Stable and Highly Efficient Hydrogen Evolution from Seawater Enabled by an Unsaturated Nickel Surface Nitride
Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni‐SN@C) cataly...
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| Published in | Advanced materials (Weinheim) Vol. 33; no. 13; pp. e2007508 - n/a |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Wiley Subscription Services, Inc
01.04.2021
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni‐SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm−2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni‐SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni‐SN@C performs like Pt with the ability to generate hydronium ions in a high‐pH electrolyte. The catalyst operation is then demonstrated in a two‐electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm−2.
An unsaturated nickel surface nitride exhibits efficient and stable performance for hydrogen evolution from seawater. The origin of the activity and stability of the unique surface nitride is investigated using in situ Raman spectroscopy. By coupling with hydrazine oxidation at the anode, a flow‐electrolyzer is assembled that can deliver a current density of 1 A cm−2 with a small cell voltage of 0.7 V. |
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| AbstractList | Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni‐SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm−2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni‐SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni‐SN@C performs like Pt with the ability to generate hydronium ions in a high‐pH electrolyte. The catalyst operation is then demonstrated in a two‐electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm−2. Electrocatalytic production of hydrogen from seawater provides a route to low-cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni-SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm-2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni-SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni-SN@C performs like Pt with the ability to generate hydronium ions in a high-pH electrolyte. The catalyst operation is then demonstrated in a two-electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm-2 .Electrocatalytic production of hydrogen from seawater provides a route to low-cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni-SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm-2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni-SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni-SN@C performs like Pt with the ability to generate hydronium ions in a high-pH electrolyte. The catalyst operation is then demonstrated in a two-electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm-2 . Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni‐SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm−2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni‐SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni‐SN@C performs like Pt with the ability to generate hydronium ions in a high‐pH electrolyte. The catalyst operation is then demonstrated in a two‐electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm−2. An unsaturated nickel surface nitride exhibits efficient and stable performance for hydrogen evolution from seawater. The origin of the activity and stability of the unique surface nitride is investigated using in situ Raman spectroscopy. By coupling with hydrazine oxidation at the anode, a flow‐electrolyzer is assembled that can deliver a current density of 1 A cm−2 with a small cell voltage of 0.7 V. Electrocatalytic production of hydrogen from seawater provides a route to low-cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni-SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni-SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni-SN@C performs like Pt with the ability to generate hydronium ions in a high-pH electrolyte. The catalyst operation is then demonstrated in a two-electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm . Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER) using seawater is greatly hindered by the lack of active and stable catalysts. Herein, an unsaturated nickel surface nitride (Ni‐SN@C) catalyst that is active and stable for the HER in alkaline seawater is prepared. It achieves a low overpotential of 23 mV at a current density of 10 mA cm −2 in alkaline seawater electrolyte, which is superior to Pt/C. Compared to conventional transition metal nitrides or metal/metal nitride heterostructures, the Ni‐SN@C has no detectable bulk nickel nitride phase. Instead, unsaturated NiN bonding on the surface is present. In situ Raman measurements show that the Ni‐SN@C performs like Pt with the ability to generate hydronium ions in a high‐pH electrolyte. The catalyst operation is then demonstrated in a two‐electrode electrolyzer system, coupling with hydrazine oxidation at the anode. Using this system, a cell voltage of only 0.7 V is required to achieve a current density of 1 A cm −2 . |
| Author | Jin, Huanyu Tang, Cheng Slattery, Ashley Vasileff, Anthony Qiao, Shi‐Zhang Li, Laiquan Wang, Xuesi |
| Author_xml | – sequence: 1 givenname: Huanyu surname: Jin fullname: Jin, Huanyu organization: The University of Adelaide – sequence: 2 givenname: Xuesi surname: Wang fullname: Wang, Xuesi organization: The University of Adelaide – sequence: 3 givenname: Cheng surname: Tang fullname: Tang, Cheng organization: The University of Adelaide – sequence: 4 givenname: Anthony surname: Vasileff fullname: Vasileff, Anthony organization: The University of Adelaide – sequence: 5 givenname: Laiquan surname: Li fullname: Li, Laiquan organization: The University of Adelaide – sequence: 6 givenname: Ashley surname: Slattery fullname: Slattery, Ashley organization: The University of Adelaide – sequence: 7 givenname: Shi‐Zhang orcidid: 0000-0002-4568-8422 surname: Qiao fullname: Qiao, Shi‐Zhang email: s.qiao@adelaide.edu.au organization: The University of Adelaide |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/33624901$$D View this record in MEDLINE/PubMed |
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| Snippet | Electrocatalytic production of hydrogen from seawater provides a route to low‐cost and clean energy conversion. However, the hydrogen evolution reaction (HER)... Electrocatalytic production of hydrogen from seawater provides a route to low-cost and clean energy conversion. However, the hydrogen evolution reaction (HER)... |
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| SubjectTerms | Anodizing Catalysts Clean energy Current density electrocatalysis Electrolytes Energy conversion Heterostructures Hydrazines hydrogen evolution Hydrogen evolution reactions Hydrogen production Hydronium ions in situ Raman spectroscopy hydrazine oxidation Materials science Metal nitrides Nickel nickel surface nitride Oxidation Platinum Seawater Transition metals |
| Title | Stable and Highly Efficient Hydrogen Evolution from Seawater Enabled by an Unsaturated Nickel Surface Nitride |
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