Preferential Cation Vacancies in Perovskite Hydroxide for the Oxygen Evolution Reaction
The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacan...
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| Published in | Angewandte Chemie International Edition Vol. 57; no. 28; pp. 8691 - 8696 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Wiley Subscription Services, Inc
09.07.2018
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| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1433-7851 1521-3773 1521-3773 |
| DOI | 10.1002/anie.201805520 |
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| Abstract | The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies‐rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X‐ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH)4. The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance.
Argon plasma can ensure preferential Sn vacancies on the surface of SnCoFe perovskite hydroxide, which exhibits a much higher current density and a lower overpotential for the oxygen evolution reaction. |
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| AbstractList | The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies‐rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X‐ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH)4. The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance. The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies-rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X-ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH)4 . The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance.The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies-rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X-ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH)4 . The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance. The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies-rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X-ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH) . The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance. The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies‐rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X‐ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH) 4 . The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance. The oxygen evolution reaction (OER) is an ideal model to study the relationship between the activity and the surface properties of catalysts. Defect engineering has been extensively developed to tune the electrocatalytic activity for OER. Compared to the anion vacancies in metal oxides, cation vacancies are more challenging to selectively generate, and the insight into the structure and activity of cation vacancies‐rich catalysts are lacked. Herein, using SnCoFe perovskite hydroxide as a precursor, abundant Sn vacancies on the surface were preferentially produced by Ar plasma. Sn vacancies could be preferentially produced as confirmed by the X‐ray absorption spectra, probably owing to the lower lattice energy and weaker chemical bonds of Sn(OH)4. The Sn vacancies promoted the exposure of active CoFe sites, resulting in an amorphous surface layer, modulated the conductivity, and thus enhanced the OER performance. Argon plasma can ensure preferential Sn vacancies on the surface of SnCoFe perovskite hydroxide, which exhibits a much higher current density and a lower overpotential for the oxygen evolution reaction. |
| Author | Hao, Li Qiao, Man Chen, Dawei Lu, Ying‐Rui Wang, Shuangyin Li, Yafei Liu, Dongdong Dong, Chung‐Li |
| Author_xml | – sequence: 1 givenname: Dawei surname: Chen fullname: Chen, Dawei organization: Hunan University – sequence: 2 givenname: Man surname: Qiao fullname: Qiao, Man organization: Nanjing Normal University – sequence: 3 givenname: Ying‐Rui surname: Lu fullname: Lu, Ying‐Rui organization: Tamkang University – sequence: 4 givenname: Li surname: Hao fullname: Hao, Li organization: Hunan University – sequence: 5 givenname: Dongdong surname: Liu fullname: Liu, Dongdong organization: Hunan University – sequence: 6 givenname: Chung‐Li surname: Dong fullname: Dong, Chung‐Li email: cldong@mail.tku.edu.tw organization: Tamkang University – sequence: 7 givenname: Yafei surname: Li fullname: Li, Yafei email: liyafei@njnu.edu.cn organization: Nanjing Normal University – sequence: 8 givenname: Shuangyin orcidid: 0000-0001-7185-9857 surname: Wang fullname: Wang, Shuangyin email: shuangyinwang@hnu.edu.cn organization: Hunan University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29771458$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | Absorption spectra Bonding strength Catalysis Catalysts Cations Chemical bonds defects electrocatalysts Lattice vacancies Organic chemistry Oxides Oxygen oxygen evolution reaction Oxygen evolution reactions Perovskites Surface layers Surface properties vacancies |
| Title | Preferential Cation Vacancies in Perovskite Hydroxide for the Oxygen Evolution Reaction |
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