Palladium dispersed in three-dimensional polyaniline networks as the catalyst for hydrogen peroxide electro-reduction in an acidic medium

A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of −0....

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Published inRSC advances Vol. 5; no. 114; pp. 948 - 9415
Main Authors Guo, Fen, Ye, Ke, Huang, Xiaomei, Gao, Yinyi, Cheng, Kui, Wang, Guiling, Cao, Dianxue
Format Journal Article
LanguageEnglish
Published 01.01.2015
Subjects
carbon fibers
catalysts
catalytic activity
Chlorofluorocarbons
dielectric spectroscopy
Electrochemical impedance spectroscopy
Electrodes
electrosynthesis
Fourier transform infrared spectroscopy
Hydrogen peroxide
Networks
Palladium
particle size
polyaniline
Polyanilines
scanning electron microscopy
silver
silver chloride
sulfuric acid
Voltammetry
X-ray diffraction
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Abstract A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of −0.4 V vs. Ag/AgCl. The particle size of the Pd coated on the polyaniline chains is gradiently distributed. The as-prepared Pd/polyaniline/CFC electrode is characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FITR) and X-ray diffraction (XRD). The hydrogen peroxide (H 2 O 2 ) electro-reduction reaction in H 2 SO 4 solutions on the Pd/polyaniline/CFC electrode is investigated using cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS). The results reveal that the electrode exhibited high catalytic activity and excellent stability in the strong oxidizing solution of H 2 O 2 and H 2 SO 4 . Polyaniline itself shows electro-catalytic activity towards H 2 O 2 to some extent involving the chemical-electrochemical (C-E) coupling mechanism. A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks.
AbstractList A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of −0.4 V vs. Ag/AgCl. The particle size of the Pd coated on the polyaniline chains is gradiently distributed. The as-prepared Pd/polyaniline/CFC electrode is characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FITR) and X-ray diffraction (XRD). The hydrogen peroxide (H₂O₂) electro-reduction reaction in H₂SO₄ solutions on the Pd/polyaniline/CFC electrode is investigated using cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS). The results reveal that the electrode exhibited high catalytic activity and excellent stability in the strong oxidizing solution of H₂O₂ and H₂SO₄. Polyaniline itself shows electro-catalytic activity towards H₂O₂ to some extent involving the chemical–electrochemical (C–E) coupling mechanism.
A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of −0.4 V vs. Ag/AgCl. The particle size of the Pd coated on the polyaniline chains is gradiently distributed. The as-prepared Pd/polyaniline/CFC electrode is characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FITR) and X-ray diffraction (XRD). The hydrogen peroxide (H 2 O 2 ) electro-reduction reaction in H 2 SO 4 solutions on the Pd/polyaniline/CFC electrode is investigated using cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS). The results reveal that the electrode exhibited high catalytic activity and excellent stability in the strong oxidizing solution of H 2 O 2 and H 2 SO 4 . Polyaniline itself shows electro-catalytic activity towards H 2 O 2 to some extent involving the chemical-electrochemical (C-E) coupling mechanism. A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks.
A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of -0.4 V vs. Ag/AgCl. The particle size of the Pd coated on the polyaniline chains is gradiently distributed. The as-prepared Pd/polyaniline/CFC electrode is characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FITR) and X-ray diffraction (XRD). The hydrogen peroxide (H2O2) electro-reduction reaction in H2SO4 solutions on the Pd/polyaniline/CFC electrode is investigated using cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS). The results reveal that the electrode exhibited high catalytic activity and excellent stability in the strong oxidizing solution of H2O2 and H2SO4. Polyaniline itself shows electro-catalytic activity towards H2O2 to some extent involving the chemical-electrochemical (C-E) coupling mechanism.
A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline matrix on the carbon fiber cloth (CFC) in the reduction state is electro-synthesized by cyclic voltammetry and has a lower vertex potential of −0.4 V vs. Ag/AgCl. The particle size of the Pd coated on the polyaniline chains is gradiently distributed. The as-prepared Pd/polyaniline/CFC electrode is characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FITR) and X-ray diffraction (XRD). The hydrogen peroxide (H 2 O 2 ) electro-reduction reaction in H 2 SO 4 solutions on the Pd/polyaniline/CFC electrode is investigated using cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS). The results reveal that the electrode exhibited high catalytic activity and excellent stability in the strong oxidizing solution of H 2 O 2 and H 2 SO 4 . Polyaniline itself shows electro-catalytic activity towards H 2 O 2 to some extent involving the chemical–electrochemical (C–E) coupling mechanism.
Author Wang, Guiling
Gao, Yinyi
Cao, Dianxue
Guo, Fen
Ye, Ke
Huang, Xiaomei
Cheng, Kui
AuthorAffiliation College of Materials Science and Chemical Engineering
Key Laboratory of Superlight Materials and Surface Technology of Ministry of Education
Harbin Engineering University
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Snippet A novel Pd/polyaniline/CFC electrode is prepared by electroless deposition of palladium (Pd) onto three-dimensional polyaniline networks. The polyaniline...
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SubjectTerms carbon fibers
catalysts
catalytic activity
Chlorofluorocarbons
dielectric spectroscopy
Electrochemical impedance spectroscopy
Electrodes
electrosynthesis
Fourier transform infrared spectroscopy
Hydrogen peroxide
Networks
Palladium
particle size
polyaniline
Polyanilines
scanning electron microscopy
silver
silver chloride
sulfuric acid
Voltammetry
X-ray diffraction
Title Palladium dispersed in three-dimensional polyaniline networks as the catalyst for hydrogen peroxide electro-reduction in an acidic medium
URI https://www.proquest.com/docview/1835599485
https://www.proquest.com/docview/2352427701
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