Sonochemical synthesis of silver nanoparticles anchored reduced graphene oxide nanosheets for selective and sensitive detection of glutathione

•Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electro...

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Published inUltrasonics sonochemistry Vol. 39; pp. 363 - 373
Main Authors Vinoth, Victor, Wu, Jerry J., Asiri, Abdullah M., Anandan, Sambandam
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 01.11.2017
Subjects
AgNPs(TMSPED)-rGO nanosheets
Amperometric measurement
Cyclic voltammetry
Glutathione
Transmission electron microscopy
Cyclic voltammetry
Amperometric measurement
AgNPs(TMSPED)-rGO nanosheets
Transmission electron microscopy
Glutathione
AgNPs((TMSPED))-rGO nanosheets
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Abstract •Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electrocatalytic activity towards the oxidation of glutathione.•The AgNPs(TMSPED)-rGO/GC exhibits low oxidation potential (0.14V) and detection limit (0.1µM) for glutathione sensor.•The AgNPs(TMSPED)-rGO/GC to be an effective sensor for direct determination of glutathione real samples. Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries.
AbstractList Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs -rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs , pristine rGO and as prepared AgNPs -rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs -rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries.
•Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization results in AgNPs interlinked with rGO nanosheets through N-[3-trimethoxysilyl)propyl] ethylenediamine.•The AgNPs(TMSPED)-rGO/GC show high electrocatalytic activity towards the oxidation of glutathione.•The AgNPs(TMSPED)-rGO/GC exhibits low oxidation potential (0.14V) and detection limit (0.1µM) for glutathione sensor.•The AgNPs(TMSPED)-rGO/GC to be an effective sensor for direct determination of glutathione real samples. Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries.
Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets via sonochemical irradiation method, using an aqueous solution mixture of GO and AgNO3 in the presence of N-[3(trimethoxysilyl)propyl] ethylenediamine (TMSPED) without any reducing agent. As synthesized decorated nanosheets was thoroughly characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) spectroscopy, Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). Pristine AgNPs(TMSPED), pristine rGO(TMSPED) and as prepared AgNPs(TMSPED)-rGO materials were employed to modify the glassy carbon (GC) electrode and demonstrated its excellent electrocatalytic activities towards glutathione (GSH). Voltammetry and amperometry measurements were utilized to assess the electrochemical properties towards the glutathione detection. When the Ag nanoparticles were anchored onto the rGO surface, the observed results illustrated that the electrocatalytic properties of rGO might be enhanced. The resulting sensor exhibits excellent repeatability and long-term stability. Furthermore, AgNPs(TMSPED)-rGO/GC electrode able to be employed for the selective determination of GSH in amperometric analysis in the presence of ascorbic acid (AA), dopamine (DA), uric acid (UA) and glucose. Finally, this modified electrode was effectively applied to determine glutathione in real samples with good recoveries.
Author Anandan, Sambandam
Asiri, Abdullah M.
Wu, Jerry J.
Vinoth, Victor
Author_xml – sequence: 1
  givenname: Victor
  surname: Vinoth
  fullname: Vinoth, Victor
  organization: Nanomaterials and Solar Energy Conversion Lab, Department of Chemistry, National Institute of Technology, Tiruchirappalli 620 015, India
– sequence: 2
  givenname: Jerry J.
  surname: Wu
  fullname: Wu, Jerry J.
  email: jjwu@fcu.edu.tw
  organization: Department of Environmental Engineering and Science, Feng Chia University, Taichung 407, Taiwan
– sequence: 3
  givenname: Abdullah M.
  surname: Asiri
  fullname: Asiri, Abdullah M.
  organization: The Center of Excellence for Advanced Materials Research, King Abdulaziz University, Jeddah 21413, P.O. Box 80203, Saudi Arabia
– sequence: 4
  givenname: Sambandam
  surname: Anandan
  fullname: Anandan, Sambandam
  email: sanand@nitt.edu
  organization: Nanomaterials and Solar Energy Conversion Lab, Department of Chemistry, National Institute of Technology, Tiruchirappalli 620 015, India
BackLink https://www.ncbi.nlm.nih.gov/pubmed/28732957$$D View this record in MEDLINE/PubMed
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Keywords Cyclic voltammetry
Amperometric measurement
AgNPs(TMSPED)-rGO nanosheets
Transmission electron microscopy
Glutathione
AgNPs((TMSPED))-rGO nanosheets
Language English
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Snippet •Through sonochemical method, silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets were prepared.•Detailed characterization...
Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs -rGO) nanosheets via...
Developed here an eco-friendly, one-pot approach toward rapid synthesis of silver nanoparticles anchored reduced graphene oxide (AgNPs(TMSPED)-rGO) nanosheets...
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StartPage 363
SubjectTerms AgNPs(TMSPED)-rGO nanosheets
Amperometric measurement
Cyclic voltammetry
Glutathione
Transmission electron microscopy
Title Sonochemical synthesis of silver nanoparticles anchored reduced graphene oxide nanosheets for selective and sensitive detection of glutathione
URI https://dx.doi.org/10.1016/j.ultsonch.2017.04.035
https://www.ncbi.nlm.nih.gov/pubmed/28732957
https://search.proquest.com/docview/1922508725
Volume 39
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