Direct synthesis of unimodal and bimodal nanoporous carbon
Unimodal and bimodal nanoporous (mesoporous) carbons have been synthesized by simply removing silica from carbon/silica nanocomposites. The sucrose/silica nanocomposites are directly prepared by the sol–gel process of tetraethyl orthosilicate (TEOS) with or without colloidal silica particles in the...
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| Published in | Microporous and mesoporous materials Vol. 74; no. 1; pp. 73 - 78 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier Inc
20.09.2004
Elsevier |
| Subjects | |
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| Abstract | Unimodal and bimodal nanoporous (mesoporous) carbons have been synthesized by simply removing silica from carbon/silica nanocomposites. The sucrose/silica nanocomposites are directly prepared by the sol–gel process of tetraethyl orthosilicate (TEOS) with or without colloidal silica particles in the presence of carbon precursor molecules (i.e., sucrose). Subsequent carbonization converts the sucrose/silica nanocomposites into nonporous carbon/silica composites. Removal of the silica templates results in nanoporous carbons with high surface areas (e.g., >1500 m
2/g) and pore volumes (e.g., >1.0 cm
3/g). Using TEOS as the only silica source, nanoporous carbons with unimodal ∼2 nm worm-like pores are produced. Nanoporous carbons with bimodal ∼2 and ∼27 nm diameter pores have been prepared by using both the TEOS-derived silica network and the colloidal silica particles as templates. |
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| AbstractList | Unimodal and bimodal nanoporous (mesoporous) carbons have been synthesized by simply removing silica from carbon/silica nanocomposites. The sucrose/silica nanocomposites are directly prepared by the sol–gel process of tetraethyl orthosilicate (TEOS) with or without colloidal silica particles in the presence of carbon precursor molecules (i.e., sucrose). Subsequent carbonization converts the sucrose/silica nanocomposites into nonporous carbon/silica composites. Removal of the silica templates results in nanoporous carbons with high surface areas (e.g., >1500 m
2/g) and pore volumes (e.g., >1.0 cm
3/g). Using TEOS as the only silica source, nanoporous carbons with unimodal ∼2 nm worm-like pores are produced. Nanoporous carbons with bimodal ∼2 and ∼27 nm diameter pores have been prepared by using both the TEOS-derived silica network and the colloidal silica particles as templates. |
| Author | Lu, Yunfeng Hu, Qingyuan Pang, Jiebin Eric Hampsey, J. Wu, Zhiwang He, Jibao |
| Author_xml | – sequence: 1 givenname: Jiebin surname: Pang fullname: Pang, Jiebin email: jpang@tulane.edu organization: Department of Chemical and Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA – sequence: 2 givenname: Qingyuan surname: Hu fullname: Hu, Qingyuan organization: Department of Chemical and Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA – sequence: 3 givenname: Zhiwang surname: Wu fullname: Wu, Zhiwang organization: Department of Chemical and Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA – sequence: 4 givenname: J. surname: Eric Hampsey fullname: Eric Hampsey, J. organization: Department of Chemical and Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA – sequence: 5 givenname: Jibao surname: He fullname: He, Jibao organization: Microscopy Lab, Coordinated Instrumentation Facility, Tulane University, New Orleans, LA 70118, USA – sequence: 6 givenname: Yunfeng surname: Lu fullname: Lu, Yunfeng email: ylu@tulane.edu organization: Department of Chemical and Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA |
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| Keywords | Hierarchical Bimodal Nanoporous carbon Templating synthesis Unimodal Scanning electron microscopy Adsorption isotherm Nitrogen Carbon Porous material Silica Transmission electron microscopy Synthesis Nanocomposite |
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| Snippet | Unimodal and bimodal nanoporous (mesoporous) carbons have been synthesized by simply removing silica from carbon/silica nanocomposites. The sucrose/silica... |
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| SubjectTerms | Bimodal Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Hierarchical Nanoporous carbon Porous materials Templating synthesis Unimodal |
| Title | Direct synthesis of unimodal and bimodal nanoporous carbon |
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