Vibrational Circular Dichroism Spectroscopy toward Intercalation Compounds of Sodium Montmorillonite: Evidences for Molecular Packing of Enantiopure Monovalent Ir(III) Complexes within Interlayer Spaces
Solid state vibrational circular dichroism (SD-VCD) spectra were recorded on the intercalation compounds of sodium montmorillonite with a chiral iridium(III) complex. The complex used was Δ- (or Λ-)[Ir(bzq)2(phen)]+ (bzqH = benzo[h]quinoline; phen = 1,10-phenanthroline). The complex formed mono- or...
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Published in | Applied clay science Vol. 228; p. 106621 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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01.10.2022
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Abstract | Solid state vibrational circular dichroism (SD-VCD) spectra were recorded on the intercalation compounds of sodium montmorillonite with a chiral iridium(III) complex. The complex used was Δ- (or Λ-)[Ir(bzq)2(phen)]+ (bzqH = benzo[h]quinoline; phen = 1,10-phenanthroline). The complex formed mono- or bi-molecular layers in interlayer spaces, depending on the adsorption amount to 50% or 100% cation exchange capacity (CEC), respectively. Notably, the VCD signals were sensitive enough to reveal the detailed molecular interactions in adsorption layers. Signal enhancement was achieved by the coherent delocalization of vibrational motions over tightly bound associates. Models of molecular packing were proposed with the help of theoretical simulations.
Intensity of a VCD signal reflected molecular packing in the intercalation states of three-bladed propeller-type iridium(III) complexes. [Display omitted]
•Mono- or bi-molecular layers were formed by enantiopure complexes at 50 or 100% CEC loading.•The packing structures of monovalent intercalated Ir(III) complexes were investigated by VCD.•VCD signals were sensitive enough to reflect intermolecular interactions. |
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AbstractList | Solid state vibrational circular dichroism (SD-VCD) spectra were recorded on the intercalation compounds of sodium montmorillonite with a chiral iridium(III) complex. The complex used was Δ- (or Λ-)[Ir(bzq)2(phen)]+ (bzqH = benzo[h]quinoline; phen = 1,10-phenanthroline). The complex formed mono- or bi-molecular layers in interlayer spaces, depending on the adsorption amount to 50% or 100% cation exchange capacity (CEC), respectively. Notably, the VCD signals were sensitive enough to reveal the detailed molecular interactions in adsorption layers. Signal enhancement was achieved by the coherent delocalization of vibrational motions over tightly bound associates. Models of molecular packing were proposed with the help of theoretical simulations.
Intensity of a VCD signal reflected molecular packing in the intercalation states of three-bladed propeller-type iridium(III) complexes. [Display omitted]
•Mono- or bi-molecular layers were formed by enantiopure complexes at 50 or 100% CEC loading.•The packing structures of monovalent intercalated Ir(III) complexes were investigated by VCD.•VCD signals were sensitive enough to reflect intermolecular interactions. |
ArticleNumber | 106621 |
Author | Sato, Hisako Yamagishi, Akihiko Hara, Mitsuo Takimoto, Kazuyoshi Yoshida, Jun |
Author_xml | – sequence: 1 givenname: Hisako surname: Sato fullname: Sato, Hisako email: sato.hisako.my@ehime-u.ac.jp organization: Ehime University, Graduate School of Science and Engineering, 2-5 Bunkyo-chou, Matsuyama, Ehime 790-8577, Japan – sequence: 2 givenname: Kazuyoshi surname: Takimoto fullname: Takimoto, Kazuyoshi organization: Ehime University, Graduate School of Science and Engineering, 2-5 Bunkyo-chou, Matsuyama, Ehime 790-8577, Japan – sequence: 3 givenname: Akihiko surname: Yamagishi fullname: Yamagishi, Akihiko organization: Toho University, School of Medicine, Ota-ku, Tokyo 143-8540, Japan – sequence: 4 givenname: Jun surname: Yoshida fullname: Yoshida, Jun organization: Nihon University, Department of Chemistry, College of Humanities & Sciences, 3-25-40 Sakurajosui, Setagaya-ku, Tokyo 156-8550, Japan – sequence: 5 givenname: Mitsuo surname: Hara fullname: Hara, Mitsuo organization: Nagoya University, Department of Molecular and Macromolecular Chemistry, Graduate School of Engineering, Furo-cho, Chikusa-ku, Nagoya 464-8603, Japan |
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CitedBy_id | crossref_primary_10_1016_j_clay_2024_107290 crossref_primary_10_1016_j_clay_2023_107108 crossref_primary_10_1016_j_saa_2024_123851 |
Cites_doi | 10.1016/S1389-5567(00)00008-3 10.1021/ja00289a051 10.1039/C9CC00164F 10.1246/cl.161043 10.1016/0169-1317(96)00010-5 10.1346/CCMN.2012.0600407 10.1039/C7CP02544K 10.1039/C7DT00606C 10.1021/acs.langmuir.7b00512 10.1016/j.saa.2021.120761 10.1021/acs.analchem.0c02990 10.1039/b009939m 10.1039/D0CP00713G 10.1021/acs.chemrev.9b00636 10.1016/S0924-2031(02)00065-6 10.1039/D0CC04977H 10.1016/j.clay.2014.04.010 10.1039/C7NJ04688J 10.1021/acs.jpclett.1c01682 10.1246/bcsj.20210101 10.1346/CCMN.1991.0390603 10.1021/cr00034a005 10.1039/C7CP05114J |
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Keywords | Montmorillonite Iridium complex Vibrational circular dichroism |
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Snippet | Solid state vibrational circular dichroism (SD-VCD) spectra were recorded on the intercalation compounds of sodium montmorillonite with a chiral iridium(III)... |
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SubjectTerms | Iridium complex Montmorillonite Vibrational circular dichroism |
Title | Vibrational Circular Dichroism Spectroscopy toward Intercalation Compounds of Sodium Montmorillonite: Evidences for Molecular Packing of Enantiopure Monovalent Ir(III) Complexes within Interlayer Spaces |
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