Mechanochemical Pretreatment for Efficient Solvent‐Free Synthesis of SSZ‐13 Zeolite
The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill. Contrary to manual grinding in a mortar, the proposed automatized approach is scalable and reproducible. This solvent‐free process provided a hu...
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| Published in | Chemistry : a European journal Vol. 25; no. 52; pp. 12068 - 12073 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
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18.09.2019
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| Abstract | The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill. Contrary to manual grinding in a mortar, the proposed automatized approach is scalable and reproducible. This solvent‐free process provided a huge gain in product/gel ratios, significantly minimized reaction space and organic structure‐directing agent use, and allowed for the elimination of agitation. Obtained materials were comparable to the product of “classical” syntheses. The use of different silica sources resulted in SSZ‐13 zeolites with various characteristics: different Si/Al ratio and crystal size.
Activation by milling led to the solvent‐free synthesis of SSZ‐13 zeolite with a huge gain in terms of product/gel ratio. The automatized pretreatment process performed by planetary mill resulted in successful synthesis, whereas the manual mechanochemical approach failed. |
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| AbstractList | The economical and environmentally benign synthesis of SSZ-13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill. Contrary to manual grinding in a mortar, the proposed automatized approach is scalable and reproducible. This solvent-free process provided a huge gain in product/gel ratios, significantly minimized reaction space and organic structure-directing agent use, and allowed for the elimination of agitation. Obtained materials were comparable to the product of "classical" syntheses. The use of different silica sources resulted in SSZ-13 zeolites with various characteristics: different Si/Al ratio and crystal size. Abstract The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill. Contrary to manual grinding in a mortar, the proposed automatized approach is scalable and reproducible. This solvent‐free process provided a huge gain in product/gel ratios, significantly minimized reaction space and organic structure‐directing agent use, and allowed for the elimination of agitation. Obtained materials were comparable to the product of “classical” syntheses. The use of different silica sources resulted in SSZ‐13 zeolites with various characteristics: different Si/Al ratio and crystal size. The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill. Contrary to manual grinding in a mortar, the proposed automatized approach is scalable and reproducible. This solvent‐free process provided a huge gain in product/gel ratios, significantly minimized reaction space and organic structure‐directing agent use, and allowed for the elimination of agitation. Obtained materials were comparable to the product of “classical” syntheses. The use of different silica sources resulted in SSZ‐13 zeolites with various characteristics: different Si/Al ratio and crystal size. Activation by milling led to the solvent‐free synthesis of SSZ‐13 zeolite with a huge gain in terms of product/gel ratio. The automatized pretreatment process performed by planetary mill resulted in successful synthesis, whereas the manual mechanochemical approach failed. |
| Author | Tokarova, Venceslava Klein, Petr Mlekodaj, Kinga Dedecek, Jiri Zouzelka, Radek Pashkova, Veronika Brabec, Libor Rathousky, Jiri |
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| Snippet | The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill.... The economical and environmentally benign synthesis of SSZ-13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary mill.... Abstract The economical and environmentally benign synthesis of SSZ‐13 zeolite was possible due to the mechanochemical activation of dry reagents by planetary... |
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| SubjectTerms | Aluminum Chemistry Grinding mills mechanochemistry Mortars (material) planetary mill Planetary mills Pretreatment Reagents Silica Silicon dioxide solvent-free Solvents Synthesis Zeolites |
| Title | Mechanochemical Pretreatment for Efficient Solvent‐Free Synthesis of SSZ‐13 Zeolite |
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