Iron oxide-silica nanocomposites yielded by chemical route and sol–gel method
Magnetic nanoparticles yielded by chemical route were surface modified with stabilizing agents being further coated by sol–gel method with silica shell to be used for various applications. Iron oxide magnetic cores were dispersed in water by single citrate layer and, respectively, by double oleate h...
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| Published in | Journal of sol-gel science and technology Vol. 79; no. 3; pp. 457 - 465 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.09.2016
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0928-0707 1573-4846 |
| DOI | 10.1007/s10971-016-3996-1 |
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| Abstract | Magnetic nanoparticles yielded by chemical route were surface modified with stabilizing agents being further coated by sol–gel method with silica shell to be used for various applications. Iron oxide magnetic cores were dispersed in water by single citrate layer and, respectively, by double oleate hydrophilic coating. Sol–gel reaction with tetraethylorthosilicate provided further coating with silica that confers increased reactivity for ligand coupling. Microstructural and magnetic properties were investigated by standard methods evidencing nanometric size, good crystallinity, and superparamagnetic behavior. Comparative analysis evidenced similar crystallite size for both citrate- and oleate-coated magnetic nanoparticles, while granularity was changed after silica adding. Saturation magnetization diminished less for oleate-stabilized nanoparticles than for citrate-stabilized ones after silica coating and moderate thermal treatment. Such prepared magnetic nanocomposites could have possible utilization as magnetic vectors for targeted biomolecules.
Graphical Abstract |
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| AbstractList | Magnetic nanoparticles yielded by chemical route were surface modified with stabilizing agents being further coated by sol–gel method with silica shell to be used for various applications. Iron oxide magnetic cores were dispersed in water by single citrate layer and, respectively, by double oleate hydrophilic coating. Sol–gel reaction with tetraethylorthosilicate provided further coating with silica that confers increased reactivity for ligand coupling. Microstructural and magnetic properties were investigated by standard methods evidencing nanometric size, good crystallinity, and superparamagnetic behavior. Comparative analysis evidenced similar crystallite size for both citrate- and oleate-coated magnetic nanoparticles, while granularity was changed after silica adding. Saturation magnetization diminished less for oleate-stabilized nanoparticles than for citrate-stabilized ones after silica coating and moderate thermal treatment. Such prepared magnetic nanocomposites could have possible utilization as magnetic vectors for targeted biomolecules.Graphical Abstract Magnetic nanoparticles yielded by chemical route were surface modified with stabilizing agents being further coated by sol–gel method with silica shell to be used for various applications. Iron oxide magnetic cores were dispersed in water by single citrate layer and, respectively, by double oleate hydrophilic coating. Sol–gel reaction with tetraethylorthosilicate provided further coating with silica that confers increased reactivity for ligand coupling. Microstructural and magnetic properties were investigated by standard methods evidencing nanometric size, good crystallinity, and superparamagnetic behavior. Comparative analysis evidenced similar crystallite size for both citrate- and oleate-coated magnetic nanoparticles, while granularity was changed after silica adding. Saturation magnetization diminished less for oleate-stabilized nanoparticles than for citrate-stabilized ones after silica coating and moderate thermal treatment. Such prepared magnetic nanocomposites could have possible utilization as magnetic vectors for targeted biomolecules. Graphical Abstract |
| Author | Puscasu, E. Lupu, N. Creanga, D. Balasoiu, M. Sacarescu, L. Oanca, G. Grigoras, M. |
| Author_xml | – sequence: 1 givenname: E. surname: Puscasu fullname: Puscasu, E. organization: Physics Faculty, “Alexandru Ioan Cuza” University – sequence: 2 givenname: L. surname: Sacarescu fullname: Sacarescu, L. organization: “Petru Poni” Institute of Macromolecular Chemistry – sequence: 3 givenname: N. surname: Lupu fullname: Lupu, N. organization: National Institute of Research and Development for Technical Physics – sequence: 4 givenname: M. surname: Grigoras fullname: Grigoras, M. organization: National Institute of Research and Development for Technical Physics – sequence: 5 givenname: G. surname: Oanca fullname: Oanca, G. organization: Physics Faculty, “Alexandru Ioan Cuza” University – sequence: 6 givenname: M. surname: Balasoiu fullname: Balasoiu, M. organization: Joint Institute for Nuclear Research, Horia Hulubei Institute of Physics and Nuclear Engineering – sequence: 7 givenname: D. surname: Creanga fullname: Creanga, D. email: dorina.creanga@gmail.com, mdor@uaic.ro organization: Physics Faculty, “Alexandru Ioan Cuza” University |
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| CitedBy_id | crossref_primary_10_1088_1742_6596_994_1_012009 crossref_primary_10_1016_j_talo_2022_100129 crossref_primary_10_1016_j_addr_2019_01_005 crossref_primary_10_1016_j_micromeso_2020_110858 crossref_primary_10_1021_acs_iecr_2c03338 crossref_primary_10_1088_1742_6596_848_1_012026 crossref_primary_10_1080_15421406_2020_1731085 |
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| Keywords | Citrate Superparamagnetic nanocomposites Iron oxides Oleate double layer Sol–gel coating |
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| SubjectTerms | Biomolecules Ceramics Chemistry and Materials Science Coating colloids Composites Crystallites etc. fibers Glass Heat treatment Inorganic Chemistry Iron oxides Magnetic cores Magnetic properties Magnetic saturation Materials Science Nanocomposites Nanoparticles Nanostructure Nanotechnology Natural Materials Optical and Electronic Materials Organic chemistry Original Paper: Nano-structured materials (particles Silica gel Silicon dioxide Sol gel process Sol-gel processes Stabilizers (agents) |
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| Title | Iron oxide-silica nanocomposites yielded by chemical route and sol–gel method |
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