallized with two independent molecules in the asymmetric unit (A and B). The piperidinol ring in molecule B is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both molecules these rings have a chair conformation, including the minor component in molecule B. Their mean planes are inclined to the benzene ring by 45.57 (13)° in molecule A, and by 50.5 (4)° for the major component of the piperidine ring in molecule B. In the crystal, the individual molecules are linked by O—H...O hydrogen bonds, forming chains of A and B molecules along the [100] direction. The chains are interlinked by C—H...O hydrogen bonds, forming ribbons. The title compound, C 13 H 16 ClNO 2 , crystallized with two independent molecules in the asymmetric unit ( A and B ). The piperidinol ring in molecule B is disordered over two positions with a site occupancy ratio of 0.667 (5):0.333 (5). In both molecules these rings have a chair conformation, including the minor component in molecule B . Their mean planes are inclined to the benzene ring by 45.57 (13)° in molecule A , and by 50.5 (4)° for the major component of the piperidine ring in molecule B . In the crystal, the individual molecules are linked by O—H...O hydrogen bonds, forming chains of A and B molecules along the [100] direction. The chains are interlinked by C—H...O hydrogen bonds, forming ribbons. |
| Author | Revathi, B K Dhanalakshmi, K Usha, G Reuben Jonathan, D Kalai Sevi, K |
| Author_xml | – sequence: 1 givenname: B K surname: Revathi fullname: Revathi, B K organization: PG and Research Department of Physics, Queen Mary's College, Chennai-4, Tamilnadu, India – sequence: 2 givenname: D surname: Reuben Jonathan fullname: Reuben Jonathan, D organization: Department of Chemistry, Madras Christian College, Chennai-59, India – sequence: 3 givenname: K surname: Kalai Sevi fullname: Kalai Sevi, K organization: SCRI, Anna hospital Campus, Chennai-106, Tamilnadu, India – sequence: 4 givenname: K surname: Dhanalakshmi fullname: Dhanalakshmi, K organization: Anna Siddha Medical College, Chennai-106, Tamilnadu, India – sequence: 5 givenname: G surname: Usha fullname: Usha, G organization: PG and Research Department of Physics, Queen Mary's College, Chennai-4, Tamilnadu, India |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26594432$$D View this record in MEDLINE/PubMed |
| BookMark | eNplkUtr3DAUhUVJaNI0P6CbMsvpQo1e1mNTKEMfgUAWTVelCD2uYweP5Up2qf997U4aErK64ujc7x44r9BRn3pA6A0l7ykl6uIbI5U02hBaESqJkS_Q6SrhVTt69D5B56XcEUKoqLis2Et0wmRlhODsFN3s8lxG123KmKcwThk2qd78EHgbmi7lhPcwNnju3g0N9Mv8uRW4mXHM6c-Mh3aA3Ma2x3S1rFa3pnyNjmvXFTi_n2fo--dPN7uv-Or6y-Xu4xUOgqoRa-PA0ailryU1uuYEmCZaUVY7R7Q0lWNaSOVJkMBZ5WRkWsmgpPacR8rP0OWBG5O7s0Nu9y7PNrnW_hNSvrUuj23owC52b6LwQQsjQvQmeK-Y1KDBCx7VwvpwYA2T30MM0I_ZdU-gT3_6trG36bcVUihB1jDbe0BOvyYoo923JUDXuR7SVCxVwkhCCeOLlR6sIadSMtQPZyixa7n2WbnLztvH-R42_lfJ_wIS2KC5 |
| Cites_doi | 10.1107/S0021889892010331 10.1107/S2053229614024218 10.1097/00000539-200012000-00038 10.1107/S0108768102003324 10.1107/S2056989014026851 10.1107/S2056989015007653 10.1107/S0021889812029111 10.1021/jm980028+ 10.1016/0040-4020(95)00254-6 |
| ContentType | Journal Article |
| Copyright | Revathi et al. 2015 2015 |
| Copyright_xml | – notice: Revathi et al. 2015 2015 |
| DBID | NPM AAYXX CITATION 7X8 5PM DOA |
| DOI | 10.1107/S2056989015016096 |
| DatabaseName | PubMed CrossRef MEDLINE - Academic PubMed Central (Full Participant titles) DOAJ |
| DatabaseTitle | PubMed CrossRef MEDLINE - Academic |
| DatabaseTitleList | MEDLINE - Academic PubMed CrossRef |
| Database_xml | – sequence: 1 dbid: DOA name: DOAJ Directory of Open Access Journals url: https://www.doaj.org/ sourceTypes: Open Website – sequence: 2 dbid: NPM name: PubMed url: https://proxy.k.utb.cz/login?url=http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed sourceTypes: Index Database |
| DeliveryMethod | fulltext_linktorsrc |
| DocumentTitleAlternate | C13H16ClNO2 |
| EISSN | 2056-9890 |
| EndPage | o704 |
| ExternalDocumentID | oai_doaj_org_article_3d1b9d4bc8494cdb9cbb7268e8eb43d7 10_1107_S2056989015016096 26594432 |
| Genre | Journal Article |
| GroupedDBID | 5VS AAFWJ ADBBV ADRAZ ALMA_UNASSIGNED_HOLDINGS AOIJS BCNDV EBS EJD GROUPED_DOAJ H13 HH5 HYE IPNFZ KQ8 M48 M~E NPM OK1 PGMZT RCJ RIG ROL RPM AAYXX AFPKN CITATION 7X8 5PM |
| ID | FETCH-LOGICAL-c417t-89aea1d86bf6198f30e2808712faa08695a28467b0c6e325a6d2876c768b33d13 |
| IEDL.DBID | RPM |
| ISSN | 2056-9890 |
| IngestDate | Tue Oct 22 15:10:41 EDT 2024 Tue Sep 17 21:27:16 EDT 2024 Fri Oct 25 00:10:03 EDT 2024 Fri Aug 23 01:11:37 EDT 2024 Tue Oct 15 23:55:24 EDT 2024 |
| IsDoiOpenAccess | true |
| IsOpenAccess | true |
| IsPeerReviewed | true |
| IsScholarly | true |
| Issue | Pt 10 |
| Keywords | piperidine derivative crystal structure hydrogen bonding |
| Language | English |
| License | This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| LinkModel | DirectLink |
| MergedId | FETCHMERGED-LOGICAL-c417t-89aea1d86bf6198f30e2808712faa08695a28467b0c6e325a6d2876c768b33d13 |
| Notes | ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
| OpenAccessLink | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4647401/ |
| PMID | 26594432 |
| PQID | 1749601023 |
| PQPubID | 23479 |
| ParticipantIDs | doaj_primary_oai_doaj_org_article_3d1b9d4bc8494cdb9cbb7268e8eb43d7 pubmedcentral_primary_oai_pubmedcentral_nih_gov_4647401 proquest_miscellaneous_1749601023 crossref_primary_10_1107_S2056989015016096 pubmed_primary_26594432 |
| PublicationCentury | 2000 |
| PublicationDate | 2015-10-01 |
| PublicationDateYYYYMMDD | 2015-10-01 |
| PublicationDate_xml | – month: 10 year: 2015 text: 2015-10-01 day: 01 |
| PublicationDecade | 2010 |
| PublicationPlace | England |
| PublicationPlace_xml | – name: England |
| PublicationTitle | Acta crystallographica. Section E, Crystallographic communications |
| PublicationTitleAlternate | Acta Crystallogr E Crystallogr Commun |
| PublicationYear | 2015 |
| Publisher | International Union of Crystallography |
| Publisher_xml | – name: International Union of Crystallography |
| References | 8697062 - Obes Res. 1995 Nov;3 Suppl 4:591S-603S 12037360 - Acta Crystallogr B. 2002 Jun;58(Pt 3 Pt 1):389-97 11094008 - Anesth Analg. 2000 Dec;91(6):1499-505 25567568 - Acta Crystallogr C Struct Chem. 2015 Jan;71(Pt 1):3-8 9599245 - J Med Chem. 1998 May 21;41(11):1962-9 Revathi (bg2567_bb13) 2015; 71 Campfield (bg2567_bb6) 1995; 3 bg2567_bb7 Bruno (bg2567_bb5) 2002; 58 Prathebha (bg2567_bb12) 2015; 71 bg2567_bb9 Kozikowski (bg2567_bb11) 1998; 41 Farrugia (bg2567_bb8) 2012; 45 Sheldrick (bg2567_bb14) 2015; 71 Bräu (bg2567_bb3) 2000; 91 Bolzani (bg2567_bb2) 1995; 51 bg2567_bb4 Altomare (bg2567_bb1) 1993; 26 Gulluoglu (bg2567_bb10) 2007 |
| References_xml | – volume: 26 start-page: 343 year: 1993 ident: bg2567_bb1 publication-title: J. Appl. Cryst. doi: 10.1107/S0021889892010331 contributor: fullname: Altomare – start-page: 834 year: 2007 ident: bg2567_bb10 publication-title: J. Mol. Struct. contributor: fullname: Gulluoglu – volume: 71 start-page: 3 year: 2015 ident: bg2567_bb14 publication-title: Acta Cryst. C doi: 10.1107/S2053229614024218 contributor: fullname: Sheldrick – volume: 91 start-page: 1499 year: 2000 ident: bg2567_bb3 publication-title: Anesth. Analg. doi: 10.1097/00000539-200012000-00038 contributor: fullname: Bräu – volume: 58 start-page: 389 year: 2002 ident: bg2567_bb5 publication-title: Acta Cryst. B doi: 10.1107/S0108768102003324 contributor: fullname: Bruno – volume: 3 start-page: 591S year: 1995 ident: bg2567_bb6 publication-title: Obes. Res. Clin. Pract. contributor: fullname: Campfield – ident: bg2567_bb9 – volume: 71 start-page: o39 year: 2015 ident: bg2567_bb12 publication-title: Acta Cryst. E doi: 10.1107/S2056989014026851 contributor: fullname: Prathebha – ident: bg2567_bb7 – volume: 71 start-page: o359 year: 2015 ident: bg2567_bb13 publication-title: Acta Cryst. E doi: 10.1107/S2056989015007653 contributor: fullname: Revathi – volume: 45 start-page: 849 year: 2012 ident: bg2567_bb8 publication-title: J. Appl. Cryst. doi: 10.1107/S0021889812029111 contributor: fullname: Farrugia – ident: bg2567_bb4 – volume: 41 start-page: 1962 year: 1998 ident: bg2567_bb11 publication-title: J. Med. Chem. doi: 10.1021/jm980028+ contributor: fullname: Kozikowski – volume: 51 start-page: 5929 year: 1995 ident: bg2567_bb2 publication-title: Tetrahedron doi: 10.1016/0040-4020(95)00254-6 contributor: fullname: Bolzani |
| SSID | ssj0001453652 |
| Score | 1.9893856 |
| Snippet | The title compound, C13H16ClNO2, crystallized with two independent mol-ecules in the asymmetric unit (A and B). The piperidinol ring in mol-ecule B is... The title compound, C 13 H 16 ClNO 2 , crystallized with two independent molecules in the asymmetric unit ( A and B ). The piperidinol ring in molecule B is... The title compound, C 13 H 16 ClNO 2 , crystallized with two independent molecules in the asymmetric unit ( A and B ). The piperidinol ring in molecule B is... The title compound, C13H16ClNO2, crystallized with two independent molecules in the asymmetric unit (A and B). The piperidinol ring in molecule B is disordered... |
| SourceID | doaj pubmedcentral proquest crossref pubmed |
| SourceType | Open Website Open Access Repository Aggregation Database Index Database |
| StartPage | o703 |
| SubjectTerms | crystal structure Data Reports hydrogen bonding piperidine derivative |
| SummonAdditionalLinks | – databaseName: DOAJ dbid: DOA link: http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwrV1Ni9swEBUlp15KS7_cbosLPaQFEVkay9KxDV1CD-2hXVhYitFIMgkEZ9mPQ_59Z-xkSbaFXnqVhD3MDMx71viNEO87r2NyrpIx10pCVkn6GlDalJRBizF0Q5fvN7s4g6_n9fnBqC_uCRvlgUfHzUyq0CfA6MBDTOgjYqOtyy4jmDT-R678AZkavq5AbewwbkdThZfe-f2VJtGd2Q9e5DVCQ5VVLNh_UJQG7f6_Ac77fZMHhej0sXi0Q5Dlp9HyJ-JB7p-K7_OrLeG8dTnqwd5e5XLTlRcgp3FJjHzDg6K36w_c0LVd_5qCXG4TN7BcrljpmOoXcTza52Oh3_T5mTg7_fJzvpC7WQkyQtXcSOdDDlVyFjuiRK4zKmuniA3pLgSiLb4OmqEGqmiz0XWwibiSjcQ20JCPzXMx4ce_FGXj0SW-gDHZAxIecGA6NBgjE2nrCvFx76z2cpTEaAcqoZr2D88W4jO78-4gq1kPCxTjdhfj9l8xLsS7fTBayn6-0gh93txet8SnPFNKbQrxYgzO3au0rT2A0YVojsJ2ZMvxTr9aDgrbYIEnFb76H8a_Fg8JZNVjA-CJmFAa5DcEZG7w7ZCzvwFHKO-L priority: 102 providerName: Directory of Open Access Journals – databaseName: Scholars Portal Journals: Open Access dbid: M48 link: http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwrV3PaxUxEA61vXgRxVbXH2WFHqoQ3U2y2eQgUoul9KAH-6AgsmSSrK_w2K2vLbj_vTPZfcWn7-h185NJwnzfzscMYwetFT4YU3Ifq4KrWARuKwVch1BI0OBdm1S-n_XpTJ1dVBdbbFXeajLg9UZqR_WkZsvF218_hw_44N-PIvb63VeBXtyaRN5LjZj8HtsRlJeLlHwT2k-_XFQldarBQwM4jZjinBtnWfNUKaH_JhT6t5jyD-908pA9mGBlfjTeg0dsK3aP2Zfj5YDgb5GPSWJvlzHv2_yb4od-jjS9p-rRw-I1qbyGxfdDxedDIFXL1SWlP0anhsQP26mb6_ou7rLZyafz41M-FVDgXpX1DTfWRVcGo6FFnmRaWURhCqRIonUOuYytnCD8AYXXUYrK6YAESnukICBlKOUe26bpn7K8tmACRWVktAoQJBglW5DgPbFrbTL2ZmWs5mrMk9EkflHUzT-WzdhHMuddR0pxnT70yx_N9GIaXB9sUOCNssoHsB6gFtpEE0HJUGfs1eowGnwSFOdwXexvrxskWZZ4ppAZezIezt1SQldWKSkyVq8d29pe1lu6y3lKu620ovKFz_7H5p-z-4i8qlEV-IJt4zWILxHd3MB-urO_AZCa9lQ priority: 102 providerName: Scholars Portal |
| Title | Crystal structure of [4-(chloro-meth-yl)phen-yl](4-hy-droxy-piperidin-1-yl)methanone |
| URI | https://www.ncbi.nlm.nih.gov/pubmed/26594432 https://search.proquest.com/docview/1749601023 https://pubmed.ncbi.nlm.nih.gov/PMC4647401 https://doaj.org/article/3d1b9d4bc8494cdb9cbb7268e8eb43d7 |
| Volume | 71 |
| hasFullText | 1 |
| inHoldings | 1 |
| isFullTextHit | |
| isPrint | |
| link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV1da9RAFB3aPvkiil-xWiL4UIXpJvOVmUddLEWoCFqoiIS5MxN3YZssa_uwP2r_xP4y70yS0lWffAkhmWTC3BvuOZmTM4S8bgxzXuuSuiALKkLhqZECqPK-4KDA2SapfD-pswvx8VJe7hE5_guTRPsO5ift4uqknc-StnJ55SajTmzy-XwqlIgLyU32yT4m6B2Knj6sCMmVZMMMJrKbyReGVd7oRO5LhZg9OgAraYTgbKccJdf-f0HNPxWTd0rQ6QNyf8CO-bv-GR-SvdA-It-mqzUivEXeO8HerELeNfl3QY_dDLl4t93ERaK3m_XiTZRzxZ0fx4LO1tuNjxKW7WY5j27HWMOQ52Gr2Ny2XRsek4vTD1-nZ3RYL4E6UVbXVBsbbOm1ggZpkW54EZgukBGxxlqkLkZaFuEGFE4FzqRVHvmScsg4gHNf8ifkIN7-GckrA9rHSRgejADEBFrwBjg4F8m00hl5Ow5bvextMepEJ4qq_mu4M_I-Duxtw-honQ50q5_1ENca-wfjBTgtjHAejAOomNJBBxDcVxl5NYalxjcgTmvYNnQ3v2rkVCbSSsYz8rQP021XY5gzUu0EcOdZds9g0iWX7SHJnv_3lYfkHqIr2Sv_XpADzILwEhHMNRwl5o_bc6GPUvb-Bv9l9cI |
| link.rule.ids | 230,315,730,783,787,867,888,2109,2228,24332,27938,27939,53806,53808 |
| linkProvider | National Library of Medicine |
| linkToHtml | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV3LjtMwFL0ahgVseIhXeBaJxYCUNvEr9hIqRgVmRkjMoEEIRfEjtKKTVKVdlH_qT_TLuHaS0XRgA7sodmIn19Y9Jz45BnhRKmKslGlsHE9i5hIbK850LKxNqBbaFGVQ-R6J0Ql7f8pPd4B3_8IE0b7Rk341PetXk3HQVs7OzKDTiQ0-Hg6ZYH4jucEVuIrzNREXSHr4tMI4FZy0a5jIbwafCOZ5JQO9TwWidu8BLLhijJKthBR8-_8GNi9rJi8kof2b8LnrfqM9-dFfLnTf_Lrk7PjPz3cLbrSwtPe6Kb4NO666A1-G8xWCx2mvMZldzl2vLntfWbxnxkjz683a7z-9Wa-mL71SzB9822PxeLVZW9_DzXo28UbKmB6RQmItX72o6srdhZP9t8fDUdxuxRAblmaLWKrCFamVQpfIuGRJE0dkgmSLlEWBrEjxgngkoxMjHCW8EBapmDBIZjSlNqX3YNff_gH0MqWl9es71CmmEW5IRktNtTGepwsZwasuHvmscdzIA1NJsvyPOEbwxkfsvKI3yw4n6vn3vH2lObavlWXaSKaYsVoZrTMipJNOM2qzCJ538c5xcvkVk6Jy9fJnjnRNecZKaAT3m_ifN9WNnwiyrZGx1ZftEox3MPBu4_vwv698BtdGx4cH-cG7ow-P4DqCON4IDB_DLo4I9wSB0kI_DdPiN8VBFfQ |
| linkToPdf | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV3bjtMwELVgkRAvXMQtXIPEw4KUJrEdx36EQrXcVivBSgsIRRnboRXdpCrtQ_mn_kS_jLGTrNqFp32Lkkl8mbE8Jz46Q8jzSlFtpEwjbbMk4jYxkco4RMKYhIEAXVae5XsoDo75-5PsZKvUlyfta5gM6unpoJ6MPbdydqrjnicWH30acsFdIbl4Zqr4MrmCazaRW0Dd_17hGRMZ7c4xEePEnynu9Up6iJ8KzNydDrDIFOeM7mxKXrv_fwnned7k1kY0ukG-9UNo-Se_BssFDPSfc-qOFxrjTXK9S0_DV63JLXLJ1rfJ1-F8hUnkNGzFZpdzGzZV-J1H-3qMcL_ZrF0d6s16NX3hGGPu4sc-j8arzdq4Xm7Ws4kTVMZtEqEkWjnzsm5qe4ccj95-GR5EXUmGSPM0X0RSlbZMjRRQIfKSFUssxcnPU1qVJaIjlZXUZTSQaGEZzUphEJIJjaAGGDMpu0v23OfvkzBXII0752FWccC0Q3JWAQOtHV4XMiAve58Us1Z5o_CIJcmLf3wZkNfOa2eGTjTb32jmP4tuWgtsH5ThoCVXXBtQGiCnQlppgTOTB-RZ7_MCF5k7OSlr2yx_FwjblEOulAXkXhsDZ031MRSQfCc6dvqy-wR97oW8Ox8_uPCbT8nVozej4uO7ww8PyTXM5bKWZ_iI7GFA2MeYLy3giV8ZfwFheRh0 |
| openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Crystal+structure+of+%5B4-%28chloromethyl%29phenyl%5D%284-hydroxypiperidin-1-yl%29methanone&rft.jtitle=Acta+crystallographica.+Section+E%2C+Crystallographic+communications&rft.au=B.+K.+Revathi&rft.au=D.+Reuben+Jonathan&rft.au=K.+Kalai+Sevi&rft.au=K.+Dhanalakshmi&rft.date=2015-10-01&rft.pub=International+Union+of+Crystallography&rft.issn=2056-9890&rft.eissn=2056-9890&rft.volume=71&rft.issue=10&rft.spage=o703&rft.epage=o704&rft_id=info:doi/10.1107%2FS2056989015016096&rft.externalDBID=DOA&rft.externalDocID=oai_doaj_org_article_3d1b9d4bc8494cdb9cbb7268e8eb43d7 |
| thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=2056-9890&client=summon |
| thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=2056-9890&client=summon |
| thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=2056-9890&client=summon |