Nitrogen-doped carbon quantum dots: Facile synthesis and application as a “turn-off” fluorescent probe for detection of Hg2+ ions

A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5±1.0nm and exhibit excitation wavelength-depende...

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Published in	Biosensors & bioelectronics Vol. 55; pp. 83 - 90
Main Authors	Zhang, Ruizhong, Chen, Wei
Format	Journal Article
Language	English
Published	Kidlington Elsevier B.V 15.05.2014 Elsevier
Subjects	Biological and medical sciences biosensors Biotechnology Carbon Carbon - chemistry detection limit Fluorescence fluorescent dyes Fluorescent Dyes - analysis Fluorescent Dyes - chemical synthesis Folic acid Fundamental and applied biological sciences. Psychology Ions - analysis Ions - chemistry lakes Mercury Mercury - analysis Mercury - chemistry metal ions Molecular Probe Techniques monitoring nitrogen Nitrogen - chemistry Quantum Dots Sensor Spectrometry, Fluorescence - methods tap water Water Pollutants, Chemical - analysis Fluorescence Quantum dots Carbon Mercury Folic acid Sensor Quantum dot Nanoparticle Nitrogen Probe Detector Detection Application
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Abstract	A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5±1.0nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470nm, respectively. Furthermore, due to the effective quenching effect of Hg2+ ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg2+ ions with a detection limit of 0.23μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg2+ even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg2+ ions sensor can be successfully applied to the determination of Hg2+ in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg2+ in environmental application. [Display omitted] •N-doped carbon quantum dots (N-CQDs) are synthesized by using folic acid as carbon and nitrogen sources.•The N-CQDs with average size of 4.5±1.0nm exhibit excitation wavelength-dependent fluorescence.•The N-CQDs can serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg2+ ions.•The N-CQDs-based Hg2+ ions sensor can be applied to real lake water samples with excellent sensitivity and selectivity.
AbstractList	A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5 ± 1.0 nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470 nm, respectively. Furthermore, due to the effective quenching effect of Hg(2+) ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg(2+) ions with a detection limit of 0.23 μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg(2+) even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg(2+) ions sensor can be successfully applied to the determination of Hg(2+) in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg(2+) in environmental application.A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5 ± 1.0 nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470 nm, respectively. Furthermore, due to the effective quenching effect of Hg(2+) ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg(2+) ions with a detection limit of 0.23 μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg(2+) even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg(2+) ions sensor can be successfully applied to the determination of Hg(2+) in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg(2+) in environmental application. A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5±1.0nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470nm, respectively. Furthermore, due to the effective quenching effect of Hg2+ ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg2+ ions with a detection limit of 0.23μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg2+ even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg2+ ions sensor can be successfully applied to the determination of Hg2+ in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg2+ in environmental application. A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5±1.0nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470nm, respectively. Furthermore, due to the effective quenching effect of Hg2+ ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg2+ ions with a detection limit of 0.23μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg2+ even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg2+ ions sensor can be successfully applied to the determination of Hg2+ in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg2+ in environmental application. [Display omitted] •N-doped carbon quantum dots (N-CQDs) are synthesized by using folic acid as carbon and nitrogen sources.•The N-CQDs with average size of 4.5±1.0nm exhibit excitation wavelength-dependent fluorescence.•The N-CQDs can serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg2+ ions.•The N-CQDs-based Hg2+ ions sensor can be applied to real lake water samples with excellent sensitivity and selectivity. A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic acid as both carbon and nitrogen sources. The as-prepared N-CQDs have an average size of 4.5 ± 1.0 nm and exhibit excitation wavelength-dependent fluorescence with the maximum emission and excitation at 390 and 470 nm, respectively. Furthermore, due to the effective quenching effect of Hg(2+) ions, such N-CQDs are found to serve as an effective fluorescent sensing platform for lable-free sensitive detection of Hg(2+) ions with a detection limit of 0.23 μM. The selectivity experiments reveal that the fluorescent sensor is specific for Hg(2+) even with interference by high concentrations of other metal ions. Most importantly, the N-CQDs-based Hg(2+) ions sensor can be successfully applied to the determination of Hg(2+) in tap water and real lake water samples. With excellent sensitivity and selectivity, such stable and cheap carbon materials are potentially suitable for monitoring of Hg(2+) in environmental application.
Author	Chen, Wei Zhang, Ruizhong
Author_xml	– sequence: 1 givenname: Ruizhong surname: Zhang fullname: Zhang, Ruizhong organization: State Key Laboratory of Electroanalytical Chemistry, Changchun institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, Jilin, China – sequence: 2 givenname: Wei surname: Chen fullname: Chen, Wei email: weichen@ciac.ac.cn organization: State Key Laboratory of Electroanalytical Chemistry, Changchun institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, Jilin, China
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Snippet	A facile, economical and straightforward hydrothermal strategy is used to prepare highly luminescent nitrogen-doped carbon quantum dots (N-CQDs) by using folic...
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SubjectTerms	Biological and medical sciences biosensors Biotechnology Carbon Carbon - chemistry detection limit Fluorescence fluorescent dyes Fluorescent Dyes - analysis Fluorescent Dyes - chemical synthesis Folic acid Fundamental and applied biological sciences. Psychology Ions - analysis Ions - chemistry lakes Mercury Mercury - analysis Mercury - chemistry metal ions Molecular Probe Techniques monitoring nitrogen Nitrogen - chemistry Quantum Dots Sensor Spectrometry, Fluorescence - methods tap water Water Pollutants, Chemical - analysis
Title	Nitrogen-doped carbon quantum dots: Facile synthesis and application as a “turn-off” fluorescent probe for detection of Hg2+ ions
URI	https://dx.doi.org/10.1016/j.bios.2013.11.074 https://www.ncbi.nlm.nih.gov/pubmed/24365697 https://www.proquest.com/docview/1499140971 https://www.proquest.com/docview/2000131092
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