In situ FTIR spectra investigation of the photocatalytic degradation of gaseous toluene over a novel hedgehog-like CaFe2O4 hollow-structured materials
A novel hedgehog-like CaFe2O4 hollow microspheres was successfully fabricated by a simple template-assisted method with post-heat treatment. Especially, the hollow architecture was assembled by the nanorods, the surface areas could reach 111.5 m2·g−1. Due to the enhanced light scattering by the holl...
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| Published in | Catalysis communications Vol. 130; p. 105754 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.10.2019
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| Subjects | |
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| Abstract | A novel hedgehog-like CaFe2O4 hollow microspheres was successfully fabricated by a simple template-assisted method with post-heat treatment. Especially, the hollow architecture was assembled by the nanorods, the surface areas could reach 111.5 m2·g−1. Due to the enhanced light scattering by the hollow architecture, the effective charges separation by the assembled nanorods and the strong catalytic oxidizing performances by the Fe-base spinel material, the hedgehog-like CaFe2O4 catalysts showed marvelous catalytic performance for gaseous toluene degradation. Besides, by in situ FTIR technique, the degradation mechanism of gaseous toluene was clarified clearly based on the detected intermediates and final products in real time.
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•A novel hedgehog-like CaFe2O4 hollow microspheres were fabricated.•The photocatalytic degradation process was verified by the in situ FTIR spectra.•The gaseous toluene conversion ratio reached 76% after 8 h under mild conditions. |
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| AbstractList | A novel hedgehog-like CaFe2O4 hollow microspheres was successfully fabricated by a simple template-assisted method with post-heat treatment. Especially, the hollow architecture was assembled by the nanorods, the surface areas could reach 111.5 m2·g−1. Due to the enhanced light scattering by the hollow architecture, the effective charges separation by the assembled nanorods and the strong catalytic oxidizing performances by the Fe-base spinel material, the hedgehog-like CaFe2O4 catalysts showed marvelous catalytic performance for gaseous toluene degradation. Besides, by in situ FTIR technique, the degradation mechanism of gaseous toluene was clarified clearly based on the detected intermediates and final products in real time.
[Display omitted]
•A novel hedgehog-like CaFe2O4 hollow microspheres were fabricated.•The photocatalytic degradation process was verified by the in situ FTIR spectra.•The gaseous toluene conversion ratio reached 76% after 8 h under mild conditions. |
| ArticleNumber | 105754 |
| Author | Wang, Penglei Yang, Xudong Zhang, Long Yin, Zhifan Fan, Shiying Liu, Baojun Long, Dan Li, Xinyong Wang, Xinyang |
| Author_xml | – sequence: 1 givenname: Zhifan surname: Yin fullname: Yin, Zhifan organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 2 givenname: Baojun surname: Liu fullname: Liu, Baojun organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 3 givenname: Shiying surname: Fan fullname: Fan, Shiying organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 4 givenname: Penglei surname: Wang fullname: Wang, Penglei organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 5 givenname: Xinyang surname: Wang fullname: Wang, Xinyang organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 6 givenname: Dan surname: Long fullname: Long, Dan organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 7 givenname: Long surname: Zhang fullname: Zhang, Long organization: Xurihua Environmental Protection Technology, Wuhan, China – sequence: 8 givenname: Xudong surname: Yang fullname: Yang, Xudong organization: Xurihua Environmental Protection Technology, Wuhan, China – sequence: 9 givenname: Xinyong orcidid: 0000-0002-0495-6208 surname: Li fullname: Li, Xinyong email: xyli@dlut.edu.cn organization: State Key Laboratory of Fine Chemicals, Key Laboratory of Industrial Ecology and Environmental Engineering (MOE), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China |
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| Snippet | A novel hedgehog-like CaFe2O4 hollow microspheres was successfully fabricated by a simple template-assisted method with post-heat treatment. Especially, the... |
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| SubjectTerms | Gaseous toluene Hierarchical hollow architecture Photocatalysis Spinel-type CaFe2O4 |
| Title | In situ FTIR spectra investigation of the photocatalytic degradation of gaseous toluene over a novel hedgehog-like CaFe2O4 hollow-structured materials |
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