Nanoceramics and novel functionalized silicate-based magnetic nanocomposites as substitutional disinfectants for water and wastewater purification
Herein, we successfully synthesized nano-porous Co 2 O 3 /Cu 2 O 3 : Al 2 O 3 : SiO 2 ((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h. The crystallization behavior and spectroscopic properties were investigated using X-ray diffraction, field emission-scanning e...
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Published in | Environmental science and pollution research international Vol. 27; no. 21; pp. 26668 - 26680 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Berlin/Heidelberg
Springer Berlin Heidelberg
01.07.2020
Springer Nature B.V |
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Abstract | Herein, we successfully synthesized nano-porous Co
2
O
3
/Cu
2
O
3
: Al
2
O
3
: SiO
2
((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h. The crystallization behavior and spectroscopic properties were investigated using X-ray diffraction, field emission-scanning electron microscopy, and Fourier-transform infrared absorption spectra analysis. The antibiotic properties of the nano-porous CAS, 5Co-CAS, and 9Co-CAS magnetic nanocomposites was studied against some potentially pathogenic bacteria in water and wastewater samples. The bacteria tested included
Escherichia coli
,
Salmonella enterica
,
Pseudomonas aeruginosa
,
Listeria monocytogenes
,
Staphylococcus aureus
,
Enterococcus faecalis
, and
Bacillus subtilis
. Incorporating Co
2
O
3
resulted in the identification of three peaks at 2θ = 10.2°, 13.4°, and 15°. The introduction of cobalt nanoparticles created a ferromagnetic behavior in the CAS nanoceramic, with the magnetic moment and saturation values increasing with increased Co
2
O
3
doping. 9Co-CAS was most potent against all the tested pathogens with minimum inhibitory concentrations of 25 mg/L within 40 min for
E. coli
and
P. aeruginosa
and 50 mg/L within 10 min for
S. enterica
; the lowest antibacterial activity was observed with the unmodified CAS. The findings revealed that the manufactured nanocomposite materials were potent disinfectants with a promising application for water and wastewater treatment. |
---|---|
AbstractList | Herein, we successfully synthesized nano-porous Co
O
/Cu
O
: Al
O
: SiO
((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h. The crystallization behavior and spectroscopic properties were investigated using X-ray diffraction, field emission-scanning electron microscopy, and Fourier-transform infrared absorption spectra analysis. The antibiotic properties of the nano-porous CAS, 5Co-CAS, and 9Co-CAS magnetic nanocomposites was studied against some potentially pathogenic bacteria in water and wastewater samples. The bacteria tested included Escherichia coli, Salmonella enterica, Pseudomonas aeruginosa, Listeria monocytogenes, Staphylococcus aureus, Enterococcus faecalis, and Bacillus subtilis. Incorporating Co
O
resulted in the identification of three peaks at 2θ = 10.2°, 13.4°, and 15°. The introduction of cobalt nanoparticles created a ferromagnetic behavior in the CAS nanoceramic, with the magnetic moment and saturation values increasing with increased Co
O
doping. 9Co-CAS was most potent against all the tested pathogens with minimum inhibitory concentrations of 25 mg/L within 40 min for E. coli and P. aeruginosa and 50 mg/L within 10 min for S. enterica; the lowest antibacterial activity was observed with the unmodified CAS. The findings revealed that the manufactured nanocomposite materials were potent disinfectants with a promising application for water and wastewater treatment. Herein, we successfully synthesized nano-porous Co 2 O 3 /Cu 2 O 3 : Al 2 O 3 : SiO 2 ((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h. The crystallization behavior and spectroscopic properties were investigated using X-ray diffraction, field emission-scanning electron microscopy, and Fourier-transform infrared absorption spectra analysis. The antibiotic properties of the nano-porous CAS, 5Co-CAS, and 9Co-CAS magnetic nanocomposites was studied against some potentially pathogenic bacteria in water and wastewater samples. The bacteria tested included Escherichia coli , Salmonella enterica , Pseudomonas aeruginosa , Listeria monocytogenes , Staphylococcus aureus , Enterococcus faecalis , and Bacillus subtilis . Incorporating Co 2 O 3 resulted in the identification of three peaks at 2θ = 10.2°, 13.4°, and 15°. The introduction of cobalt nanoparticles created a ferromagnetic behavior in the CAS nanoceramic, with the magnetic moment and saturation values increasing with increased Co 2 O 3 doping. 9Co-CAS was most potent against all the tested pathogens with minimum inhibitory concentrations of 25 mg/L within 40 min for E. coli and P. aeruginosa and 50 mg/L within 10 min for S. enterica ; the lowest antibacterial activity was observed with the unmodified CAS. The findings revealed that the manufactured nanocomposite materials were potent disinfectants with a promising application for water and wastewater treatment. Herein, we successfully synthesized nano-porous Co2O3/Cu2O3: Al2O3: SiO2 ((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h. The crystallization behavior and spectroscopic properties were investigated using X-ray diffraction, field emission-scanning electron microscopy, and Fourier-transform infrared absorption spectra analysis. The antibiotic properties of the nano-porous CAS, 5Co-CAS, and 9Co-CAS magnetic nanocomposites was studied against some potentially pathogenic bacteria in water and wastewater samples. The bacteria tested included Escherichia coli, Salmonella enterica, Pseudomonas aeruginosa, Listeria monocytogenes, Staphylococcus aureus, Enterococcus faecalis, and Bacillus subtilis. Incorporating Co2O3 resulted in the identification of three peaks at 2θ = 10.2°, 13.4°, and 15°. The introduction of cobalt nanoparticles created a ferromagnetic behavior in the CAS nanoceramic, with the magnetic moment and saturation values increasing with increased Co2O3 doping. 9Co-CAS was most potent against all the tested pathogens with minimum inhibitory concentrations of 25 mg/L within 40 min for E. coli and P. aeruginosa and 50 mg/L within 10 min for S. enterica; the lowest antibacterial activity was observed with the unmodified CAS. The findings revealed that the manufactured nanocomposite materials were potent disinfectants with a promising application for water and wastewater treatment. |
Author | Abou Hammad, Ali B. Hemdan, Bahaa A. Abia, Akebe Luther King El Nahwary, Amany M. |
Author_xml | – sequence: 1 givenname: Ali B. surname: Abou Hammad fullname: Abou Hammad, Ali B. organization: Solid-State Physics Department, Physics Research Division, National Research Centre – sequence: 2 givenname: Amany M. surname: El Nahwary fullname: El Nahwary, Amany M. organization: Solid-State Physics Department, Physics Research Division, National Research Centre – sequence: 3 givenname: Bahaa A. surname: Hemdan fullname: Hemdan, Bahaa A. email: bahaa_nrc@yahoo.com organization: Water Pollution Research Department, Environmental Research Division, National Research Centre – sequence: 4 givenname: Akebe Luther King orcidid: 0000-0002-5194-2810 surname: Abia fullname: Abia, Akebe Luther King email: lutherkinga@yahoo.fr organization: Antimicrobial Research Unit, College of Health Sciences, University of KwaZulu-Natal |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/32378108$$D View this record in MEDLINE/PubMed |
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Keywords | RT magnetization Sol-gel method Bacterial pathogens Magnetic nanoparticles Minimum inhibitory concentration SiO Water and wastewater treatment CoCuAlSi nanocomposite SiO2 |
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Snippet | Herein, we successfully synthesized nano-porous Co
2
O
3
/Cu
2
O
3
: Al
2
O
3
: SiO
2
((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at... Herein, we successfully synthesized nano-porous Co O /Cu O : Al O : SiO ((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4 h.... Herein, we successfully synthesized nano-porous Co2O3/Cu2O3: Al2O3: SiO2 ((0, 5, 7, 9) Co-CAS) using the acidic sol-gel approach and calcined at 800 °C for 4... |
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SubjectTerms | Anti-Bacterial Agents Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Carbamate pesticides Carbamates (tradename) Cholinesterase Chronic exposure Cobalt Correlation coefficients Crystallization Disease control Disinfectants E coli Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Environmental science Erythrocytes Escherichia coli Exposure Females Gynecology Inflammatory diseases Inhibitors Listeria monocytogenes Magnetic Phenomena Microbial Sensitivity Tests Nanocomposites Obstetrics Organophosphates Pelvic inflammatory disease Pesticides Research Article Silicates Silicon Dioxide Spectroscopy, Fourier Transform Infrared Waste Water Waste Water Technology Wastewater purification Wastewater treatment Water Water Management Water Pollution Control X-Ray Diffraction |
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Title | Nanoceramics and novel functionalized silicate-based magnetic nanocomposites as substitutional disinfectants for water and wastewater purification |
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