In situ study of the oxidation of ZrB2 and ZrB2-SiC materials by monitoring the LIF signal of BO2 radicals

•First application of the Laser Induced Fluorescence technique to investigate the in situ oxidation of UHTC samples.•Detection of the BO2 radicals in the gas phase above UHTC materials during an oxidation test up to 1873K.•Determination of the volatile species formed during oxidation.•In situ oxidat...

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Published inCorrosion science Vol. 148; pp. 31 - 38
Main Authors Guérineau, V., Julian-Jankowiak, A., Vilmart, G., Dorval, N.
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier Ltd 01.03.2019
Elsevier BV
Elsevier
Subjects
A. Ceramic
Air flow
B. Spectroscopy
B.Laser induced fluorescence
C. High temperature corrosion
C. Oxidation
Carbon dioxide
Carbon dioxide lasers
Engineering Sciences
Laser induced fluorescence
Lasers
Materials
Oxidation
Radicals
Refractory materials
Signal monitoring
Silicon dioxide
Vapor phases
Zirconium compounds
C. High temperature corrosion
B. Spectroscopy
C. Oxidation
A. Ceramic
B.Laser induced fluorescence
HIGH TEMPERATURE CORROSION
OXIDATION
ZRB2
CERAMIC
SPECTROSCOPY
UHTC
ZRB2-SIC
LIF
LASER INDUCED FLUORESCENCE
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Abstract •First application of the Laser Induced Fluorescence technique to investigate the in situ oxidation of UHTC samples.•Detection of the BO2 radicals in the gas phase above UHTC materials during an oxidation test up to 1873K.•Determination of the volatile species formed during oxidation.•In situ oxidation mechanisms. In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples in air, in order to provide an in situ and real-time monitoring of their thermal oxidation. Samples are heated up to 1923 K in air flow with a 2 kW CO2 laser. The BO2 fluorescence and the laser transmission signals are monitored throughout the temperature ramp. This technique allows to detect the key steps of the oxidation (silica formation,...) and to propose more precise oxidation mechanisms as a function of temperature.
AbstractList In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples in air, in order to provide an in situ and real-time monitoring of their thermal oxidation. Samples are heated up to 1923 K in air flow with a 2 kW CO2 laser. The BO2 fluorescence and the laser transmission signals are monitored throughout the temperature ramp. This technique allows to detect the key steps of the oxidation (silica formation,...) and to propose more precise oxidation mechanisms as a function of temperature. Dans cette étude, la Fluorescence Induite par Laser (LIF) est utilisée pour suivre des espèces gazeuses telles que BO2(g) émises lors de l'oxydation de matériaux tels que ZrB2 ou ZrB2-SiC. Des échantillons de compositions ZrB2 etZrB2-20 vol % SiC sont chauffés dans une enceinte spécifique à la pression atmosphérique, sous air et jusqu'à 1650°C grâce à un laser CO2 de 2kW.La LIF de BO2(g) est étudiée dans le système électronique A2u - X2g avec un laser d'excitation à 547nm et une détection de la fluorescence à 580nm. Les signaux de fluorescence et d'absorption enregistrés lors de la chauffe nous ont permis de détecter les étapes clés de l'oxydation comme, le début de l'oxydation de SiC, le remplissage de la couche vitreuse ou encore l'évaporation catastrophique de la couche vitreuse.Le signal LIF a été corrélé aux réactions possibles de B2O3 avec l'air. Ce diagnostic in situ nous a permis de proposer des mécanismes d'oxydation plus précis au cours de la montée en température.
In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples in air, in order to provide an in situ and real-time monitoring of their thermal oxidation. Samples are heated up to 1923 K in air flow with a 2 kW CO2 laser. The BO2 fluorescence and the laser transmission signals are monitored throughout the temperature ramp. This technique allows to detect the key steps of the oxidation (silica formation,...) and to propose more precise oxidation mechanisms as a function of temperature.
•First application of the Laser Induced Fluorescence technique to investigate the in situ oxidation of UHTC samples.•Detection of the BO2 radicals in the gas phase above UHTC materials during an oxidation test up to 1873K.•Determination of the volatile species formed during oxidation.•In situ oxidation mechanisms. In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples in air, in order to provide an in situ and real-time monitoring of their thermal oxidation. Samples are heated up to 1923 K in air flow with a 2 kW CO2 laser. The BO2 fluorescence and the laser transmission signals are monitored throughout the temperature ramp. This technique allows to detect the key steps of the oxidation (silica formation,...) and to propose more precise oxidation mechanisms as a function of temperature.
Author Dorval, N.
Julian-Jankowiak, A.
Vilmart, G.
Guérineau, V.
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Keywords C. High temperature corrosion
B. Spectroscopy
C. Oxidation
A. Ceramic
B.Laser induced fluorescence
HIGH TEMPERATURE CORROSION
OXIDATION
ZRB2
CERAMIC
SPECTROSCOPY
UHTC
ZRB2-SIC
LIF
LASER INDUCED FLUORESCENCE
Language English
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Snippet •First application of the Laser Induced Fluorescence technique to investigate the in situ oxidation of UHTC samples.•Detection of the BO2 radicals in the gas...
In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples...
In this study, the Laser Induced Fluorescence (LIF) technique is used to detect BO2 radicals in the gas phase above heated ZrB2 and ZrB2-20 vol. % SiC samples...
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StartPage 31
SubjectTerms A. Ceramic
Air flow
B. Spectroscopy
B.Laser induced fluorescence
C. High temperature corrosion
C. Oxidation
Carbon dioxide
Carbon dioxide lasers
Engineering Sciences
Laser induced fluorescence
Lasers
Materials
Oxidation
Radicals
Refractory materials
Signal monitoring
Silicon dioxide
Vapor phases
Zirconium compounds
Title In situ study of the oxidation of ZrB2 and ZrB2-SiC materials by monitoring the LIF signal of BO2 radicals
URI https://dx.doi.org/10.1016/j.corsci.2018.11.032
https://www.proquest.com/docview/2199232282
https://hal.science/hal-01985750
Volume 148
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