Effect of Temperature and Chloride Concentration on the Anodic Formation of Nanoporous Gold Films in Chloride Solutions
The preparation of nanoporous gold (NPG) has been the subject of extensive research, and the anodization of Au in chloride solutions has received recent attention as an efficient and time‐saving method. In the present work, the effects of reaction temperature and Cl– concentration on the anodic form...
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| Published in | Bulletin of the Korean Chemical Society Vol. 36; no. 9; pp. 2337 - 2343 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Weinheim
Wiley-VCH Verlag GmbH & Co. KGaA
01.09.2015
Wiley‐VCH Verlag GmbH & Co. KGaA 대한화학회 |
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| Abstract | The preparation of nanoporous gold (NPG) has been the subject of extensive research, and the anodization of Au in chloride solutions has received recent attention as an efficient and time‐saving method. In the present work, the effects of reaction temperature and Cl– concentration on the anodic formation of NPG structures were investigated. The anodization efficiency was evaluated in terms of the roughness factor (R
f) of NPG layers, which varied as a function of these two reaction parameters. The R
f of NPG gradually increased with temperature up to 40 °C and then leveled off at higher temperatures. In terms of Cl– concentration, 1.0 M yielded the maximum R
f of the NPG. The dependence of the anodization efficiency on the two reaction parameters was examined with regard to the electrochemical dissolution of Au as well as the formation of Au–Cl complexes and protective surface oxide layers. The mechanistic aspects of the anodic formation of NPG give insight into the efficient preparation of highly porous NPG structures. |
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| AbstractList | The preparation of nanoporous gold (NPG) has been the subject of extensive research, and the anodization of Au in chloride solutions has received recent attention as an efficient and time‐saving method. In the present work, the effects of reaction temperature and Cl– concentration on the anodic formation of NPG structures were investigated. The anodization efficiency was evaluated in terms of the roughness factor (R
f) of NPG layers, which varied as a function of these two reaction parameters. The R
f of NPG gradually increased with temperature up to 40 °C and then leveled off at higher temperatures. In terms of Cl– concentration, 1.0 M yielded the maximum R
f of the NPG. The dependence of the anodization efficiency on the two reaction parameters was examined with regard to the electrochemical dissolution of Au as well as the formation of Au–Cl complexes and protective surface oxide layers. The mechanistic aspects of the anodic formation of NPG give insight into the efficient preparation of highly porous NPG structures. The preparation of nanoporous gold ( NPG ) has been the subject of extensive research, and the anodization of Au in chloride solutions has received recent attention as an efficient and time‐saving method. In the present work, the effects of reaction temperature and Cl – concentration on the anodic formation of NPG structures were investigated. The anodization efficiency was evaluated in terms of the roughness factor ( R f ) of NPG layers, which varied as a function of these two reaction parameters. The R f of NPG gradually increased with temperature up to 40 °C and then leveled off at higher temperatures. In terms of Cl – concentration, 1.0 M yielded the maximum R f of the NPG . The dependence of the anodization efficiency on the two reaction parameters was examined with regard to the electrochemical dissolution of Au as well as the formation of Au–Cl complexes and protective surface oxide layers. The mechanistic aspects of the anodic formation of NPG give insight into the efficient preparation of highly porous NPG structures. The preparation of nanoporous gold (NPG) has been the subject of extensive research, and the anodization of Au in chloride solutions has received recent attention as an efficient and time-saving method. In the present work, the effects of reaction temperature and Cl– concentration on the anodic formation of NPG structures were investigated. The anodization efficiency was evaluated in terms of the roughness factor (Rf) of NPG layers, which varied as a function of these two reaction parameters. The R f of NPG gradually increased with temperature up to 40 °C and then leveled off at higher temperatures. In terms of Cl– concentration, 1.0 M yielded the maximum R f of the NPG. The dependence of the anodization efficiency on the two reaction parameters was examined with regard to the electrochemical dissolution of Au as well as the formation of Au–Cl complexes and protective surface oxide layers. The mechanistic aspects of the anodic formation of NPG give insight into the efficient preparation of highly porous NPG structures. KCI Citation Count: 5 |
| Author | Kim, Jongwon Kim, Minju Lee, Euna Jeong, Hwakyeung |
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| CitedBy_id | crossref_primary_10_1002_bkcs_12528 crossref_primary_10_5796_electrochemistry_20_00079 crossref_primary_10_1002_elan_201800252 crossref_primary_10_1002_elan_201800867 crossref_primary_10_1002_adem_201800574 |
| Cites_doi | 10.1002/adma.200400792 10.1002/elan.200900514 10.1007/BF03215452 10.1038/35068529 10.1149/2.0551409jes 10.1351/pac199163050711 10.1021/cm701939v 10.1038/nmat3391 10.1149/1.2124085 10.1016/j.elecom.2008.03.003 10.1016/j.electacta.2012.07.040 10.1016/j.bios.2011.01.044 10.1021/ac8017197 10.1021/nn201443p 10.1039/c2an35294j 10.1515/zpch-1965-22910 10.1021/j100393a002 10.1021/ac0507035 10.1002/anie.201005700 10.1021/la500732z 10.1016/0022-0728(93)87035-T 10.1126/science.1183591 10.1016/j.apsusc.2014.01.082 10.1016/j.jcat.2007.10.017 |
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| SubjectTerms | Anodization Chloride concentration Nanoporous gold Temperature 화학 |
| Title | Effect of Temperature and Chloride Concentration on the Anodic Formation of Nanoporous Gold Films in Chloride Solutions |
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