Compaction and clay content control mudrock porosity

Mudrocks, ubiquitous yet poorly understood sedimentary rocks with significant variations in composition and physical properties, form seals for geological carbon dioxide and energy (e.g., hydrogen and methane) storage, repositories for radioactive waste disposal, and reservoirs for natural gas. Unde...

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Published in	Energy (Oxford) Vol. 289; p. 129966
Main Authors	Rezaeyan, Amirsaman, Kampman, Niko, Pipich, Vitaliy, Barnsley, Lester C., Rother, Gernot, Magill, Clayton, Ma, Jingsheng, Busch, Andreas
Format	Journal Article
Language	English
Published	United States Elsevier Ltd 15.02.2024 Elsevier
Subjects	carbon dioxide clay fraction energy GEOSCIENCES hydrogen methane mineralogy Mudrock multivariate analysis Multivariate statistics natural gas neutrons Porosity radioactive waste Small-angle neutron scattering (SANS) stratigraphy Very small-angle neutron scattering (VSANS) waste disposal Small-angle neutron scattering (SANS) Porosity Multivariate statistics Mudrock Very small-angle neutron scattering (VSANS)
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Abstract	Mudrocks, ubiquitous yet poorly understood sedimentary rocks with significant variations in composition and physical properties, form seals for geological carbon dioxide and energy (e.g., hydrogen and methane) storage, repositories for radioactive waste disposal, and reservoirs for natural gas. Understanding the controls on mudrock pore structure is essential for evaluating their porosity. The identification and quantification of controls depend on the nano-to micron scale pore network, which are the subject of this study. Small-angle (SANS) and very small-angle neutron scattering (VSANS) experiments were conducted on 13 diverse mudrock sets, characterised by differences in mineralogy, stratigraphy, maturity, and depositional environment. We performed multivariate statistics to systematically characterise the pore structure in 71 samples cross a 5 μm–2 nm pore size range. Our results indicate a multivariate approach more effectively captures the complex controls on porosity rather than single parameters. Compaction and clay content emerge as key primary and secondary controls on mudrock porosity, respectively, upon which we introduce a new porosity classification. Our complementary experimental-statistical assessment involving SANS-derived multiscale porosity sheds new light on the influence of structural controls on storage or production capacity in mudrocks. [Display omitted] •Compaction is the primary and clay the secondary control on mudrock porosity.•While TOC barely affects mudrock porosity, it influences meso/macropores the most.•Mudrock controls influence porosity across various scales.
AbstractList	Mudrocks, ubiquitous yet poorly understood sedimentary rocks with significant variations in composition and physical properties, form seals for geological carbon dioxide and energy (e.g., hydrogen and methane) storage, repositories for radioactive waste disposal, and reservoirs for natural gas. Understanding the controls on mudrock pore structure is essential for evaluating their porosity. The identification and quantification of controls depend on the nano-to micron scale pore network, which are the subject of this study. Small-angle (SANS) and very small-angle neutron scattering (VSANS) experiments were conducted on 13 diverse mudrock sets, characterised by differences in mineralogy, stratigraphy, maturity, and depositional environment. We performed multivariate statistics to systematically characterise the pore structure in 71 samples cross a 5 μm–2 nm pore size range. Our results indicate a multivariate approach more effectively captures the complex controls on porosity rather than single parameters. Compaction and clay content emerge as key primary and secondary controls on mudrock porosity, respectively, upon which we introduce a new porosity classification. Our complementary experimental-statistical assessment involving SANS-derived multiscale porosity sheds new light on the influence of structural controls on storage or production capacity in mudrocks. Mudrocks, ubiquitous yet poorly understood sedimentary rocks with significant variations in composition and physical properties, form seals for geological carbon dioxide and energy (e.g., hydrogen and methane) storage, repositories for radioactive waste disposal, and reservoirs for natural gas. Understanding the controls on mudrock pore structure is essential for evaluating their porosity. The identification and quantification of controls depend on the nano-to micron scale pore network, which are the subject of this study. Small-angle (SANS) and very small-angle neutron scattering (VSANS) experiments were conducted on 13 diverse mudrock sets, characterised by differences in mineralogy, stratigraphy, maturity, and depositional environment. We performed multivariate statistics to systematically characterise the pore structure in 71 samples cross a 5 μm–2 nm pore size range. Our results indicate a multivariate approach more effectively captures the complex controls on porosity rather than single parameters. Compaction and clay content emerge as key primary and secondary controls on mudrock porosity, respectively, upon which we introduce a new porosity classification. Our complementary experimental-statistical assessment involving SANS-derived multiscale porosity sheds new light on the influence of structural controls on storage or production capacity in mudrocks. [Display omitted] •Compaction is the primary and clay the secondary control on mudrock porosity.•While TOC barely affects mudrock porosity, it influences meso/macropores the most.•Mudrock controls influence porosity across various scales.
ArticleNumber	129966
Author	Kampman, Niko Magill, Clayton Ma, Jingsheng Rezaeyan, Amirsaman Pipich, Vitaliy Rother, Gernot Busch, Andreas Barnsley, Lester C.
Author_xml	– sequence: 1 givenname: Amirsaman orcidid: 0000-0002-5608-8115 surname: Rezaeyan fullname: Rezaeyan, Amirsaman email: amirsaman.rezaeyan@hw.ac.uk, amirsaman.rezaeyan@gmail.com organization: Lyell Centre, Institute of GeoEnergy Engineering, Heriot-Watt University, Edinburgh, EH14 4AS, UK – sequence: 2 givenname: Niko surname: Kampman fullname: Kampman, Niko organization: Nuclear Waste Services, Didcot, OX11 0GD, UK – sequence: 3 givenname: Vitaliy surname: Pipich fullname: Pipich, Vitaliy organization: Forschungszentrum Jülich GmbH, Jülich Centre for Neutron Science JCNS at Heinz Maier-Leibnitz Zentrum MLZ, Garching, 85748, Germany – sequence: 4 givenname: Lester C. orcidid: 0000-0002-1341-905X surname: Barnsley fullname: Barnsley, Lester C. organization: Forschungszentrum Jülich GmbH, Jülich Centre for Neutron Science JCNS at Heinz Maier-Leibnitz Zentrum MLZ, Garching, 85748, Germany – sequence: 5 givenname: Gernot surname: Rother fullname: Rother, Gernot organization: Chemical Sciences Division, Oak Ridge National Laboratory, Oak Ridge, TN, 37922, USA – sequence: 6 givenname: Clayton orcidid: 0000-0002-7447-6277 surname: Magill fullname: Magill, Clayton organization: Lyell Centre, Institute of Life and Earth Sciences, Heriot-Watt University, Edinburgh, EH14 4AS, UK – sequence: 7 givenname: Jingsheng surname: Ma fullname: Ma, Jingsheng organization: Institute of GeoEnergy Engineering, Heriot-Watt University, Edinburgh, EH14 4AS, UK – sequence: 8 givenname: Andreas orcidid: 0000-0002-3279-5202 surname: Busch fullname: Busch, Andreas organization: Lyell Centre, Institute of GeoEnergy Engineering, Heriot-Watt University, Edinburgh, EH14 4AS, UK
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Keywords	Small-angle neutron scattering (SANS) Porosity Multivariate statistics Mudrock Very small-angle neutron scattering (VSANS)
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Snippet	Mudrocks, ubiquitous yet poorly understood sedimentary rocks with significant variations in composition and physical properties, form seals for geological...
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StartPage	129966
SubjectTerms	carbon dioxide clay fraction energy GEOSCIENCES hydrogen methane mineralogy Mudrock multivariate analysis Multivariate statistics natural gas neutrons Porosity radioactive waste Small-angle neutron scattering (SANS) stratigraphy Very small-angle neutron scattering (VSANS) waste disposal
Title	Compaction and clay content control mudrock porosity
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