A near-ambient-pressure XPS study on catalytic CO oxidation reaction over a Ru(101¯0) surface

We investigated the interactions of CO and O2 with Ru(101¯0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface under near realistic pressure conditions by using a combination of near-ambient-pressure x-ray photoelectron spectroscopy and differential p...

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Published in	Surface science Vol. 621; pp. 128 - 132
Main Authors	Toyoshima, Ryo, Shimura, Masahiro, Yoshida, Masaaki, Monya, Yuji, Suzuki, Kazuma, Amemiya, Kenta, Mase, Kazuhiko, Mun, Bongjin Simon, Kondoh, Hiroshi
Format	Journal Article
Language	English
Published	Kidlington Elsevier B.V 01.03.2014 Elsevier
Subjects	Carbon dioxide Carbon monoxide Catalysis Catalysts CO oxidation Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Exact sciences and technology Mass spectroscopy Near-ambient-pressure XPS Oxidation Oxides Physics Ru([formula omitted]) X-ray photoelectron spectroscopy Mass spectroscopy Ru(101¯0) Catalysis CO oxidation Near-ambient-pressure XPS Catalytic reaction Ru Oxidation X-ray photoelectron spectra
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Abstract	We investigated the interactions of CO and O2 with Ru(101¯0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface under near realistic pressure conditions by using a combination of near-ambient-pressure x-ray photoelectron spectroscopy and differential pumping mass spectroscopy. At lower temperatures (T<190°C), most of the surface keeps metallic and is covered by both chemisorbed atomic oxygen and CO, and the CO2 formation rate is relatively slow. At higher temperatures, the reaction rate significantly increases and reaches the saturation, where the Ru surface is dominated by a bulk oxide (i.e. RuO2). [Display omitted] •CO exposure onto Ru(101¯0) with ambient pressure causes partial dissociation of CO.•Catalytic CO oxidation reaction was studied by in-situ NAP-XPS and mass measurements.•Thin layer of the RuO2 bulk oxide on Ru(101¯0) is a catalytically active phase.
AbstractList	We investigated the interactions of CO and O2 with Ru(101¯0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface under near realistic pressure conditions by using a combination of near-ambient-pressure x-ray photoelectron spectroscopy and differential pumping mass spectroscopy. At lower temperatures (T<190°C), most of the surface keeps metallic and is covered by both chemisorbed atomic oxygen and CO, and the CO2 formation rate is relatively slow. At higher temperatures, the reaction rate significantly increases and reaches the saturation, where the Ru surface is dominated by a bulk oxide (i.e. RuO2). [Display omitted] •CO exposure onto Ru(101¯0) with ambient pressure causes partial dissociation of CO.•Catalytic CO oxidation reaction was studied by in-situ NAP-XPS and mass measurements.•Thin layer of the RuO2 bulk oxide on Ru(101¯0) is a catalytically active phase. We investigated the interactions of CO and O sub(2) with Ru(1010) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface under near realistic pressure conditions by using a combination of near-ambient-pressure x-ray photoelectron spectroscopy and differential pumping mass spectroscopy. At lower temperatures (T < 190 [degrees]C), most of the surface keeps metallic and is covered by both chemisorbed atomic oxygen and CO, and the CO sub(2) formation rate is relatively slow. At higher temperatures, the reaction rate significantly increases and reaches the saturation, where the Ru surface is dominated by a bulk oxide (i.e. RuO sub(2)). We investigated the interactions of CO and O2 with Ru(101[macr]0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface under near realistic pressure conditions by using a combination of near-ambient-pressure x-ray photoelectron spectroscopy and differential pumping mass spectroscopy. At lower temperatures (T < 190 degree C), most of the surface keeps metallic and is covered by both chemisorbed atomic oxygen and CO, and the CO2 formation rate is relatively slow. At higher temperatures, the reaction rate significantly increases and reaches the saturation, where the Ru surface is dominated by a bulk oxide (i.e. RuO2).
Author	Yoshida, Masaaki Monya, Yuji Mase, Kazuhiko Suzuki, Kazuma Amemiya, Kenta Mun, Bongjin Simon Toyoshima, Ryo Kondoh, Hiroshi Shimura, Masahiro
Author_xml	– sequence: 1 givenname: Ryo surname: Toyoshima fullname: Toyoshima, Ryo organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan – sequence: 2 givenname: Masahiro orcidid: 0000-0001-5310-3888 surname: Shimura fullname: Shimura, Masahiro organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan – sequence: 3 givenname: Masaaki surname: Yoshida fullname: Yoshida, Masaaki organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan – sequence: 4 givenname: Yuji surname: Monya fullname: Monya, Yuji organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan – sequence: 5 givenname: Kazuma surname: Suzuki fullname: Suzuki, Kazuma organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan – sequence: 6 givenname: Kenta surname: Amemiya fullname: Amemiya, Kenta organization: Institute of Materials Structure Science, High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba, Ibaraki 305-0801, Japan – sequence: 7 givenname: Kazuhiko surname: Mase fullname: Mase, Kazuhiko organization: Institute of Materials Structure Science, High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba, Ibaraki 305-0801, Japan – sequence: 8 givenname: Bongjin Simon surname: Mun fullname: Mun, Bongjin Simon organization: Department of Physics and Photon Science, Gwangju Institute of Science and Technology, Gwangju 500-712, Republic of Korea – sequence: 9 givenname: Hiroshi surname: Kondoh fullname: Kondoh, Hiroshi email: kondoh@chem.keio.ac.jp organization: Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa 223-8522, Japan
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Keywords	Mass spectroscopy Ru(101¯0) Catalysis CO oxidation Near-ambient-pressure XPS Catalytic reaction Ru Oxidation X-ray photoelectron spectra
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Snippet	We investigated the interactions of CO and O2 with Ru(101¯0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the surface... We investigated the interactions of CO and O2 with Ru(101[macr]0) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the... We investigated the interactions of CO and O sub(2) with Ru(1010) single crystal surfaces, and studied the in-situ catalytic oxidation reaction of CO on the...
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SubjectTerms	Carbon dioxide Carbon monoxide Catalysis Catalysts CO oxidation Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Exact sciences and technology Mass spectroscopy Near-ambient-pressure XPS Oxidation Oxides Physics Ru([formula omitted]) X-ray photoelectron spectroscopy
Title	A near-ambient-pressure XPS study on catalytic CO oxidation reaction over a Ru(101¯0) surface
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