Sonochemical synthesis of silver nanoparticles anchored reduced graphene oxide nanosheets for selective and sensitive detection of glutathione
•Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electro...
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Published in | Ultrasonics sonochemistry Vol. 39; pp. 363 - 373 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.11.2017
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Abstract | •Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electrocatalytic activity towards the oxidation of glutathione.•The AgNPs(TMSPED)-rGO/GC exhibits low oxidation potential (0.14V) and detection limit (0.1µM) for glutathione sensor.•The AgNPs(TMSPED)-rGO/GC to be an effective sensor for direct determination of glutathione real samples.
Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries. |
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AbstractList | Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs
-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO
in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs
, pristine rGO
and as prepared AgNPs
-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs
-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries. •Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electrocatalytic activity towards the oxidation of glutathione.•The AgNPs(TMSPED)-rGO/GC exhibits low oxidation potential (0.14V) and detection limit (0.1µM) for glutathione sensor.•The AgNPs(TMSPED)-rGO/GC to be an effective sensor for direct determination of glutathione real samples. Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries. Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries. |
Author | Anandan, Sambandam Asiri, Abdullah M. Wu, Jerry J. Vinoth, Victor |
Author_xml | – sequence: 1 givenname: Victor surname: Vinoth fullname: Vinoth, Victor organization: Nanomaterials and Solar Energy Conversion Lab, Department of Chemistry, National Institute of Technology, Tiruchirappalli 620 015, India – sequence: 2 givenname: Jerry J. surname: Wu fullname: Wu, Jerry J. email: jjwu@fcu.edu.tw organization: Department of Environmental Engineering and Science, Feng Chia University, Taichung 407, Taiwan – sequence: 3 givenname: Abdullah M. surname: Asiri fullname: Asiri, Abdullah M. organization: The Center of Excellence for Advanced Materials Research, King Abdulaziz University, Jeddah 21413, P.O. Box 80203, Saudi Arabia – sequence: 4 givenname: Sambandam surname: Anandan fullname: Anandan, Sambandam email: sanand@nitt.edu organization: Nanomaterials and Solar Energy Conversion Lab, Department of Chemistry, National Institute of Technology, Tiruchirappalli 620 015, India |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28732957$$D View this record in MEDLINE/PubMed |
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Keywords | Cyclic voltammetry Amperometric measurement AgNPs(TMSPED)-rGO nanosheets Transmission electron microscopy Glutathione AgNPs((TMSPED))-rGO nanosheets |
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Commun. doi: 10.1016/S1388-2481(01)00213-2 contributor: fullname: Ozeoemena |
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Snippet | •Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization... Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs -rGO) nanosheets via... Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets... |
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SubjectTerms | AgNPs(TMSPED)-rGO nanosheets Amperometric measurement Cyclic voltammetry Glutathione Transmission electron microscopy |
Title | Sonochemical synthesis of silver nanoparticles anchored reduced graphene oxide nanosheets for selective and sensitive detection of glutathione |
URI | https://dx.doi.org/10.1016/j.ultsonch.2017.04.035 https://www.ncbi.nlm.nih.gov/pubmed/28732957 https://search.proquest.com/docview/1922508725 |
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