Manganese films electrodeposited at different potentials and temperatures in ionic liquid and their application as electrode materials for supercapacitors

Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP–NTf 2) ionic liquid is demonstrated in this study. Crystal structures and surface morphologies of the Mn films deposited at various potentials (from −1.8 V to −2.2 V) and temperatures (from 50 °C to...

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Published inElectrochimica acta Vol. 53; no. 13; pp. 4447 - 4453
Main Authors Chang, Jeng-Kuei, Huang, Chiung-Hui, Tsai, Wen-Ta, Deng, Ming-Jay, Sun, I-Wen, Chen, Po-Yu
Format Journal Article
LanguageEnglish
Published Oxford Elsevier Ltd 20.05.2008
Elsevier
Subjects
Applied sciences
Capacitors. Resistors. Filters
Chemistry
Electrical engineering. Electrical power engineering
Electrochemistry
Electrodeposition
Exact sciences and technology
General and physical chemistry
Ionic liquid
Manganese
Pseudocapacitance
Study of interfaces
Supercapacitor
Various equipment and components
Supercapacitor
Electrodeposition
Pseudocapacitance
Manganese
Ionic liquid
Scanning electron microscopy
Temperature effect
Transition metal
Electrolytic capacitor
Electrode material
X ray diffraction
Operating conditions
Surface structure
Electrodes
Morphology
Nickel
Electrochemical reaction
Specific capacity
Electrical characteristic
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Abstract Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP–NTf 2) ionic liquid is demonstrated in this study. Crystal structures and surface morphologies of the Mn films deposited at various potentials (from −1.8 V to −2.2 V) and temperatures (from 50 °C to 110 °C) were examined with an X-ray diffractometer (XRD) and a scanning electron microscope (SEM), respectively. Experimental results indicate that the deposited Mn films were amorphous in nature; however, their morphologies strongly depended on the deposition conditions. After being anodized in Na 2SO 4 solution, the deposited Mn was transformed to Mn oxide. Electrochemical properties of the Mn oxides were evaluated using cyclic voltammetry (CV). It was confirmed that the different Mn deposition conditions caused the variations in pseudocapacitive performance of the oxide electrodes. The oxide (∼0.1 mg) anodized from the Mn deposited at −1.8 V and 50 °C had the highest specific capacitance of 402 F/g measured at a CV scan rate of 5 mV/s. Its capacitance retained ratio after 500 CV testing cycles was as high as 94%.
AbstractList Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP-NTf2) ionic liquid is demonstrated in this study. Crystal structures and surface morphologies of the Mn films deposited at various potentials (from -1.8V to -2.2V) and temperatures (from 50 deg C to 110 deg C) were examined with an X-ray diffractometer (XRD) and a scanning electron microscope (SEM), respectively. Experimental results indicate that the deposited Mn films were amorphous in nature; however, their morphologies strongly depended on the deposition conditions. After being anodized in Na2SO4 solution, the deposited Mn was transformed to Mn oxide. Electrochemical properties of the Mn oxides were evaluated using cyclic voltammetry (CV). It was confirmed that the different Mn deposition conditions caused the variations in pseudocapacitive performance of the oxide electrodes. The oxide (0.1mg) anodized from the Mn deposited at -1.8V and 50 deg C had the highest specific capacitance of 402F/g measured at a CV scan rate of 5mV/s. Its capacitance retained ratio after 500 CV testing cycles was as high as 94%.
Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP–NTf 2) ionic liquid is demonstrated in this study. Crystal structures and surface morphologies of the Mn films deposited at various potentials (from −1.8 V to −2.2 V) and temperatures (from 50 °C to 110 °C) were examined with an X-ray diffractometer (XRD) and a scanning electron microscope (SEM), respectively. Experimental results indicate that the deposited Mn films were amorphous in nature; however, their morphologies strongly depended on the deposition conditions. After being anodized in Na 2SO 4 solution, the deposited Mn was transformed to Mn oxide. Electrochemical properties of the Mn oxides were evaluated using cyclic voltammetry (CV). It was confirmed that the different Mn deposition conditions caused the variations in pseudocapacitive performance of the oxide electrodes. The oxide (∼0.1 mg) anodized from the Mn deposited at −1.8 V and 50 °C had the highest specific capacitance of 402 F/g measured at a CV scan rate of 5 mV/s. Its capacitance retained ratio after 500 CV testing cycles was as high as 94%.
Author Deng, Ming-Jay
Chen, Po-Yu
Sun, I-Wen
Tsai, Wen-Ta
Chang, Jeng-Kuei
Huang, Chiung-Hui
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  givenname: Po-Yu
  surname: Chen
  fullname: Chen, Po-Yu
  organization: Faculty of Medicinal and Applied Chemistry, Kaohsiung Medical University, Kaohsiung, Taiwan
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Issue 13
Keywords Supercapacitor
Electrodeposition
Pseudocapacitance
Manganese
Ionic liquid
Scanning electron microscopy
Temperature effect
Transition metal
Electrolytic capacitor
Electrode material
X ray diffraction
Operating conditions
Surface structure
Electrodes
Morphology
Nickel
Electrochemical reaction
Specific capacity
Electrical characteristic
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Snippet Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP–NTf 2) ionic liquid is demonstrated in this study....
Electrodeposition of manganese (Mn) in butylmethylpyrrolidinium bis(trifluoromethylsulfony)imide (BMP-NTf2) ionic liquid is demonstrated in this study. Crystal...
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SubjectTerms Applied sciences
Capacitors. Resistors. Filters
Chemistry
Electrical engineering. Electrical power engineering
Electrochemistry
Electrodeposition
Exact sciences and technology
General and physical chemistry
Ionic liquid
Manganese
Pseudocapacitance
Study of interfaces
Supercapacitor
Various equipment and components
Title Manganese films electrodeposited at different potentials and temperatures in ionic liquid and their application as electrode materials for supercapacitors
URI https://dx.doi.org/10.1016/j.electacta.2008.01.036
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