Synthesis of self-supported non-precious metal catalysts for oxygen reduction reaction with preserved nanostructures from the polyaniline nanofiber precursor

Non-precious metal catalysts (NPMCs) for the oxygen reduction reaction (ORR) are an active subject of recent research on proton exchange membrane fuel cells. In this study, we report a new approach to preparation of self-supported and nano-structured NPMCs using pre-prepared polyaniline (PANI) nanof...

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Published inJournal of power sources Vol. 225; pp. 129 - 136
Main Authors Hu, Yang, Zhao, Xiao, Huang, Yunjie, Li, Qingfeng, Bjerrum, Niels J., Liu, Changpeng, Xing, Wei
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 01.03.2013
Elsevier
Subjects
Active site
Activity
Applied sciences
Catalysis
Catalysts: preparations and properties
Chemistry
Direct energy conversion and energy accumulation
Electrical engineering. Electrical power engineering
Electrical power engineering
Electrochemical conversion: primary and secondary batteries, fuel cells
Energy
Energy. Thermal use of fuels
Equipments for energy generation and conversion: thermal, electrical, mechanical energy, etc
Exact sciences and technology
Fuel cells
General and physical chemistry
Heat-treatment
Non-precious metal catalyst
Oxygen reduction reaction
Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
Activity
Non-precious metal catalyst
Oxygen reduction reaction
Active site
Heat-treatment
Oxygen
Heat treatment
Nanostructured material
Non metallic material
Nanofiber
Nanostructure
Carbon
Chemical reduction
Catalyst activity
Proton exchange membrane fuel cells
Catalyst
Aniline polymer
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Abstract Non-precious metal catalysts (NPMCs) for the oxygen reduction reaction (ORR) are an active subject of recent research on proton exchange membrane fuel cells. In this study, we report a new approach to preparation of self-supported and nano-structured NPMCs using pre-prepared polyaniline (PANI) nanofibers as both nitrogen and carbon precursors. The synthesized NPMCs possess nanoworm structures preserved from the PANI precursor and exhibit high onset potential of 0.905 V vs. RHE and selective activity of nearly four-electron ORR pathways. A significant enhancement in the intrinsic activity and onset potential for the ORR is observed when the Fe content in the precursor is increased from 0 to 3.0 wt.%, while further addition to 10.0 wt.% results in a decrease in the catalytic activity. ► Novel preparation of self-supported and nano-structured NPMCs for ORR. ► An onset potential of 0.905 V vs. RHE and nearly four-electron ORR pathway. ► Effects of ferrous species in precursors on the final catalysts explored. ► Onset ORR potentials increasing with the initial Fe content from 0 to 3.0 wt.%.
AbstractList Non-precious metal catalysts (NPMCs) for the oxygen reduction reaction (ORR) are an active subject of recent research on proton exchange membrane fuel cells. In this study, we report a new approach to preparation of self-supported and nano-structured NPMCs using pre-prepared polyaniline (PANI) nanofibers as both nitrogen and carbon precursors. The synthesized NPMCs possess nanoworm structures preserved from the PANI precursor and exhibit high onset potential of 0.905 V vs. RHE and selective activity of nearly four-electron ORR pathways. A significant enhancement in the intrinsic activity and onset potential for the ORR is observed when the Fe content in the precursor is increased from 0 to 3.0 wt.%, while further addition to 10.0 wt.% results in a decrease in the catalytic activity.
Non-precious metal catalysts (NPMCs) for the oxygen reduction reaction (ORR) are an active subject of recent research on proton exchange membrane fuel cells. In this study, we report a new approach to preparation of self-supported and nano-structured NPMCs using pre-prepared polyaniline (PANI) nanofibers as both nitrogen and carbon precursors. The synthesized NPMCs possess nanoworm structures preserved from the PANI precursor and exhibit high onset potential of 0.905 V vs. RHE and selective activity of nearly four-electron ORR pathways. A significant enhancement in the intrinsic activity and onset potential for the ORR is observed when the Fe content in the precursor is increased from 0 to 3.0 wt.%, while further addition to 10.0 wt.% results in a decrease in the catalytic activity. ► Novel preparation of self-supported and nano-structured NPMCs for ORR. ► An onset potential of 0.905 V vs. RHE and nearly four-electron ORR pathway. ► Effects of ferrous species in precursors on the final catalysts explored. ► Onset ORR potentials increasing with the initial Fe content from 0 to 3.0 wt.%.
Author Liu, Changpeng
Xing, Wei
Zhao, Xiao
Bjerrum, Niels J.
Hu, Yang
Huang, Yunjie
Li, Qingfeng
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  givenname: Changpeng
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– sequence: 7
  givenname: Wei
  surname: Xing
  fullname: Xing, Wei
  email: xingwei@ciac.jl.cn
  organization: State Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China
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Keywords Activity
Non-precious metal catalyst
Oxygen reduction reaction
Active site
Heat-treatment
Oxygen
Heat treatment
Nanostructured material
Non metallic material
Nanofiber
Nanostructure
Carbon
Chemical reduction
Catalyst activity
Proton exchange membrane fuel cells
Catalyst
Aniline polymer
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Snippet Non-precious metal catalysts (NPMCs) for the oxygen reduction reaction (ORR) are an active subject of recent research on proton exchange membrane fuel cells....
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SubjectTerms Active site
Activity
Applied sciences
Catalysis
Catalysts: preparations and properties
Chemistry
Direct energy conversion and energy accumulation
Electrical engineering. Electrical power engineering
Electrical power engineering
Electrochemical conversion: primary and secondary batteries, fuel cells
Energy
Energy. Thermal use of fuels
Equipments for energy generation and conversion: thermal, electrical, mechanical energy, etc
Exact sciences and technology
Fuel cells
General and physical chemistry
Heat-treatment
Non-precious metal catalyst
Oxygen reduction reaction
Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
Title Synthesis of self-supported non-precious metal catalysts for oxygen reduction reaction with preserved nanostructures from the polyaniline nanofiber precursor
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