Molecularly imprinted polymer functionalized flower-like BiOBr microspheres for photoelectrochemical sensing of chloramphenicol
In this study, an ultrasensitive photoelectrochemical (PEC) sensor showing a high selectivity to for chloramphenicol (CAP) was successfully constructed, based on the molecularly imprinted polymers (MIPs) functionalized photoelectrochemically active materials. The 3D flower-like BiOBr with large spec...
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| Published in | Electrochimica acta Vol. 344; p. 136161 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
01.06.2020
Elsevier BV |
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| Abstract | In this study, an ultrasensitive photoelectrochemical (PEC) sensor showing a high selectivity to for chloramphenicol (CAP) was successfully constructed, based on the molecularly imprinted polymers (MIPs) functionalized photoelectrochemically active materials. The 3D flower-like BiOBr with large specific surface area was synthesized by a simple hydrothermal process and was employed as a matrix to graft the MIPs recognition element (denoted as MIPs-PEC). SEM, TEM, FTIR, XPS, XRD and UV–vis spectroscopy were used to investigate the microstructure characteristics of the as-obtained MIPs-PEC sensor. During the PEC sensing process, MIPs were prepared via a simple thermal polymerization process provided numerous recognition sites, which improved the sensor’s selectivity to CAP. The results showed that photocurrent response signal generated by photo-induced MIPs/BrOBr/ITO electrodes was proportional to the logarithm of CAP concentration over the range from 1.00 ⅹ 10−2 to 1.00 ⅹ 103 ng mL−1 with a low detection limit is 3.02 pg mL−1 (S/N = 3). MIPs-PEC sensor exhibited high selectivity and stability, low cost, and applicability to the determination of CAP in real samples.
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•A rapid and ultrasensitive signal-off MIPs-PEC sensor developed for CAP detection.•3D flower-sphere BiOBr with large specific surface area was successfully synthesized.•The first smart integration of BiOBr with MIPs fabricating a novel PEC sensing platform.•This method has high selectivity and can be applied to thedetermination of CAP in water. |
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| AbstractList | In this study, an ultrasensitive photoelectrochemical (PEC) sensor showing a high selectivity to for chloramphenicol (CAP) was successfully constructed, based on the molecularly imprinted polymers (MIPs) functionalized photoelectrochemically active materials. The 3D flower-like BiOBr with large specific surface area was synthesized by a simple hydrothermal process and was employed as a matrix to graft the MIPs recognition element (denoted as MIPs-PEC). SEM, TEM, FTIR, XPS, XRD and UV–vis spectroscopy were used to investigate the microstructure characteristics of the as-obtained MIPs-PEC sensor. During the PEC sensing process, MIPs were prepared via a simple thermal polymerization process provided numerous recognition sites, which improved the sensor’s selectivity to CAP. The results showed that photocurrent response signal generated by photo-induced MIPs/BrOBr/ITO electrodes was proportional to the logarithm of CAP concentration over the range from 1.00 ⅹ 10−2 to 1.00 ⅹ 103 ng mL−1 with a low detection limit is 3.02 pg mL−1 (S/N = 3). MIPs-PEC sensor exhibited high selectivity and stability, low cost, and applicability to the determination of CAP in real samples.
[Display omitted]
•A rapid and ultrasensitive signal-off MIPs-PEC sensor developed for CAP detection.•3D flower-sphere BiOBr with large specific surface area was successfully synthesized.•The first smart integration of BiOBr with MIPs fabricating a novel PEC sensing platform.•This method has high selectivity and can be applied to thedetermination of CAP in water. In this study, an ultrasensitive photoelectrochemical (PEC) sensor showing a high selectivity to for chloramphenicol (CAP) was successfully constructed, based on the molecularly imprinted polymers (MIPs) functionalized photoelectrochemically active materials. The 3D flower-like BiOBr with large specific surface area was synthesized by a simple hydrothermal process and was employed as a matrix to graft the MIPs recognition element (denoted as MIPs-PEC). SEM, TEM, FTIR, XPS, XRD and UV–vis spectroscopy were used to investigate the microstructure characteristics of the as-obtained MIPs-PEC sensor. During the PEC sensing process, MIPs were prepared via a simple thermal polymerization process provided numerous recognition sites, which improved the sensor's selectivity to CAP. The results showed that photocurrent response signal generated by photo-induced MIPs/BrOBr/ITO electrodes was proportional to the logarithm of CAP concentration over the range from 1.00 ⅹ 10−2 to 1.00 ⅹ 103 ng mL−1 with a low detection limit is 3.02 pg mL−1 (S/N = 3). MIPs-PEC sensor exhibited high selectivity and stability, low cost, and applicability to the determination of CAP in real samples. |
| ArticleNumber | 136161 |
| Author | Wang, Yuping Zhou, Haifei Zhang, Zheng Jiang, Caiyun |
| Author_xml | – sequence: 1 givenname: Zheng surname: Zhang fullname: Zhang, Zheng organization: School of Chemistry and Material Science, Jiangsu Provincial Key Laboratory of Materials Cycling and Pollution Control, Nanjing Normal University, Nanjing, 210046, China – sequence: 2 givenname: Haifei surname: Zhou fullname: Zhou, Haifei organization: School of Chemistry and Material Science, Jiangsu Provincial Key Laboratory of Materials Cycling and Pollution Control, Nanjing Normal University, Nanjing, 210046, China – sequence: 3 givenname: Caiyun surname: Jiang fullname: Jiang, Caiyun organization: Department of Engineering and Technology, Jiangsu Institute of Commerce, Nanjing, 211168, China – sequence: 4 givenname: Yuping surname: Wang fullname: Wang, Yuping email: wangyuping@njnu.edu.cn organization: School of Chemistry and Material Science, Jiangsu Provincial Key Laboratory of Materials Cycling and Pollution Control, Nanjing Normal University, Nanjing, 210046, China |
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| Keywords | Photoelectrochemical sensing Chloramphenicol Molecularly imprinted polymers Flower-like BiOBr |
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| SubjectTerms | Chloramphenicol Chloromycetin Flower-like BiOBr Imprinted polymers Microspheres Molecularly imprinted polymers Photoelectric effect Photoelectric emission Photoelectrochemical sensing Recognition Selectivity Sensors Three dimensional flow X ray photoelectron spectroscopy |
| Title | Molecularly imprinted polymer functionalized flower-like BiOBr microspheres for photoelectrochemical sensing of chloramphenicol |
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