Eco-friendly synthesis of Fe3O4 nanoparticles: Evaluation of their catalytic activity in methylene blue degradation by kinetic adsorption models
In this work the green synthesis of Fe3O4 nanoparticles by cynara cardunculus leaf extract is presented. This green synthesis route offers a novel and eco-friendly alternative to obtaining of iron oxides nanoparticles. Functional nanoparticles with potential catalytic applications, particularly for...
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| Published in | Results in physics Vol. 12; pp. 989 - 995 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.03.2019
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | In this work the green synthesis of Fe3O4 nanoparticles by cynara cardunculus leaf extract is presented. This green synthesis route offers a novel and eco-friendly alternative to obtaining of iron oxides nanoparticles. Functional nanoparticles with potential catalytic applications, particularly for water remediation containing organic dyes were synthetized. The structural characterization of the Fe3O4 nanoparticles were carried out by scanning electron microscopy (SEM), X-ray diffraction, techniques. Calculation to obtaining the crystallite size by Williamson –Hall method were performed. Additionally, Raman spectroscopy support the Fe3O4 characterization. Posteriorly, the Fe3O4 nanoparticles were evaluated on the methylene blue degradation. Kinetic adsorption models were employed to establish the behavior during the methylene blue degradation process. Pseudo first order, Pseudo second order, Intraparticle diffusion and Elovich Models were calculated based on the experimental data obtained. Calculations as the correlation factor indicates the best linear fit between the theoretical models and the experimental data obtained during the blue methylene degradation. |
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| AbstractList | In this work the green synthesis of Fe3O4 nanoparticles by cynara cardunculus leaf extract is presented. This green synthesis route offers a novel and eco-friendly alternative to obtaining of iron oxides nanoparticles. Functional nanoparticles with potential catalytic applications, particularly for water remediation containing organic dyes were synthetized. The structural characterization of the Fe3O4 nanoparticles were carried out by scanning electron microscopy (SEM), X-ray diffraction, techniques. Calculation to obtaining the crystallite size by Williamson –Hall method were performed. Additionally, Raman spectroscopy support the Fe3O4 characterization. Posteriorly, the Fe3O4 nanoparticles were evaluated on the methylene blue degradation. Kinetic adsorption models were employed to establish the behavior during the methylene blue degradation process. Pseudo first order, Pseudo second order, Intraparticle diffusion and Elovich Models were calculated based on the experimental data obtained. Calculations as the correlation factor indicates the best linear fit between the theoretical models and the experimental data obtained during the blue methylene degradation. In this work the green synthesis of Fe3O4 nanoparticles by cynara cardunculus leaf extract is presented. This green synthesis route offers a novel and eco-friendly alternative to obtaining of iron oxides nanoparticles. Functional nanoparticles with potential catalytic applications, particularly for water remediation containing organic dyes were synthetized. The structural characterization of the Fe3O4 nanoparticles were carried out by scanning electron microscopy (SEM), X-ray diffraction, techniques. Calculation to obtaining the crystallite size by Williamson –Hall method were performed. Additionally, Raman spectroscopy support the Fe3O4 characterization. Posteriorly, the Fe3O4 nanoparticles were evaluated on the methylene blue degradation. Kinetic adsorption models were employed to establish the behavior during the methylene blue degradation process. Pseudo first order, Pseudo second order, Intraparticle diffusion and Elovich Models were calculated based on the experimental data obtained. Calculations as the correlation factor indicates the best linear fit between the theoretical models and the experimental data obtained during the blue methylene degradation. Keywords: Green synthesis, Fe3O4 nanoparticles, Kinetic adsorption models, Methylene blue degradation |
| Author | Pérez, Ramiro Mondragón-Sánchez, María de Lourdes Robles-Cortés, Anel Ivonne Ruíz-Baltazar, Álvaro de Jesús Reyes-López, Simón Yobanny |
| Author_xml | – sequence: 1 givenname: Álvaro de Jesús surname: Ruíz-Baltazar fullname: Ruíz-Baltazar, Álvaro de Jesús email: aruizbaltazar@fata.unam.mx organization: CONACYT-Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Santiago de Querétaro, Querétaro C.P. 76230, Mexico – sequence: 2 givenname: Simón Yobanny surname: Reyes-López fullname: Reyes-López, Simón Yobanny email: simon.reyes@uacj.mx organization: Instituto de Ciencias Biomédicas, Universidad Autónoma de Ciudad Juárez, Estocolmo s/n, Ciudad Juárez, Chihuahua C.P. 32300, Mexico – sequence: 3 givenname: María de Lourdes surname: Mondragón-Sánchez fullname: Mondragón-Sánchez, María de Lourdes organization: Tecnológico Nacional de México/Instituto Tecnológico de Morelia, Posgrado en Metalúrgia, Av. Tecnológico 1500, col, Lomas de Santiaguito, C.P. 58120 Morelia, MICH, Mexico – sequence: 4 givenname: Anel Ivonne surname: Robles-Cortés fullname: Robles-Cortés, Anel Ivonne organization: Tecnológico Nacional de México/Instituto Tecnológico de Morelia, Posgrado en Metalúrgia, Av. Tecnológico 1500, col, Lomas de Santiaguito, C.P. 58120 Morelia, MICH, Mexico – sequence: 5 givenname: Ramiro surname: Pérez fullname: Pérez, Ramiro organization: Instituto de Ciencias Físicas, Universidad Nacional Autónoma de México, Av. Universidad s/n, Col. Chamilpa, Cuernavaca, MOR 62210, Mexico |
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| Keywords | Green synthesis Kinetic adsorption models Methylene blue degradation Fe3O4 nanoparticles |
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| Title | Eco-friendly synthesis of Fe3O4 nanoparticles: Evaluation of their catalytic activity in methylene blue degradation by kinetic adsorption models |
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