High resolution imaging analysis of CdSe/ZnS core–shell quantum dots (QDs) using Cs-corrected HR-TEM/STEM
CdSe/ZnS core–shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency, narrow-band, and particle-size-tunable photoluminescence. In particular, their small size results in the quantum confinement of semiconductor nano...
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Published in | Journal of materials science. Materials in electronics Vol. 24; no. 10; pp. 3744 - 3748 |
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Main Authors | , , , , |
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Language | English |
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01.10.2013
Springer Springer Nature B.V |
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Abstract | CdSe/ZnS core–shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency, narrow-band, and particle-size-tunable photoluminescence. In particular, their small size results in the quantum confinement of semiconductor nano-crystals, which widens their energy gaps. In general, high resolution imaging analyses of QDs using a transmission electron microscope are very difficult due to their significantly small size. Successful imaging depends on the capabilities of TEM equipment and the contrast of the QDs sample relative to the supporting film. In this work, all imaging analyses were performed on a TEM equipped with a probe Cs corrector. The samples for observing QDs were prepared by drying each QDs solution on a lacey carbon Cu (300 mesh) grid previously coated with an ultra-thin graphene monolayer (thickness = 0.3 nm), due to the need to minimize the effect of the supported film. |
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AbstractList | CdSe/ZnS core–shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency, narrow-band, and particle-size-tunable photoluminescence. In particular, their small size results in the quantum confinement of semiconductor nano-crystals, which widens their energy gaps. In general, high resolution imaging analyses of QDs using a transmission electron microscope are very difficult due to their significantly small size. Successful imaging depends on the capabilities of TEM equipment and the contrast of the QDs sample relative to the supporting film. In this work, all imaging analyses were performed on a TEM equipped with a probe Cs corrector. The samples for observing QDs were prepared by drying each QDs solution on a lacey carbon Cu (300 mesh) grid previously coated with an ultra-thin graphene monolayer (thickness = 0.3 nm), due to the need to minimize the effect of the supported film. CdSe/ZnS core-shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency, narrow-band, and particle-size-tunable photoluminescence. In particular, their small size results in the quantum confinement of semiconductor nano-crystals, which widens their energy gaps. In general, high resolution imaging analyses of QDs using a transmission electron microscope are very difficult due to their significantly small size. Successful imaging depends on the capabilities of TEM equipment and the contrast of the QDs sample relative to the supporting film. In this work, all imaging analyses were performed on a TEM equipped with a probe Cs corrector. The samples for observing QDs were prepared by drying each QDs solution on a lacey carbon Cu (300 mesh) grid previously coated with an ultra-thin graphene monolayer (thickness = 0.3 nm), due to the need to minimize the effect of the supported film.[PUBLICATION ABSTRACT] CdSe/ZnS core-shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency, narrow-band, and particle-size-tunable photoluminescence. In particular, their small size results in the quantum confinement of semiconductor nano-crystals, which widens their energy gaps. In general, high resolution imaging analyses of QDs using a transmission electron microscope are very difficult due to their significantly small size. Successful imaging depends on the capabilities of TEM equipment and the contrast of the QDs sample relative to the supporting film. In this work, all imaging analyses were performed on a TEM equipped with a probe Cs corrector. The samples for observing QDs were prepared by drying each QDs solution on a lacey carbon Cu (300 mesh) grid previously coated with an ultra-thin graphene monolayer (thickness = 0.3 nm), due to the need to minimize the effect of the supported film. |
Author | Cho, Myungju Park, Kyuho Jang, Dongseon Jang, Youngil Shin, Huiyoun |
Author_xml | – sequence: 1 givenname: Huiyoun surname: Shin fullname: Shin, Huiyoun email: hy.shin@lge.com organization: Materials Characterization Team, Materials and Components Laboratory, LG Electronics Advanced Research Institute – sequence: 2 givenname: Dongseon surname: Jang fullname: Jang, Dongseon organization: Materials Characterization Team, Materials and Components Laboratory, LG Electronics Advanced Research Institute – sequence: 3 givenname: Youngil surname: Jang fullname: Jang, Youngil organization: Materials Characterization Team, Materials and Components Laboratory, LG Electronics Advanced Research Institute – sequence: 4 givenname: Myungju surname: Cho fullname: Cho, Myungju organization: Materials Characterization Team, Materials and Components Laboratory, LG Electronics Advanced Research Institute – sequence: 5 givenname: Kyuho surname: Park fullname: Park, Kyuho organization: Materials Characterization Team, Materials and Components Laboratory, LG Electronics Advanced Research Institute |
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Keywords | Graphene Membrane Graphene Monolayer Transmission Electron Microscope Specimen Stem HAADF Image CdSe Core Quantum confinement Tunable circuit Particle size High resolution Quantum dot Photoluminescence Coatings Zinc sulfide Energy gap Light emission Imaging Nanodot Copper Scanning transmission electron microscopy Nanocrystal Ultrathin films II-VI compound Core shell structure Quantum yield Narrow band Carbon Coated material Cadmium selenides Thickness Transmission electron microscopy Graphene High efficiency Zero band gap semiconductors Drying |
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Snippet | CdSe/ZnS core–shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency,... CdSe/ZnS core-shell structured nano-crystal quantum dots (QDs) are ideal candidates for light-emission applications due to their high quantum efficiency,... |
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SubjectTerms | Applied sciences Cadmium selenides Characterization and Evaluation of Materials Chemistry and Materials Science Condensed matter: electronic structure, electrical, magnetic, and optical properties Cross-disciplinary physics: materials science; rheology Electronics Exact sciences and technology High resolution Imaging Intermetallics Materials Materials Science Metals. Metallurgy Nanocrystals Nanoscale materials and structures: fabrication and characterization Optical and Electronic Materials Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Photoluminescence Physics Production techniques Quantum confinement Quantum dots Semiconductors Surface treatment Transmission electron microscopy |
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Title | High resolution imaging analysis of CdSe/ZnS core–shell quantum dots (QDs) using Cs-corrected HR-TEM/STEM |
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