Rheological and Electrical Study of a Composite Material Based on an Epoxy Polymer Containing Cyclotriphosphazene

In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin Diglycidyl Ether of Bisphenol A (DGEBA) reinforced with hexaglycidyl cyclotriphosphazene (HGCP). The epoxy system was cured with 4,4’-methyle...

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Published inPolymers Vol. 12; no. 4; p. 921
Main Authors Dagdag, O., El Gouri, M., El Mansouri, A., Outzourhit, A., El Harfi, A., Cherkaoui, O., El Bachiri, A., Hamed, O., Jodeh, S., Hanbali, G., Khalaf, B.
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 16.04.2020
MDPI
Subjects
Bisphenol A
Composite materials
Curing
Electrical properties
Epoxy resins
Frequency variation
Mars
Mathematical analysis
Mechanical properties
Methylene dianiline
Modulus of elasticity
Morphology
Nanoparticles
Physical properties
Polymer matrix composites
Polymers
Rheological properties
Rheology
Room temperature
Viscoelasticity
United States > US
rheological and electrical behavior
epoxy resin
HGCP
composite
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Abstract In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin Diglycidyl Ether of Bisphenol A (DGEBA) reinforced with hexaglycidyl cyclotriphosphazene (HGCP). The epoxy system was cured with 4,4’-methylene dianiline (MDA). DGEBA-HGCP-MDA epoxy composite materials with reinforced HGCP which varied from 5% to 10% by weight were prepared by mixing in the molten state. The morphology was evaluated by SEM. The rheological behavior was studied using small deformation rheology. The electrical characterization was carried out with a frequency variation range from 1 Hz to 100 KHz at room temperature. These measurements revealed that the rheological and electrical behaviors strongly depend on the quantity of HGCP in the DGEBA matrix. The linear viscoelastic properties study reveals that the modulus of elasticity G’ is dependent on the amount of HGCP present in the epoxy resin DGEBA. The capacitance-frequency measurements suggest a distribution of localized states in the band gap of the blends.
AbstractList In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin Diglycidyl Ether of Bisphenol A (DGEBA) reinforced with hexaglycidyl cyclotriphosphazene (HGCP). The epoxy system was cured with 4,4'-methylene dianiline (MDA). DGEBA-HGCP-MDA epoxy composite materials with reinforced HGCP which varied from 5% to 10% by weight were prepared by mixing in the molten state. The morphology was evaluated by SEM. The rheological behavior was studied using small deformation rheology. The electrical characterization was carried out with a frequency variation range from 1 Hz to 100 KHz at room temperature. These measurements revealed that the rheological and electrical behaviors strongly depend on the quantity of HGCP in the DGEBA matrix. The linear viscoelastic properties study reveals that the modulus of elasticity G' is dependent on the amount of HGCP present in the epoxy resin DGEBA. The capacitance-frequency measurements suggest a distribution of localized states in the band gap of the blends.
In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin Diglycidyl Ether of Bisphenol A (DGEBA) reinforced with hexaglycidyl cyclotriphosphazene (HGCP). The epoxy system was cured with 4,4'-methylene dianiline (MDA). DGEBA-HGCP-MDA epoxy composite materials with reinforced HGCP which varied from 5% to 10% by weight were prepared by mixing in the molten state. The morphology was evaluated by SEM. The rheological behavior was studied using small deformation rheology. The electrical characterization was carried out with a frequency variation range from 1 Hz to 100 KHz at room temperature. These measurements revealed that the rheological and electrical behaviors strongly depend on the quantity of HGCP in the DGEBA matrix. The linear viscoelastic properties study reveals that the modulus of elasticity G' is dependent on the amount of HGCP present in the epoxy resin DGEBA. The capacitance-frequency measurements suggest a distribution of localized states in the band gap of the blends.In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin Diglycidyl Ether of Bisphenol A (DGEBA) reinforced with hexaglycidyl cyclotriphosphazene (HGCP). The epoxy system was cured with 4,4'-methylene dianiline (MDA). DGEBA-HGCP-MDA epoxy composite materials with reinforced HGCP which varied from 5% to 10% by weight were prepared by mixing in the molten state. The morphology was evaluated by SEM. The rheological behavior was studied using small deformation rheology. The electrical characterization was carried out with a frequency variation range from 1 Hz to 100 KHz at room temperature. These measurements revealed that the rheological and electrical behaviors strongly depend on the quantity of HGCP in the DGEBA matrix. The linear viscoelastic properties study reveals that the modulus of elasticity G' is dependent on the amount of HGCP present in the epoxy resin DGEBA. The capacitance-frequency measurements suggest a distribution of localized states in the band gap of the blends.
Author Jodeh, S.
Hamed, O.
Khalaf, B.
Outzourhit, A.
El Bachiri, A.
El Gouri, M.
Cherkaoui, O.
El Mansouri, A.
Hanbali, G.
El Harfi, A.
Dagdag, O.
AuthorAffiliation 2 LPSCM, Department of physics, Faculty of Sciences Semlalia, Cadi Ayyad University, Marrakech PB 2390, Morocco; a.elmansouri@ucam.ac.ma
7 Department of Chemistry, An-Najah National University, Nablus P. O. Box 7, Palestine; ohamed@najah.edu (O.H.); g.hanbali@najah.edu (G.H.); bayan.kh107@hotmail.com (B.K.)
3 Nanomaterials for Energy and Environment Laboratory, Cadi Ayyad University, Marrakech PB 2390, Morocco; aoutzour@ucam.ac.ma
6 University Department, Royal Naval School, Sour Jdid Boulevard, Casablanca B.P 16303, Morocco; abderrahimelbachiri71@gmail.com
4 Laboratory of Advanced Materials and Process Engineering, Department of Chemistry, Faculty of Science, Ibn Tofail University, BP 133, Kenitra 14000, Morocco; a.elharfi@outlook.fr
5 Higher School of Textile and Clothing Industries, Laboratory REMTEX, Oulfa BP 7731, Casablanca, Morocco; cherkaoui@esith.ac.ma
1 Laboratory of Industrial Technologies and Services (LITS), Department of Process Engineering, Height School of Technology, Sidi Mo
AuthorAffiliation_xml – name: 1 Laboratory of Industrial Technologies and Services (LITS), Department of Process Engineering, Height School of Technology, Sidi Mohammed Ben Abdallah University, P.O. Box 2427, Fez 30000, Morocco; gouri_mustapha@yahoo.fr
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– name: 7 Department of Chemistry, An-Najah National University, Nablus P. O. Box 7, Palestine; ohamed@najah.edu (O.H.); g.hanbali@najah.edu (G.H.); bayan.kh107@hotmail.com (B.K.)
– name: 4 Laboratory of Advanced Materials and Process Engineering, Department of Chemistry, Faculty of Science, Ibn Tofail University, BP 133, Kenitra 14000, Morocco; a.elharfi@outlook.fr
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epoxy resin
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Snippet In this work, we have studied, formulated, prepared, and characterized the rheological and electrical behavior of a composite material based on an epoxy resin...
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StartPage 921
SubjectTerms Bisphenol A
Composite materials
Curing
Electrical properties
Epoxy resins
Frequency variation
Mars
Mathematical analysis
Mechanical properties
Methylene dianiline
Modulus of elasticity
Morphology
Nanoparticles
Physical properties
Polymer matrix composites
Polymers
Rheological properties
Rheology
Room temperature
Viscoelasticity
Title Rheological and Electrical Study of a Composite Material Based on an Epoxy Polymer Containing Cyclotriphosphazene
URI https://www.ncbi.nlm.nih.gov/pubmed/32316145
https://www.proquest.com/docview/2392186400
https://www.proquest.com/docview/2393573656
https://pubmed.ncbi.nlm.nih.gov/PMC7240388
Volume 12
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