Microstructural and physical properties of magnesium oxide-doped silicon nitride ceramics

Silicon nitride based ceramics with aluminum, yttrium and magnesium oxides were produced by cold isostatic pressing and free sintering. The phase composition of the starting MgO powder obtained by the novel technology has been studied. The effect of magnesium oxide content on the structure of the pr...

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Published inResults in physics Vol. 6; pp. 82 - 83
Main Authors Sirota, V., Lukianova, O., Krasilnikov, V., Selemenev, V., Dokalov, V.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 2016
Elsevier
Subjects
Magnesium oxide
Silicon nitride
Structure
Structure
Magnesium oxide
Silicon nitride
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Abstract Silicon nitride based ceramics with aluminum, yttrium and magnesium oxides were produced by cold isostatic pressing and free sintering. The phase composition of the starting MgO powder obtained by the novel technology has been studied. The effect of magnesium oxide content on the structure of the produced materials has been investigated. It was found, that obtained materials with 1 and 2wt.% of magnesium oxide and without it have a typical β-silicon nitride structure with elongated grains. Ceramics with 5wt.% magnesia has a duplex α/β-structure with elongated and equiaxed grains. Ceramics with 2wt.% magnesium oxide has a maximum density of 2.91g/cm3. The increases in magnesium oxide content upto 5% led to decrease in the shrinkage (from 16% to 12%) and density (from 2.88 to 2.37g/cm3).
AbstractList Silicon nitride based ceramics with aluminum, yttrium and magnesium oxides were produced by cold isostatic pressing and free sintering. The phase composition of the starting MgO powder obtained by the novel technology has been studied. The effect of magnesium oxide content on the structure of the produced materials has been investigated. It was found, that obtained materials with 1 and 2 wt.% of magnesium oxide and without it have a typical β-silicon nitride structure with elongated grains. Ceramics with 5 wt.% magnesia has a duplex α/β-structure with elongated and equiaxed grains. Ceramics with 2 wt.% magnesium oxide has a maximum density of 2.91 g/cm3. The increases in magnesium oxide content upto 5% led to decrease in the shrinkage (from 16% to 12%) and density (from 2.88 to 2.37 g/cm3). Keywords: Silicon nitride, Magnesium oxide, Structure
Silicon nitride based ceramics with aluminum, yttrium and magnesium oxides were produced by cold isostatic pressing and free sintering. The phase composition of the starting MgO powder obtained by the novel technology has been studied. The effect of magnesium oxide content on the structure of the produced materials has been investigated. It was found, that obtained materials with 1 and 2wt.% of magnesium oxide and without it have a typical β-silicon nitride structure with elongated grains. Ceramics with 5wt.% magnesia has a duplex α/β-structure with elongated and equiaxed grains. Ceramics with 2wt.% magnesium oxide has a maximum density of 2.91g/cm3. The increases in magnesium oxide content upto 5% led to decrease in the shrinkage (from 16% to 12%) and density (from 2.88 to 2.37g/cm3).
Author Selemenev, V.
Sirota, V.
Dokalov, V.
Krasilnikov, V.
Lukianova, O.
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Title Microstructural and physical properties of magnesium oxide-doped silicon nitride ceramics
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