Feasibility studies of discontinuous electro-regeneration processes in environmentally-friendly plating for chromate separation from a binary system

Project work was carried out for feasibility and possible design of semi-industrial electro-regeneration units for diluted waters typical for rinse water systems in electroplating industry. Firstly, one subject of interest was the removal of CrO 4 2− ions in the concentration range between 0.06 mol...

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Published inElectrochimica acta Vol. 54; no. 9; pp. 2417 - 2424
Main Authors Bergmann, M.E. Henry, Iourtchouk, Tatiana, Rittel, Andreas, Zuleeg, Heike
Format Journal Article Conference Proceeding
LanguageEnglish
Published Kidlington Elsevier Ltd 30.03.2009
Elsevier
Subjects
Chemistry
Chromium removal
Electrochemistry
Electrodeionization
Electrodeposition
Electrodialysis
Exact sciences and technology
General and physical chemistry
Ion exchange
Miscellaneous (electroosmosis, electrophoresis, electrochromism, electrocrystallization, ...)
Rinse waters
Study of interfaces
Chromium removal
Electrodeionization
Ion exchange
Electrodialysis
Rinse waters
Water
Removal
Discontinuous
Separation
Binary system
Rinsing
Wasteless technology
Chromates
Regeneration
Inorganic anion
Chromium VI Compounds
Electrodeposition
Adsorbent
Electrochemical reaction
Ion exchange resin
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Abstract Project work was carried out for feasibility and possible design of semi-industrial electro-regeneration units for diluted waters typical for rinse water systems in electroplating industry. Firstly, one subject of interest was the removal of CrO 4 2− ions in the concentration range between 0.06 mol m −3 and 2.3 mol m −3. Ion exchange capacity of several resins under room temperature conditions was tested. A 2-compartment cell with diaphragm was found to be a suitable construction for electrochemical resin regeneration after previous discontinuous loading. The determination of resin conductivities and transport numbers was also part of the studies. Results showed sufficient high current efficiencies up to 70%. Nevertheless, low ion mobility in the resin may limit the removal rate for continuous electrodeionization. In this case, stepwise operation mode in loading and regenerating the resin bed is the only solution. Energy consumption can be lowered by using catholytes of previous electro-regeneration steps. Specific energy consumption until 0.3 kWh per treated cubic meter is to be expected.
AbstractList Project work was carried out for feasibility and possible design of semi-industrial electro-regeneration units for diluted waters typical for rinse water systems in electroplating industry. Firstly, one subject of interest was the removal of CrO42- ions in the concentration range between 0.06 mol m-3 and 2.3 mol m-3. Ion exchange capacity of several resins under room temperature conditions was tested. A 2-compartment cell with diaphragm was found to be a suitable construction for electrochemical resin regeneration after previous discontinuous loading. The determination of resin conductivities and transport numbers was also part of the studies. Results showed sufficient high current efficiencies up to 70%. Nevertheless, low ion mobility in the resin may limit the removal rate for continuous electrodeionization. In this case, stepwise operation mode in loading and regenerating the resin bed is the only solution. Energy consumption can be lowered by using catholytes of previous electro-regeneration steps. Specific energy consumption until 0.3 kWh per treated cubic meter is to be expected.
Project work was carried out for feasibility and possible design of semi-industrial electro-regeneration units for diluted waters typical for rinse water systems in electroplating industry. Firstly, one subject of interest was the removal of CrO 4 2− ions in the concentration range between 0.06 mol m −3 and 2.3 mol m −3. Ion exchange capacity of several resins under room temperature conditions was tested. A 2-compartment cell with diaphragm was found to be a suitable construction for electrochemical resin regeneration after previous discontinuous loading. The determination of resin conductivities and transport numbers was also part of the studies. Results showed sufficient high current efficiencies up to 70%. Nevertheless, low ion mobility in the resin may limit the removal rate for continuous electrodeionization. In this case, stepwise operation mode in loading and regenerating the resin bed is the only solution. Energy consumption can be lowered by using catholytes of previous electro-regeneration steps. Specific energy consumption until 0.3 kWh per treated cubic meter is to be expected.
Author Bergmann, M.E. Henry
Iourtchouk, Tatiana
Zuleeg, Heike
Rittel, Andreas
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Issue 9
Keywords Chromium removal
Electrodeionization
Ion exchange
Electrodialysis
Rinse waters
Water
Removal
Discontinuous
Separation
Binary system
Rinsing
Wasteless technology
Chromates
Regeneration
Inorganic anion
Chromium VI Compounds
Electrodeposition
Adsorbent
Electrochemical reaction
Ion exchange resin
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Snippet Project work was carried out for feasibility and possible design of semi-industrial electro-regeneration units for diluted waters typical for rinse water...
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SubjectTerms Chemistry
Chromium removal
Electrochemistry
Electrodeionization
Electrodeposition
Electrodialysis
Exact sciences and technology
General and physical chemistry
Ion exchange
Miscellaneous (electroosmosis, electrophoresis, electrochromism, electrocrystallization, ...)
Rinse waters
Study of interfaces
Title Feasibility studies of discontinuous electro-regeneration processes in environmentally-friendly plating for chromate separation from a binary system
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